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1. 发明授权

US3970703A Phenylacetic acid derivatives 失效
标题翻译：苯乙酸衍生物
公开(公告)号：US3970703A
公开(公告)日：1976-07-20
申请号：US533648
申请日：1974-12-17
申请人： Shigeyoshi Kitamura , Yositosi Okuno , Masachika Hirano
发明人： Shigeyoshi Kitamura , Yositosi Okuno , Masachika Hirano
IPC分类号： A01N31/04 , A01N37/36 , A01N43/10 , C07C43/00 , C07C69/76 , C07C43/22
CPC分类号： C07C43/00 , A01N31/04 , A01N37/36 , A01N43/10 , C07C69/76
摘要： A compound of the formula, ##SPC1##Wherein R.sub.1 is a C.sub.1.sub.-6 alkyl, a C.sub.2.sub.-6 alkenyl, a C.sub.3.sub.-6 alkynyl, a C.sub.3.sub.-6 cycloalkyl, benzyl, thienyl or a group of ##SPC2##(R.sub.4 is hydrogen, halogen, a C.sub.1.sub.-4 alkyl or methylenedioxy, and n is an integer of 1 to 5), R.sub.2 is a C.sub.1.sub.-6 alkyl, a C.sub.3.sub.-6 alkenyl or a C.sub.3.sub.-6 alkynyl, R.sub.3 is a C.sub.1.sub.-6 alkyl, a C.sub.3.sub.-6 alkenyl or a C.sub.3.sub.-6 alkynyl, (provided that R.sub.2 is a C.sub.3.sub.-6 alkynyl when R.sub.3 is a C.sub.1.sub.-6 alkyl), and A is a group of --COOR.sub.3 or --CH.sub.2 OR.sub.3, provided that R.sub.1 is a C.sub.1.sub.-6 alkyl, a C.sub.2.sub.-6 alkenyl, a C.sub.3.sub.-6 alkynyl, a C.sub.3.sub.-6 cycloalkyl or benzyl when A is a group of --CH.sub.2 OR.sub.3 (R.sub.3 is as defined above), and R.sub.3 is a C.sub.4.sub.-6 alkenyl or a C.sub.4.sub.-6 alkynyl when R.sub.1 is a group of ##SPC3##(R.sub.4 and n are as defined above) and A is a group of --COOR.sub.3, which is useful as synergist for insecticides, especially for a cyclopropane-carboxylate or a carbamate type insecticide.
摘要翻译：下式的化合物，其中R 1为C 1-6烷基，C 2-6烯基，C 3-6炔基，C 3-6环烷基，苄基，噻吩基或（R 4为氢，卤素， 4烷基或亚甲二氧基，n是1至5的整数），R 2是C 1-6烷基，C 3-6烯基或C 3-6炔基，R 3是C 1-6烷基，C 3-6烯基或（当R 3为C 1-6烷基时，R 2为C 3-6炔基），A为-COOR 3或-CH 2 OR 3基团，条件是R 1为C 1-6烷基，C 2 -6链烯基，C3-6炔基，C3-6环烷基或苄基，当A为-CH2OR3基团时（R3如上定义），R3为C4-6烯基或C4-6炔基，当R1为一组（R4和n如上所定义），A是一组-COOR3，其可用作杀虫剂的增效剂，特别是用于环丙烷羧酸盐或氨基甲酸酯类杀虫剂。

2. 发明授权

US4229469A Insecticidal alkadienylcyclopropanecarboxylates 失效
标题翻译：杀虫链烷二烯环丙烷羧酸酯
公开(公告)号：US4229469A
公开(公告)日：1980-10-21
申请号：US642920
申请日：1975-12-22
申请人： Toshio Mizutani , Nobushige Itaya , Nobuo Ohno , Takashi Matsuo , Shigeyoshi Kitamura , Yositosi Okuno
发明人： Toshio Mizutani , Nobushige Itaya , Nobuo Ohno , Takashi Matsuo , Shigeyoshi Kitamura , Yositosi Okuno
IPC分类号： C07C69/74 , A01N53/00 , A01N53/02 , A01N53/04 , C07D207/44 , C07D207/452 , C07D209/46 , C07D209/48 , C07D307/45 , C07D307/58 , C07D307/80 , C07D333/16 , C07D333/78 , C07D493/04 , A01N9/20 , C07C121/75
CPC分类号： C07D207/452 , A01N53/00 , C07D209/46 , C07D209/48 , C07D209/49 , C07D307/42 , C07D307/58 , C07D307/80 , C07D333/16 , C07D333/78 , C07D493/04
摘要： A compound of the formula, ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are respectively hydrogen atom or methyl, R.sub.5 is a member of ##STR2## wherein R.sub.6 is hydrogen atom or methyl, R.sub.7 is alkenyl, alkadienyl, alkynyl or benzyl, R.sub.8 is hydrogen atom, ethynyl or cyano, R.sub.9 is hydrogen atom, a halogen atom or alkyl, R.sub.10 is a halogen atom, alkyl, alkenyl, alkynyl, benzyl, thenyl, furylmethyl, phenoxy, substituted phenoxy or phenylthio, or R.sub.9 and R.sub.10 are bonded at the ends to form polymethylene chain containing or not containing oxygen or sulfur atom, Y is oxygen atom, sulfur atom or --CH.dbd.CH--, n is 1 or 2, Z is phthalimido, thiophthalimido, di- or tetra-hydrophthalimido or dialkylmaleimido, R.sub.11 is phenyl, thienyl or furyl and X is a halogen atom, which is useful as an active ingredient of insecticides.
摘要翻译：下式化合物，其中R 1，R 2，R 3和R 4分别是氢原子或甲基，R 5是其中R 6是氢原子或甲基，R 7是链烯基，，炔基或苄基，R8是氢原子，乙炔基或氰基，R9是氢原子，卤原子或烷基，R10是卤素原子，烷基，烯基，炔基，苄基，噻吩基，呋喃基甲基，苯氧基，取代的苯氧基或苯硫基，或R 9和R 10在末端键合以形成含有或不含氧原子或硫原子的多亚甲基链，Y为氧原子，硫原子或-CH = CH-，n为1或2，Z为苯二甲酰亚氨基，硫代邻苯二甲酰亚氨基，或四邻苯二甲酰亚胺基或二烷基马来酰亚胺基，R 11为苯基，噻吩基或呋喃基，X为卤素原子，其可用作杀虫剂的活性成分。

3. 发明授权

US4327109A Novel alkadienylcyclopropanecarboxylates 失效
标题翻译：新型的链二烯基环丙烷羧酸酯
公开(公告)号：US4327109A
公开(公告)日：1982-04-27
申请号：US142698
申请日：1980-04-22
申请人： Toshio Mizutani , Nobushige Itaya , Nobuo Ohno , Takashi Matsuo , Shigeyoshi Kitamura , Yositosi Okuno
发明人： Toshio Mizutani , Nobushige Itaya , Nobuo Ohno , Takashi Matsuo , Shigeyoshi Kitamura , Yositosi Okuno
IPC分类号： C07C69/74 , A01N53/00 , A01N53/02 , A01N53/04 , C07D207/44 , C07D207/452 , C07D209/46 , C07D209/48 , C07D307/45 , C07D307/58 , C07D307/80 , C07D333/16 , C07D333/78 , C07D493/04 , A01N43/10 , C07C69/587
CPC分类号： C07D207/452 , A01N53/00 , C07D209/46 , C07D209/48 , C07D209/49 , C07D307/42 , C07D307/58 , C07D307/80 , C07D333/16 , C07D333/78 , C07D493/04
摘要： A compound of the formula, ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are respectively hydrogen atom or methyl, R.sub.5 is a member of ##STR2## wherein R.sub.6 is hydrogen atom or methyl, R.sub.7 is alkenyl, alkadienyl, alkynyl or benzyl, R.sub.8 is hydrogen atom, ethynyl or cyano, R.sub.9 is hydrogen atom, a halogen atom or alkyl, R.sub.10 is a halogen atom, alkyl, alkenyl, alkynyl, benzyl, thenyl, furylmethyl, phenoxy, substituted phenoxy of phenylthio, or R.sub.9 and R.sub.10 are bonded at the ends to form polymethylene chain containing or not containing oxygen or sulfur atom, Y is oxygen atom, sulfur atom or --CH.dbd.CH--, n is 1 or 2, Z is phthalimido, thiophthalimido, di- or tetra-hydrophthalimido or dialkylmaleimido, R.sub.11 is phenyl, thienyl or furyl and X is a halogen atom, which is useful as an active ingredient of insecticides.
摘要翻译：下式化合物，其中R 1，R 2，R 3和R 4分别是氢原子或甲基，R 5是其中R 6是氢原子或甲基，R 7是链烯基，，炔基或苄基，R8是氢原子，乙炔基或氰基，R9是氢原子，卤素原子或烷基，R10是卤素原子，烷基，烯基，炔基，苄基，噻吩基，呋喃基甲基，苯氧基，苯硫基的取代苯氧基，或R 9和R 10在末端键合以形成含有或不含氧原子或硫原子的多亚甲基链，Y为氧原子，硫原子或-CH = CH-，n为1或2，Z为苯二甲酰亚氨基，硫代邻苯二甲酰亚氨基，或四邻苯二甲酰亚胺基或二烷基马来酰亚胺基，R 11为苯基，噻吩基或呋喃基，X为卤素原子，其可用作杀虫剂的活性成分。

4. 发明授权

US3998868A Alkadienylcyclopropanecarboxylates 失效
标题翻译：烷基二环氧乙烷
公开(公告)号：US3998868A
公开(公告)日：1976-12-21
申请号：US604789
申请日：1975-08-14
申请人： Toshio Mizutani , Nobushige Itaya , Nobuo Ohno , Takashi Matsuo , Shigeyoshi Kitamura , Yositosi Okuno
发明人： Toshio Mizutani , Nobushige Itaya , Nobuo Ohno , Takashi Matsuo , Shigeyoshi Kitamura , Yositosi Okuno
IPC分类号： C07D207/44 , C07D207/452 , C07D209/48 , C07D307/45 , C07D307/58 , C07C69/74
CPC分类号： C07D207/452 , C07D209/48 , C07D307/42 , C07D307/58 , Y10S514/939 , Y10S514/953 , Y10S514/957
摘要： A compound of the formula, ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are respectively hydrogen atom or methyl, R.sub.5 is a member of ##STR2## wherein R.sub.6 is hydrogen atom or methyl, R.sub.7 is alkenyl, alkadienyl, alkynyl or benzyl, R.sub.8 is hydrogen atom, ethynyl or cyano, R.sub.9 is hydrogen atom, a halogen atom or alkyl, R.sub.10 is a halogen atom, alkyl, alkenyl, alkynyl, benzyl, thenyl, furylmethyl, phenoxy, substituted phenoxy or phenylthio, or R.sub.9 and R.sub.10 are bonded at the ends to form polymethylene chain containing or not containing oxygen or sulfur atom, Y is oxygen atom, sulfur atom or --CH=CH--, n is 1 or 2, Z is phthalimido, thiophthalimido, di- or tetra-hydrophthalimido or dialkylmaleimido, R.sub.11 is phenyl, thienyl or furyl and X is a halogen atom, which is useful as an active ingredient of insecticides.

5. 发明授权

US3954814A Alkadienylcyclopropanecarboxylates 失效
标题翻译：二硬脂基环丙烷羧酸酯
公开(公告)号：US3954814A
公开(公告)日：1976-05-04
申请号：US265494
申请日：1972-06-23
申请人： Toshio Mizutani , Nobushige Itaya , Nobuo Ohno , Takashi Matsuo , Shigeyoshi Kitamura , Yositosi Okuno
发明人： Toshio Mizutani , Nobushige Itaya , Nobuo Ohno , Takashi Matsuo , Shigeyoshi Kitamura , Yositosi Okuno
IPC分类号： C07C69/74 , A01N53/00 , A01N53/02 , A01N53/04 , C07D207/44 , C07D207/452 , C07D209/46 , C07D209/48 , C07D307/45 , C07D307/58 , C07D307/80 , C07D333/16 , C07D333/78 , C07D493/04 , C07D307/44 , C07D307/42
CPC分类号： C07D207/452 , A01N53/00 , C07D209/46 , C07D209/48 , C07D209/49 , C07D307/42 , C07D307/58 , C07D307/80 , C07D333/16 , C07D333/78 , C07D493/04
摘要： A compound of the formula, ##EQU1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are respectively hydrogen atom or methyl, R.sub.5 is a member of ##SPC1##--CH.sub.2 Z or ##EQU2## wherein R.sub.6 is hydrogen atom or methyl, R.sub.7 is alkenyl, alkadienyl, alkynyl or benzyl, R.sub.8 is hydrogen atom, ethynyl or cyano, R.sub.9 is hydrogen atom, a halogen atom or alkyl, R.sub.10 is a halogen atom, alkyl, alkenyl, alkynyl, benzyl, thenyl, furylmethyl, phenoxy, substituted phenoxy or phenylthio, or R.sub.9 and R.sub.10 are bonded at the ends to form polymethylene chain containing or not containing oxygen or sulfur atom, Y is oxygen atom, sulfur atom or --CH=CH--, n is 1 or 2, Z is phthalimido, thiophthalimido, di- or tetra-hydrophthalimido or dialkylmaleimido, R.sub.11 is phenyl, thienyl or furyl and X is a halogen atom, which is useful as an active ingredient of insecticides.
摘要翻译：式R 3 R 4的化合物，其中R 1，R 2，R 3和R 4分别是氢原子或甲基，R 5，R 5，R 5，R 5，R 5，R 5，是-CH2Z或-CH2-CH = C-CH2-R11 | X的成员，其中R6是氢原子或甲基，R7是烯基，链二烯基，炔基或苄基，R8是氢原子，乙炔基或氰基，R9是氢原子卤素原子或烷基，R 10为卤素原子，烷基，烯基，炔基，苄基，噻吩基，呋喃基甲基，苯氧基，取代的苯氧基或苯硫基，或R 9和R 10在末端键合形成含有或不含氧的多亚甲基或硫原子，Y为氧原子，硫原子或-CH = CH-，n为1或2，Z为苯二甲酰亚氨基，硫代邻苯二甲酰亚氨基，二 - 或四 - 邻苯二甲酰亚氨基或二烷基马来酰亚氨基，R11为苯基，噻吩基或呋喃基，X为卤素原子，其可用作杀虫剂的活性成分。

6. 发明授权

US4028438A Phosphorothiolates 失效
标题翻译：磷硫酸盐
公开(公告)号：US4028438A
公开(公告)日：1977-06-07
申请号：US415682
申请日：1973-11-14
申请人： Hiroshi Tsuchiya , Kunio Mukai , Akio Kimura , Hiroshi Taya , Keimei Fujimoto , Toshiaki Ozaki , Sigeo Yamamoto , Taizo Ogawa , Tadashi Ooishi , Yositosi Okuno
发明人： Hiroshi Tsuchiya , Kunio Mukai , Akio Kimura , Hiroshi Taya , Keimei Fujimoto , Toshiaki Ozaki , Sigeo Yamamoto , Taizo Ogawa , Tadashi Ooishi , Yositosi Okuno
IPC分类号： A01N57/10 , A01N57/14 , C07F9/18 , C07F9/553 , C07F9/165 , A01N9/36
CPC分类号： A01N57/10 , A01N57/14 , C07F9/18 , C07F9/5537
摘要： Phosphorothiolates represented by the formula, ##STR1## wherein R is an alkyl; A is an alkyl, haloalkyl, alkenyl, alkinyl, alkylthioalkyl, phenylthioalkyl, phthalimidoalkyl or phenylalkyl; X is hydrogen, a halogen or an alkyl; and n is an integer of 1 to 5, are obtained by (1) reacting sodium or potassium hydrosulfide with a compound represented by the formula, ##STR2## WHEREIN R, X, and n have the same significances as mentioned above, to prepare a thiophosphate represented by the formula, ##STR3## wherein R, X and n have the same significances as mentioned above; and M is an alkali metal, and then (2) reacting said thiophosphate with a halide represented by the formula,Y--Awherein A has the same significance as mentioned above; and Y is a halogen.The phosphorothiolates have insecticidal and fungicidal activities.
摘要翻译：由式表示的硫代硫酸酯，其中R是烷基; 烷基，卤代烷基，烯基，炔基，烷硫基烷基，苯硫基烷基，苯二甲酰亚氨基烷基或苯基烷基; X是氢，卤素或烷基; （1）使氢硫化钠或氢氧化钾与下式表示的化合物反应得到，其中R 1，X，和n具有与上述相同的含义，从而制备由式表示的硫代磷酸酯，

7. 发明授权

US4113864A Phosphorothiolate pesticidal composition 失效
标题翻译：磷酸盐杀虫剂组合物
公开(公告)号：US4113864A
公开(公告)日：1978-09-12
申请号：US768875
申请日：1977-02-15
申请人： Hiroshi Tsuchiya , Kunio Mukai , Akio Kimura , Hiroshi Taya , Keimei Fujimoto , Toshiaki Ozaki , Sigeo Yamamoto , Taizo Ogawa , Tadashi Ooishi , Yositosi Okuno
发明人： Hiroshi Tsuchiya , Kunio Mukai , Akio Kimura , Hiroshi Taya , Keimei Fujimoto , Toshiaki Ozaki , Sigeo Yamamoto , Taizo Ogawa , Tadashi Ooishi , Yositosi Okuno
IPC分类号： A01N57/10 , A01N57/14 , C07F9/18 , C07F9/553 , A01N9/00 , A01N9/36
CPC分类号： C07F9/5537 , A01N57/10 , A01N57/14 , C07F9/18
摘要： Phosphorothiolates represented by the formula, ##STR1## wherein R is an alkyl; A is an alkyl, haloalkyl, alkenyl, alkinyl, alkylthioalkyl, phenylthioalkyl, phthalimidoalkyl or phenylalkyl; X is hydrogen, a halogen or an alkyl; and n is an integer of 1 to 5, are obtained by (1) reacting sodium or potassium hydrosulfide with a compound represented by the formula, ##STR2## WHEREIN R, X and n have the same significances as mentioned above, to prepare a thiophosphate represented by the formula, ##STR3## wherein R, X and n have the same significances as mentioned above; and M is an alkali metal, and then (2) reacting said thiophosphate with a halide represented by the formula,Y -- Awherein A has the same significance as mentioned above; and Y is a halogen.The phosphorothiolates have insecticidal and fungicidal activities.

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