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1. 发明授权

US09005567B2 Method for producing isolatable oxide microparticles or hydroxide microparticles 有权
标题翻译：生产可分离氧化物微粒或氢氧化物微粒的方法
公开(公告)号：US09005567B2
公开(公告)日：2015-04-14
申请号：US13818954
申请日：2011-08-26
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C01B13/14 , C01G23/047 , C01G23/053 , B01F7/00 , C01B13/36 , C01F5/02 , C01F5/20 , C01F5/14 , C01F17/00 , B01D9/00 , C01G25/02 , C01G1/02 , B82Y30/00
CPC分类号： C01G23/0536 , B01D9/0009 , B01F7/00775 , B01F7/00791 , B82Y30/00 , C01B13/36 , C01F5/02 , C01F5/14 , C01F5/20 , C01F17/0043 , C01G1/02 , C01G23/0532 , C01G25/02 , C01P2002/54 , C01P2004/04 , C01P2004/64
摘要： A method for producing isolatable oxide microparticles or hydroxide microparticles using an apparatus that processes a fluid between processing surfaces of processing members that are arranged opposite each other so as to be able to approach to or separate from each other and such that at least one can rotate relative to the other. At least two fluids are mixed and oxide microparticles or hydroxide microparticles are separated, said two fluids including: a fluid containing a microparticle raw material solution comprising a microparticle raw material mixed into a solvent, and a fluid containing a microparticle-separation solution. Immediately thereafter, the following are mixed to obtain isolatable oxide microparticles or hydroxide microparticles: a fluid containing the separated oxide microparticles or hydroxide microparticles; and a fluid containing a microparticle-treatment-substance-containing solution that contains a microparticle-treatment substance that adjusts the dispersibility of the separated oxide microparticles or hydroxide microparticles.
摘要翻译：一种用于制造可分离氧化物微粒或氢氧化物微粒的方法，该方法使用处理相互相对布置的处理构件的处理表面之间的流体以便能够彼此接近或分离并使得至少一个可旋转的装置相对于另一个。混合至少两种流体，分离氧化物微粒或氢氧化物微粒，所述两种流体包括：含有混合在溶剂中的微粒原料的微粒原料溶液的流体和含有微粒分离溶液的流体。之后，混合以下物质，得到可分离的氧化物微粒或氢氧化物微粒：含有分离的氧化物微粒或氢氧化物微粒的流体; 以及含有含微粒处理物质的溶液的流体，其含有调节分离的氧化物微粒或氢氧化物微粒的分散性的微粒处理物质。

2. 发明授权

US09468891B2 Method for producing microparticles 有权
标题翻译：微粒的制造方法
公开(公告)号：US09468891B2
公开(公告)日：2016-10-18
申请号：US14005506
申请日：2012-03-21
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： B01F3/22 , B01F7/00 , B01J19/10 , B01J19/18 , B01J19/20 , B82Y30/00 , C01G9/02 , B01F13/10
CPC分类号： B01F3/22 , B01F7/00775 , B01F7/00791 , B01F13/1027 , B01F2215/0481 , B01J19/10 , B01J19/1806 , B01J19/1875 , B01J19/1887 , B01J19/20 , B01J2219/00779 , B82Y30/00 , C01G9/02 , C01P2004/54 , C01P2004/64
摘要： The problem addressed by the present invention is to provide a method for producing microparticles. Provided is a method that is for producing microparticles and that is characterized by containing at least the following two steps: (I) a step for preparing a microparticle starting material solution by dissolving at least one type of microparticle starting material in a solvent using high speed stirring or ultrasonic waves, and (II) a step for precipitating microparticles by mixing the microparticle starting material solution and at least one type of precipitation solvent for precipitating the microparticle starting material in a thin film fluid formed between at least two processing surfaces that are disposed facing each other, are able to approach/separate from each other, and of which at least one rotates relative to the others.
摘要翻译：本发明提出的问题在于提供一种微粒的制造方法。本发明提供一种制造微粒的方法，其特征在于至少包含以下两个步骤：（I）通过使用高速将至少一种微粒起始材料溶解在溶剂中来制备微粒原料溶液的步骤搅拌或超声波，以及（II）通过将微粒原料溶液与至少一种沉淀溶剂混合，使微粒起始材料沉淀在形成在至少两个处理表面之间的薄膜流体中沉淀微粒的步骤彼此面对，能够彼此接近/分离，并且其中至少一个相对于其他旋转。

3. 发明申请

US20140001663A1 METHOD FOR PRODUCING MICROPARTICLES 有权
标题翻译：生产微生物的方法
公开(公告)号：US20140001663A1
公开(公告)日：2014-01-02
申请号：US14005506
申请日：2012-03-21
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： B01F3/22
CPC分类号： B01F3/22 , B01F7/00775 , B01F7/00791 , B01F13/1027 , B01F2215/0481 , B01J19/10 , B01J19/1806 , B01J19/1875 , B01J19/1887 , B01J19/20 , B01J2219/00779 , B82Y30/00 , C01G9/02 , C01P2004/54 , C01P2004/64
摘要： The problem addressed by the present invention is to provide a method for producing microparticles. Provided is a method that is for producing microparticles and that is characterized by containing at least the the following two steps: (I) a step for preparing a microparticle starting material solution by dissolving at least one type of microparticle starting material in a solvent using high speed stirring or ultrasonic waves, and (II) a step for precipitating microparticles by mixing the microparticle starting material solution and at least one type of precipitation solvent for precipitating the microparticle starting material in a thin film fluid formed between at least two processing surfaces that are disposed facing each other, are able to approach/separate from each other, and of which at least one rotates relative to the others.
摘要翻译：本发明提出的问题在于提供一种微粒的制造方法。本发明提供一种生产微粒的方法，其特征在于，至少包含以下两个步骤：（I）通过使用高分子量将至少一种微粒原料溶解在溶剂中来制备微粒原料溶液的步骤速度搅拌或超声波，以及（II）通过将微粒原料溶液和至少一种沉淀溶剂混合使微粒起始材料沉淀在形成在至少两个处理表面之间的薄膜流体中而使微粒沉淀的步骤彼此面对地布置，能够彼此接近/分离，并且其中至少一个相对于另一个旋转。

4. 发明申请

US20130156682A1 METHOD FOR PRODUCING ISOLATABLE OXIDE MICROPARTICLES OR HYDROXIDE MICROPARTICLES 有权
标题翻译：生产不溶性氧化镁微量元素或羟基微量元素的方法
公开(公告)号：US20130156682A1
公开(公告)日：2013-06-20
申请号：US13818954
申请日：2011-08-26
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C01G23/053 , C01F5/14 , C01F17/00
CPC分类号： C01G23/0536 , B01D9/0009 , B01F7/00775 , B01F7/00791 , B82Y30/00 , C01B13/36 , C01F5/02 , C01F5/14 , C01F5/20 , C01F17/0043 , C01G1/02 , C01G23/0532 , C01G25/02 , C01P2002/54 , C01P2004/04 , C01P2004/64
摘要： A method for producing isolatable oxide microparticles or hydroxide microparticles using an apparatus that processes a fluid between processing surfaces of processing members that are arranged opposite each other so as to be able to approach to or separate from each other and such that at least one can rotate relative to the other. At least two fluids are mixed and oxide microparticles or hydroxide microparticles are separated, said two fluids including: a fluid containing a microparticle raw material solution comprising a microparticle raw material mixed into a solvent, and a fluid containing a microparticle-separation solution. Immediately thereafter, the following are mixed to obtain isolatable oxide microparticles or hydroxide microparticles: a fluid containing the separated oxide microparticles or hydroxide microparticles; and a fluid containing a microparticle-treatment-substance-containing solution that contains a microparticle-treatment substance that adjusts the dispersibility of the separated oxide microparticles or hydroxide microparticles.
摘要翻译：一种用于制造可分离氧化物微粒或氢氧化物微粒的方法，该方法使用处理相互相对布置的处理构件的处理表面之间的流体以便能够彼此接近或分离并使得至少一个可旋转的装置相对于另一个。混合至少两种流体，分离氧化物微粒或氢氧化物微粒，所述两种流体包括：含有混合在溶剂中的微粒原料的微粒原料溶液的流体和含有微粒分离溶液的流体。之后，混合以下物质，得到可分离的氧化物微粒或氢氧化物微粒：含有分离的氧化物微粒或氢氧化物微粒的流体; 以及含有含微粒处理物质的溶液的流体，其含有调节分离的氧化物微粒或氢氧化物微粒的分散性的微粒处理物质。

5. 发明授权

US09492763B2 Method for producing microparticles having controlled crystallite diameter 有权
标题翻译：具有受控微晶直径的微粒的制造方法
公开(公告)号：US09492763B2
公开(公告)日：2016-11-15
申请号：US14232124
申请日：2012-07-05
申请人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
发明人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
IPC分类号： B01D9/00 , C04B35/626 , C22B15/00 , B01J19/18
CPC分类号： B01D9/0063 , B01D9/0054 , B01J19/1887 , B01J2219/00085 , B01J2219/00164 , B01J2219/00177 , C04B35/626 , C22B15/0089
摘要： At least two types of fluids to be processed are mixed in a thin film fluid formed between at least two processing surfaces which are approachably and separably disposed facing each other. At least one processing surface rotates relative to the other, and a substance to be separated giving a controlled crystallite diameter is caused to separate. Specific conditions related to a fluid to be processed are varied to control the crystallite diameter of the substance to be separated. The specific conditions are the type of substance to be separated; the concentration of the substance to be separated included in the raw material fluid and/or substance included in the separating fluid; the pH of the raw material fluid and/or separating material fluid; the introduction temperature of the raw material fluid and/or separating fluid; and the introduction velocity of the raw material fluid and/or separating fluid.
摘要翻译：要处理的至少两种类型的流体在形成在彼此面对地和可分离地布置的至少两个处理表面之间的薄膜流体中混合。至少一个处理表面相对于另一个处理表面旋转，并且使被分离得到受控微晶直径的物质分离。改变与待处理流体有关的特定条件以控制待分离物质的微晶直径。具体条件是要分离的物质的类型; 要分离的物质的浓度包括在分离流体中包含的原料流体和/或物质中; 原料流体和/或分离材料流体的pH; 原料流体和/或分离流体的引入温度; 以及原料流体和/或分离流体的引入速度。

6. 发明申请

US20140155247A1 METHOD FOR PRODUCING MICROPARTICLES HAVING CONTROLLED CRYSTALLITE DIAMETER 有权
标题翻译：用于生产具有控制的结晶直径的微孔的方法
公开(公告)号：US20140155247A1
公开(公告)日：2014-06-05
申请号：US14232124
申请日：2012-07-05
申请人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
发明人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
IPC分类号： B01D9/00 , C04B35/626 , C22B15/00
CPC分类号： B01D9/0063 , B01D9/0054 , B01J19/1887 , B01J2219/00085 , B01J2219/00164 , B01J2219/00177 , C04B35/626 , C22B15/0089
摘要： At least two types of fluids to be processed are mixed in a thin film fluid formed between at least two processing surfaces which are approachably and separably disposed facing each other. At least one processing surface rotates relative to the other, and a substance to be separated giving a controlled crystallite diameter is caused to separate. Specific conditions related to a fluid to be processed are varied to control the crystallite diameter of the substance to be separated. The specific conditions are the type of substance to be separated; the concentration of the substance to be separated included in the raw material fluid and/or substance included in the separating fluid; the pH of the raw material fluid and/or separating material fluid; the introduction temperature of the raw material fluid and/or separating fluid; and the introduction velocity of the raw material fluid and/or separating fluid.
摘要翻译：要处理的至少两种类型的流体在形成在彼此面对地和可分离地布置的至少两个处理表面之间的薄膜流体中混合。至少一个处理表面相对于另一个处理表面旋转，并且使被分离得到受控微晶直径的物质分离。改变与待处理流体有关的特定条件以控制待分离物质的微晶直径。具体条件是要分离的物质的类型; 要分离的物质的浓度包括在分离流体中包含的原料流体和/或物质中; 原料流体和/或分离材料流体的pH; 原料流体和/或分离流体的引入温度; 以及原料流体和/或分离流体的引入速度。

7. 发明申请

US20140121336A1 METHOD FOR INCREASING PRODUCTION VOLUME OF FINE PARTICLES USING FORCED THIN FILM FLUID TREATMENT APPARATUS 有权
标题翻译：使用强力薄膜流体处理装置增加微粒生产量的方法
公开(公告)号：US20140121336A1
公开(公告)日：2014-05-01
申请号：US14123051
申请日：2012-03-15
申请人： Masaki Maekawa , Kaeko Araki , Daisuke Honda , Masakazu Enomura
发明人： Masaki Maekawa , Kaeko Araki , Daisuke Honda , Masakazu Enomura
IPC分类号： B22F9/16 , C07D471/04 , C01G23/08
CPC分类号： B22F9/16 , B01F3/1221 , B01F7/00775 , B01F7/00791 , B01J19/1887 , B22F1/0018 , B22F1/0022 , B22F1/0025 , B22F9/24 , B22F2998/10 , B22F2999/00 , C01G23/053 , C01G23/08 , C01P2004/04 , C07D471/04 , C22C5/06
摘要： The present invention addresses the problem of providing a new method for increasing the production of fine particles. Using at least two types of fluids to be processed, a raw material fluid containing at least one type of fine particle raw material and a fluid for treating the fine particle raw material, fine particles are obtained by mixing the fluids to be processed in a thin film fluid formed between at least two processing surfaces which are disposed to be faced with each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other. At this time, the production of the fine particles is increased by introducing the raw material fluid from the centers of the processing surfaces.
摘要翻译：本发明解决了提供用于增加细颗粒的生产的新方法的问题。使用至少两种类型的待处理流体，含有至少一种类型的细粒原料的原料流体和用于处理细粒原料的流体，通过将待处理的流体以薄的在至少两个处理表面之间形成的薄膜流体，所述至少两个处理表面被设置成彼此面对，以便能够彼此接近和分离，其中至少一个相对于另一个旋转。此时，通过从处理用面的中心引入原料液，能够提高微粒的制造。

8. 发明申请

US20130220180A1 SOLID SOLUTION PIGMENT NANOPARTICLES AND METHOD FOR PRODUCING SOLID SOLUTION PIGMENT NANOPARTICLES HAVING CONTROLLED SOLID SOLUTION RATIO 有权
标题翻译：固体溶剂颜料纳米粒子及其制备具有控制固体溶液比例的固体溶解性颜料纳米粒子的方法
公开(公告)号：US20130220180A1
公开(公告)日：2013-08-29
申请号：US13883692
申请日：2011-05-20
申请人： Masaki Maekawa , Kaeko Araki , Hideyuki Oka , Daisuke Honda , Masakazu Enomura
发明人： Masaki Maekawa , Kaeko Araki , Hideyuki Oka , Daisuke Honda , Masakazu Enomura
IPC分类号： C09C1/62
CPC分类号： C07F3/06 , B01D11/0269 , B01F3/0861 , B82Y30/00 , C01P2004/64 , C01P2004/82 , C07F1/08 , C09B67/0017 , C09B67/0019 , C09B67/0026 , C09B67/0035 , C09B67/0092 , C09C1/0081 , C09C1/04 , C09C1/627
摘要： The problem addressed by the present invention is to provide; solid solution pigment nanoparticles having a homogeneous solid solution ratio; a method for producing solid solution pigment nanoparticles having a homogeneous solid solution ratio in each primary particle; and a method for controlling the solid solution ratio of solid solution pigment nanoparticles. The solid solution pigment nanoparticles are prepared by precipitating at least two types of pigment by mixing a pigment precipitation solvent and; at least one type of pigment solution wherein at least two types of pigment are dissolved in a solvent: or at least two types of pigment solution wherein at least one type of pigment is dissolved in a solvent. The solid solution pigment nanoparticles are wherein the solid solution ratio of the at least two types of pigment in the primary particles of the precipitated solid solution pigment nanoparticles with respect to the ratio of the at least two types of pigment in the pigment solution mixed with the pigment precipitation solvent having a precision within 25%.
摘要翻译：本发明提出的问题在于：具有均匀固溶比的固溶颜料纳米粒子; 一种在一次粒子中具有均匀固溶比的固溶颜料纳米粒子的制造方法; 以及控制固溶颜料纳米粒子的固溶比的方法。固溶颜料纳米粒子是通过混合颜料沉淀溶剂和至少两种颜料沉淀来制备的; 至少一种类型的颜料溶液，其中至少两种类型的颜料溶解在溶剂中：或至少两种类型的颜料溶液，其中至少一种类型的颜料溶解在溶剂中。固溶颜料纳米粒子，其中沉淀的固溶颜料纳米颗粒的初级颗粒中的至少两种类型的颜料的固溶比相对于颜料溶液中的至少两种类型的颜料与颜料沉淀溶剂的精度在25％以内。

9. 发明申请

US20140110884A1 METHOD FOR PREVENTING ADHESION OF PROCESSED MATERIAL USING FORCED THIN FILM TREATMENT APPARATUS 审中-公开
标题翻译：使用强化薄膜处理设备防止加工材料粘合的方法
公开(公告)号：US20140110884A1
公开(公告)日：2014-04-24
申请号：US14122972
申请日：2012-03-15
申请人： Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： B29C33/60
CPC分类号： B29C33/60 , B01F7/00775 , B01F7/00791 , B01J19/1887 , B29C33/58 , C07D471/04
摘要： Provided is a method for preventing a processed material from adhering to a processing surface constituting a flow path for a fluid to be processed, in a fluid processing method for mixing a fluid to be processed in a thin film fluid formed between at least two oppositely arranged processing surfaces capable of being brought together and moved apart, at least one rotating in a relative manner with respect to the other; and for obtaining a processed material. There are used at least two types of fluids to be processed among a raw material fluid including at least one type of raw material substance, and a fluid for processing the raw material substance; the fluids to be processed are mixed in a thin film fluids formed between at least two oppositely arranged processing surfaces (1, 2) capable of being brought together and moved apart, at least one rotating in a relative manner with respect to the other; and a processed material is obtained. The raw material fluid is introduced from the middle of the processing surfaces (1, 2), whereby the raw material substance processed in the space between the processing surfaces (1, 2) is prevented from adhering to the processing surfaces (1, 2).
摘要翻译：提供了一种用于防止加工材料粘附到构成待处理流体的流动路径的处理表面的方法，用于在形成在至少两个相对布置的至少两个相对布置的薄膜流体之间的薄膜流体中混合待处理流体的流体处理方法处理表面能够被聚集并移动分开，至少一个相对于另一个以相对方式旋转; 并用于获得加工材料。在包括至少一种原料物质的原料流体和用于处理原料物质的流体中使用至少两种类型的待处理流体; 要处理的流体被混合在形成在至少两个相对布置的处理表面（1,2）之间的薄膜流体中，所述处理表面能够被聚集并移动分开，至少一个相对于另一个以相对方式旋转; 得到处理后的材料。原料流体从加工面（1,2）的中部引入，从而防止在处理用面（1,2）之间的空间中加工的原料物质附着在处理用面（1,2）上，。

10. 发明授权

US09539642B2 Method for increasing production volume of fine particles using forced thin film fluid treatment apparatus 有权
标题翻译：使用强制薄膜流体处理装置提高细粒产量的方法
公开(公告)号：US09539642B2
公开(公告)日：2017-01-10
申请号：US14123051
申请日：2012-03-15
申请人： Masaki Maekawa , Kaeko Araki , Daisuke Honda , Masakazu Enomura
发明人： Masaki Maekawa , Kaeko Araki , Daisuke Honda , Masakazu Enomura
IPC分类号： B01J13/00 , B22F9/16 , B01F7/00 , B01J19/18 , C01G23/08 , C07D471/04 , B01F3/12
CPC分类号： B22F9/16 , B01F3/1221 , B01F7/00775 , B01F7/00791 , B01J19/1887 , B22F1/0018 , B22F1/0022 , B22F1/0025 , B22F9/24 , B22F2998/10 , B22F2999/00 , C01G23/053 , C01G23/08 , C01P2004/04 , C07D471/04 , C22C5/06
摘要： A method for increasing the production of fine particles is provided. The method uses at least two types of fluids to be processed, a raw material fluid containing at least one type of fine particle raw material and a fluid for treating the fine particle raw material. Fine particles are obtained by mixing the fluids to be processed in a thin film fluid formed between at least two processing surfaces which are disposed to be faced with each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other. The production of the fine particles is increased by introducing the raw material fluid from the centers of the processing surfaces.
摘要翻译：提供了增加细颗粒生产的方法。该方法使用至少两种类型的待处理流体，含有至少一种类型的细粒原料的原料流体和用于处理细粒原料的流体。通过将待处理的流体混合在形成在至少两个处理表面之间的薄膜流体中，所述薄膜流体被设置成彼此面对，以便能够彼此接近和分离，所述薄膜流体中的至少一个其相对于另一个旋转。通过从处理表面的中心引入原料流体来增加细颗粒的生产。

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