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1. 发明授权

US4473561A Fungicidal composition comprising alpha-substituted ethylphosphinic acids or their salts 失效
标题翻译：包含α-取代的乙基次膦酸或其盐的杀真菌组合物
公开(公告)号：US4473561A
公开(公告)日：1984-09-25
申请号：US365957
申请日：1982-04-06
申请人： Yukio Ishiguri , Yoshimi Yamada , Toshiro Kato , Mitsuru Sasaki , Kunio Mukai
发明人： Yukio Ishiguri , Yoshimi Yamada , Toshiro Kato , Mitsuru Sasaki , Kunio Mukai
IPC分类号： A01N57/20 , C07F9/48 , A01N9/36
CPC分类号： C07F9/4816 , A01N57/20
摘要： A fungicidal composition which comprises as an active ingredient a fungicidally effective amount of a compound of the formula: ##STR1## wherein X is a hydroxyl group or a hydroxyamino group, or its salt and an inert carrier or diluent.
摘要翻译：一种杀真菌组合物，其包含杀真菌有效量的下式化合物作为活性成分：其中X为羟基或羟基氨基，或其盐和惰性载体或稀释剂。

2. 发明授权

US4308258A Pyrimidin-4-yl-phosphorus esters and insecticidal, acaricidal or nematocidal compositions and methods using them 失效
标题翻译：嘧啶-4-基 - 磷酯和杀虫，杀螨或杀线虫的组合物和使用它们的方法
公开(公告)号：US4308258A
公开(公告)日：1981-12-29
申请号：US114737
申请日：1980-01-24
申请人： Takayuki Okabe , Kunio Mukai , Masachika Hirano
发明人： Takayuki Okabe , Kunio Mukai , Masachika Hirano
IPC分类号： A01N57/16 , A01N57/32 , C07D239/36 , C07F9/6512 , C07F9/65
CPC分类号： C07D239/36 , A01N57/16 , A01N57/32 , C07F9/65125
摘要： Pyrimidin-4-yl-phosphorothionates of the formula (I), ##STR1## wherein R is a C.sub.1 -C.sub.2 alkyl group, R.sub.1 is a C.sub.1 -C.sub.2 alkoxyl or C.sub.1 -C.sub.4 alkylamino group, R.sub.2 and R.sub.3, which may be the same or different, are each a halogen atom, a C.sub.1 -C.sub.3 alkoxyl or methylmercapto group, and X is an oxygen or sulfur atom; a process for producing pyrimidin-4-yl-phosphorothionates of the formula (I) characterized by condensing a 4-hydroxypyrimidine of the formula (II), ##STR2## wherein R.sub.2 and R.sub.3, which may be the same or different, are each a halogen atom, a C.sub.1 -C.sub.3 alkoxyl or methylmercapto group, with a halogen compound of the formula, ##STR3## wherein R is a C.sub.1 -C.sub.2 alkyl, R.sub.1 is a C.sub.1 -C.sub.2 alkoxyl or C.sub.1 -C.sub.4 alkylamino group, Y is a halogen atom and X is an oxygen or sulfur atom; an insecticide, acaricide and nematocide characterized by containing pyrimidin-4-yl-phosphorothionates of the formula (I) as an active ingredient; 4-hydroxypyrimidines of the formula (II) wherein R.sub.2 and R.sub.3, which may be the same or different, are each a halogen atom, a C.sub.2 -C.sub.3 alkoxyl or methylmercapto group; and a process for producing 4-hydroxypyrimidines of the formula (II) wherein R.sub.2 and R.sub.3, which may be the same or different, are each a halogen atom, a C.sub.2 -C.sub.3 alkoxyl or methylmercapto group, characterized by reacting an acetamidine hydrochloride of the formula, ##STR4## wherein R.sub.4 is a halogen atom, a C.sub.2 -C.sub.3 alkoxyl or methylmercapto group, with a .beta.-ketoester of the formula, ##STR5## wherein R.sub.5 is a halogen atom, a C.sub.2 -C.sub.3 alkoxyl or methylmercapto group, and R.sub.6 is a C.sub.1 -C.sub.2 alkyl group.
摘要翻译：式（I）的嘧啶-4-基 - 硫代磷酸酯，其中R是C1-C2烷基，R1是C1-C2烷氧基或C1-C4烷基氨基，R2和R3可以是各自为卤素原子，C1-C3烷氧基或甲基巯基，X为氧或硫原子; 制备式（I）的嘧啶-4-基 - 硫代磷酸酯的方法，其特征在于将式（II）的4-羟基嘧啶，其中R2和R3可以相同或不同，其中R为C1-C2烷基，R1为C1-C2烷氧基或C1-C4烷基氨基，Y为卤素原子，C1-C3烷氧基或甲基巯基，是卤素原子，X是氧或硫原子; 杀虫剂，杀螨剂和杀线虫剂，其特征在于含有式（I）的嘧啶-4-基 - 硫代磷酸酯作为活性成分; 式（II）的4-羟基嘧啶，其中R2和R3可以相同或不同，分别为卤素原子，C2-C3烷氧基或甲基巯基; 以及制备式（II）的4-羟基嘧啶的方法，其中R 2和R 3可以相同或不同，各自为卤素原子，C 2 -C 3烷氧基或甲基巯基，其特征在于使乙酸脒盐酸盐其中R 4是卤素原子，C 2 -C 3烷氧基或甲基巯基，与下式的β-酮酯，其中R 5是卤素原子，C 2 -C 3烷氧基或甲基巯基，和 R6是C1-C2烷基。

3. 发明授权

US4507284A Soil disinfectant 失效
标题翻译：土壤消毒剂
公开(公告)号：US4507284A
公开(公告)日：1985-03-26
申请号：US413141
申请日：1982-08-30
申请人： Yoshimi Yamada , Tadashi Ooishi , Toshiro Kato , Kunio Mukai
发明人： Yoshimi Yamada , Tadashi Ooishi , Toshiro Kato , Kunio Mukai
IPC分类号： A01N57/22 , C07F9/48 , A01N57/00
CPC分类号： A01N57/22 , C07F9/4841
摘要： A soil disinfectant composition for preventing and controlling diseases caused by pathogenic fungi living in soil, which comprises an effective amount of at least one of phenylphosphinic acid and its salts as an active ingredient, and at least one inert carrier or diluent.

4. 发明授权

US4366150A Soil disinfectants and method of use 失效
标题翻译：土壤消毒剂及使用方法
公开(公告)号：US4366150A
公开(公告)日：1982-12-28
申请号：US210618
申请日：1980-11-26
申请人： Yoshimi Yamada , Tadashi Ooishi , Toshiro Kato , Kunio Mukai
发明人： Yoshimi Yamada , Tadashi Ooishi , Toshiro Kato , Kunio Mukai
IPC分类号： A01N57/22 , C07F9/48
CPC分类号： A01N57/22 , C07F9/4841
摘要： A soil disinfectant composition for preventing and controlling diseases caused by pathogenic fungi living in soil, which comprises an effective amount of at least one of phenylphosphinic acid and its salts as an active ingredient, and at least one inert carrier or diluent.
摘要翻译：一种用于预防和控制由生活在土壤中的病原真菌引起的疾病的土壤消毒剂组合物，其包含有效量的至少一种苯基次膦酸及其盐作为活性成分，以及至少一种惰性载体或稀释剂。

5. 发明授权

US4015974A Amido phosphorothiolates 失效
标题翻译：酰氨基硫代磷酸酯
公开(公告)号：US4015974A
公开(公告)日：1977-04-05
申请号：US618264
申请日：1975-09-30
申请人： Takeo Satomi , Naganori Hino , Koshi Tateishi , Masachika Hirano , Kunio Mukai , Katsuji Nodera , Mitsuru Sasaki
发明人： Takeo Satomi , Naganori Hino , Koshi Tateishi , Masachika Hirano , Kunio Mukai , Katsuji Nodera , Mitsuru Sasaki
IPC分类号： A01N57/16 , C07F9/553 , C07D211/16
CPC分类号： C07F9/5532 , A01N57/16
摘要： The present invention relates to compounds of the formula: ##STR1## wherein R.sub.1 is lower alkyl, lower alkenyl, lower alkynyl, cycloalkyl, unsubstituted aralkyl, lower alkyl or halogen-substituted aralkyl or halogen-substituted alkenyl; R.sub.2 is lower alkyl; Y is hydrogen or methyl and X is lower alkyl; n is an integer of 1 to 5, and a method of producing these compounds. These compounds are eminently suited for killing weeds, injurious insects, nematodes and acaricides.
摘要翻译：本发明涉及下式的化合物：其中R 1为低级烷基，低级烯基，低级炔基，环烷基，未取代的芳烷基，低级烷基或卤素取代的芳烷基或卤素取代的链烯基; R2是低级烷基; Y是氢或甲基，X是低级烷基; n为1〜5的整数，以及这些化合物的制造方法。这些化合物特别适用于杀死杂草，有害昆虫，线虫和杀螨剂。

6. 发明授权

US3982921A Organo phosphorus herbicides 失效
标题翻译：有机磷除草剂
公开(公告)号：US3982921A
公开(公告)日：1976-09-28
申请号：US536220
申请日：1974-12-24
申请人： Takeo Satomi , Kunio Mukai , Akihiko Mine , Naganori Hino , Kohshi Tateishi , Masachika Hirano
发明人： Takeo Satomi , Kunio Mukai , Akihiko Mine , Naganori Hino , Kohshi Tateishi , Masachika Hirano
IPC分类号： C07F9/24 , A01N9/36
CPC分类号： C07F9/242
摘要： O-alkyl-O-(3-methyl-6-nitrophenyl)-N-secondary butyl-phosphorothionoamidate, which possesses herbicidal properties.
摘要翻译： O-烷基-O-（3-甲基-6-硝基苯基）-N-仲丁基 - 硫代磷酰胺，具有除草性。

7. 发明授权

US3953546A Thio(dithio)phosphorates 失效
标题翻译：硫（二硫）磷酸盐
公开(公告)号：US3953546A
公开(公告)日：1976-04-27
申请号：US487670
申请日：1974-07-11
申请人： Masachika Hirano , Kunio Mukai , Hisami Takeda
发明人： Masachika Hirano , Kunio Mukai , Hisami Takeda
IPC分类号： A01N57/14 , C07F9/18 , A01N9/36
CPC分类号： A01N57/14 , C07F9/18
摘要： Thio(dithio)-phosphorate of the formula, ##SPC1##Wherein A represents an alkyl having up to 6 carbon atoms; B represents lower alkyl having up to 4 carbon atoms; Y represents halogen, methoxy or ethoxy; X represents oxygen or sulfur; R.sub.1 represents alkyl having up to 6 carbon atoms, phenyl, phenyl substituted by halogen or phenyl substituted by lower alkyl having up to 4 carbon atoms; R.sub.2 represents hydrogen or alkyl having up to 6 carbon atoms; R.sub.3 represents hydrogen or alkyl having up to 6 carbon atoms; and n represents 0, 1 or 2, which is useful as a pesticide.
摘要翻译：硫代（二硫代） - 磷酸酯，其中A代表具有至多6个碳原子的烷基; B代表具有至多4个碳原子的低级烷基; Y表示卤素，甲氧基或乙氧基; X表示氧或硫; R 1表示具有至多6个碳原子的烷基，苯基，被卤素取代的苯基或被具有至多4个碳原子的低级烷基取代的苯基; R2代表氢或具有至多6个碳原子的烷基; R3表示氢或具有至多6个碳原子的烷基; n表示0,1或2，可用作农药。

8. 发明授权

US4320126A Triazinyl-organophosphorus esters 失效
标题翻译：三嗪基有机磷酯
公开(公告)号：US4320126A
公开(公告)日：1982-03-16
申请号：US70056
申请日：1979-08-27
申请人： Takayuki Okabe , Kunio Mukai , Masachika Hirano
发明人： Takayuki Okabe , Kunio Mukai , Masachika Hirano
IPC分类号： A01N57/08 , A01N57/24 , C07D251/30 , C07F9/6521 , C07D251/34 , A01N43/66
CPC分类号： C07D251/30 , A01N57/08 , C07F9/65215
摘要： Organophosphorus esters of the formula (I), ##STR1## wherein R is a C.sub.1 -C.sub.2 alkyl group, R.sub.1 is a C.sub.1 -C.sub.2 alkyl, C.sub.1 -C.sub.2 alkoxy, C.sub.1 -C.sub.4 alkylamino, phenyl or phenoxy group, R.sub.2 and R.sub.3, which may be the same or different, are each a C.sub.1 -C.sub.5 alkyl or methoxy C.sub.2 -C.sub.3 alkyl group and X is an oxygen or sulfur atom, a method for producing organophosphorus esters of the formula (I) characterized by condensation reaction of s-triazines of the formula, ##STR2## wherein M is a potassium or sodium atom and R.sub.2 and R.sub.3 are as defined above, with a halogenated compound of the formula, ##STR3## wherein Y is a halogen atom and R, R.sub.1 and X are as defined above, and an insecticide, acaricide and/or nematocide characterized by containing organophosphorus esters of the formula (I) as an active ingredient.
摘要翻译：式（I）的有机磷酯，其中R是C1-C2烷基，R1是C1-C2烷基，C1-C2烷氧基，C1-C4烷基氨基，苯基或苯氧基，R2和 R3可以相同或不同，分别为C1-C5烷基或甲氧基C2-C3烷基，X为氧或硫原子，制备式（I）的有机磷酯的方法，其特征在于：其中M是钾或钠原子，R 2和R 3如上定义，与下式的卤代化合物，其中Y是卤素原子，R 1，R 2和X 其特征在于含有式（I）的有机磷酯作为活性成分，所述杀虫剂，杀螨剂和/或杀线虫剂的定义如上。

9. 发明授权

US4028438A Phosphorothiolates 失效
标题翻译：磷硫酸盐
公开(公告)号：US4028438A
公开(公告)日：1977-06-07
申请号：US415682
申请日：1973-11-14
申请人： Hiroshi Tsuchiya , Kunio Mukai , Akio Kimura , Hiroshi Taya , Keimei Fujimoto , Toshiaki Ozaki , Sigeo Yamamoto , Taizo Ogawa , Tadashi Ooishi , Yositosi Okuno
发明人： Hiroshi Tsuchiya , Kunio Mukai , Akio Kimura , Hiroshi Taya , Keimei Fujimoto , Toshiaki Ozaki , Sigeo Yamamoto , Taizo Ogawa , Tadashi Ooishi , Yositosi Okuno
IPC分类号： A01N57/10 , A01N57/14 , C07F9/18 , C07F9/553 , C07F9/165 , A01N9/36
CPC分类号： A01N57/10 , A01N57/14 , C07F9/18 , C07F9/5537
摘要： Phosphorothiolates represented by the formula, ##STR1## wherein R is an alkyl; A is an alkyl, haloalkyl, alkenyl, alkinyl, alkylthioalkyl, phenylthioalkyl, phthalimidoalkyl or phenylalkyl; X is hydrogen, a halogen or an alkyl; and n is an integer of 1 to 5, are obtained by (1) reacting sodium or potassium hydrosulfide with a compound represented by the formula, ##STR2## WHEREIN R, X, and n have the same significances as mentioned above, to prepare a thiophosphate represented by the formula, ##STR3## wherein R, X and n have the same significances as mentioned above; and M is an alkali metal, and then (2) reacting said thiophosphate with a halide represented by the formula,Y--Awherein A has the same significance as mentioned above; and Y is a halogen.The phosphorothiolates have insecticidal and fungicidal activities.
摘要翻译：由式表示的硫代硫酸酯，其中R是烷基; 烷基，卤代烷基，烯基，炔基，烷硫基烷基，苯硫基烷基，苯二甲酰亚氨基烷基或苯基烷基; X是氢，卤素或烷基; （1）使氢硫化钠或氢氧化钾与下式表示的化合物反应得到，其中R 1，X，和n具有与上述相同的含义，从而制备由式表示的硫代磷酸酯，

10. 发明授权

US4023956A Amide phosphorothiolate herbicides 失效
标题翻译：酰胺硫代磷酸酯除草剂
公开(公告)号：US4023956A
公开(公告)日：1977-05-17
申请号：US611606
申请日：1975-09-09
申请人： Ryo Yoshida , Takeo Satomi , Kunio Mukai , Masachika Hirano
发明人： Ryo Yoshida , Takeo Satomi , Kunio Mukai , Masachika Hirano
IPC分类号： A01N57/14 , A01P5/00 , A01P7/04 , A01P13/00 , C07F9/165 , C07F9/173 , A01N9/36
CPC分类号： A01N57/14 , C07F9/1651
摘要： Compounds of the formula ##STR1## WHERE R.sub.1 is lower alkenyl, optionally substituted by chlorine or bromine, or R.sub.1 is alkoxyalkyl; R.sub.2 and R.sub.3 are lower alkyl; R.sub.4 is lower alkyl, lower alkoxy or halogen; and n is zero or an integer of 1-5, which are useful as herbicides, insecticides, acaricides and nematocides.
摘要翻译：其中R 1为任选被氯或溴取代的低级链烯基，或R 1为烷氧基烷基; R2和R3是低级烷基; R4是低级烷基，低级烷氧基或卤素; n为零或1-5的整数，其可用作除草剂，杀虫剂，杀螨剂和杀线虫剂。

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