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    • 1. 发明授权
    • Method for enrichment and purification of aqueous hydrogen peroxide
solution
    • 富含和纯化过氧化氢水溶液的方法
    • US5456898A
    • 1995-10-10
    • US303834
    • 1994-09-09
    • Shigeki ShimokawaYoshitsugu MinamikawaSeishi Murakami
    • Shigeki ShimokawaYoshitsugu MinamikawaSeishi Murakami
    • C01B15/013C01B15/01
    • C01B15/013C01B15/0135
    • Proposed is an improvement in a method for the preparation of an enriched and purified aqueous hydrogen peroxide solution from a crude aqueous hydrogen peroxide solution comprising the steps of evaporating the crude aqueous hydrogen peroxide solution in an evaporator into vapor with accompanying liquid in the form of a mist, separating the vapor from the mist of liquid in a gas-liquid separator and subjecting the vapor to fractionating distillation in a fractionating distillation column in order to greatly upgrade the product solution relative to the impurity content. The improvement is achieved by subjecting the crude aqueous hydrogen peroxide solution, prior to introduction into the evaporator, to a contacting treatment with a porous synthetic adsorbent resin to remove organic impurities from the crude aqueous hydrogen peroxide solution to such an extent that the crude aqueous hydrogen peroxide solution after the contacting treatment contains organic impurities in an amount not exceeding 50 ppm by weight calculated as organic carbon. Although the mechanism is not well understood, the preliminary removal of organic impurities from the crude aqueous hydrogen peroxide solution has an effect of greatly increasing the efficiency of gas-liquid separation of the vapor accompanied by a mist of liquid in the gas-liquid separator to decrease the amount of contaminant impurities introduced into the distillation column as carried by the mist.
    • 提出了从粗制过氧化氢水溶液制备富集和纯化的过氧化氢水溶液的方法的改进,包括以下步骤:将蒸发器中的粗过氧化氢水溶液蒸发成蒸汽,伴随液体为 在气 - 液分离器中分离蒸气与液雾的蒸气,并在分馏蒸馏塔中对蒸汽进行分馏,以相对于杂质含量大大提升产物溶液。 改进之处在于,将粗水过氧化氢溶液在引入蒸发器之前,与多孔合成吸附剂树脂进行接触处理以从粗过氧化氢水溶液中除去有机杂质,使得粗制氢水 接触处理后的过氧化物溶液含有不超过作为有机碳计算的50重量ppm的有机杂质。 虽然机理尚不清楚,但是从粗过氧化氢水溶液中初步除去有机杂质具有大大提高伴随气液分离器中的液体雾气的气液分离效率, 减少由雾气引入到蒸馏塔中的污染物杂质的量。
    • 6. 发明授权
    • Semiconductor processing system
    • 半导体处理系统
    • US07351291B2
    • 2008-04-01
    • US10368569
    • 2003-02-20
    • Seishi Murakami
    • Seishi Murakami
    • C23C16/00H01L21/306C23F1/00
    • H01L21/67167C23C16/54H01L21/67017H01L21/6719H01L21/67196H01L21/67201
    • A semiconductor processing system includes a load lock chamber and first to third process chambers connected to an airtight transfer chamber. The second process chamber is disposed below the first process chamber and overlaps with the first process chamber. The third process chamber is disposed at a position laterally distant from the first process chamber and leveled with the first process chamber. First to third exhaust ports are formed in the bottoms of the first to third process chambers, and connected to respective vacuum exhaust sections through first to third exhaust lines. A transfer mechanism is disposed in the transfer chamber to transfer a target substrate to and from the load lock chamber and the first to third process chambers.
    • 半导体处理系统包括负载锁定室和连接到气密传送室的第一至第三处理室。 第二处理室设置在第一处理室下方并与第一处理室重叠。 第三处理室设置在横向远离第一处理室的位置并与第一处理室平齐。 第一至第三排气口形成在第一至第三处理室的底部,并通过第一至第三排气管线连接至相应的真空排气段。 传送机构设置在传送室中以将目标基板传送到负载锁定室和第一至第三处理室。
    • 8. 发明授权
    • Barrier metal layer
    • 阻隔金属层
    • US5880526A
    • 1999-03-09
    • US843239
    • 1997-04-14
    • Tatsuo HatanoSeishi Murakami
    • Tatsuo HatanoSeishi Murakami
    • H01L21/28H01L21/3205H01L21/768H01L23/52H01L23/532H01L23/48
    • H01L21/76843H01L21/76856H01L23/53223H01L23/53257H01L2924/0002Y10S257/915
    • A barrier metal layer comprises a titanium film having a surface nitrided and modified by a nitrogen compound containing nitrogen atoms, and a titanium nitride film formed on a surface of the titanium film. The titanium film and titanium nitride film are interposed between a base layer, or a lower layer of a semiconductor device, and a metal film or an upper layer of the semiconductor device. A method of forming a barrier metal layer comprises the steps of forming a titanium film on an entire surface of an insulating layer including an inner wall of a hole, which hole is formed in a predetermined portion of the insulating layer to electrically connect a lower wiring layer and an upper wiring layer constituting a multilevel inter-connection structure of a semiconductor device, the upper wiring layer being provided on the insulating layer, the insulating layer being deposited on the lower wiring layer, the hole being formed to reach the lower wiring layer, and also forming the titanium film on a surface of the lower wiring layer exposed to a bottom of the hole, nitriding and modifying the titanium film by exposing the titanium film in an atmosphere of a nitrogen compound containing nitrogen atoms, and forming a titanium nitride film on the modified titanium film, the upper wiring layer being deposited on the titanium nitride layer.
    • 阻挡金属层包括具有氮表面氮化并被含氮原子改性的钛膜和形成在钛膜表面上的氮化钛膜。 钛膜和氮化钛膜介于半导体器件的基底层或下层之间,半导体器件的金属膜或上层之间。 形成阻挡金属层的方法包括以下步骤:在包括孔的内壁的绝缘层的整个表面上形成钛膜,该绝缘层在绝缘层的预定部分形成孔,以将下部布线 层和构成半导体器件的多层互连结构的上布线层,所述上布线层设置在所述绝缘层上,所述绝缘层沉积在所述下布线层上,所述孔形成为到达所述下布线层 并且在暴露于孔的底部的下布线层的表面上形成钛膜,通过在含有氮原子的氮化合物的气氛中暴露钛膜来氮化和改性钛膜,并且形成氮化钛 在该改性钛膜上形成薄膜,上部布线层沉积在氮化钛层上。
    • 9. 发明授权
    • Processing apparatus and heater unit
    • 加工设备和加热器单元
    • US08106335B2
    • 2012-01-31
    • US11631485
    • 2005-07-01
    • Seishi MurakamiKunihiro Tada
    • Seishi MurakamiKunihiro Tada
    • H05B3/68
    • C23C16/46C23C16/4586H01L21/67109H05B3/143
    • A processing apparatus has a placement stage that prevents generation of a crack due to heating of an embedded heater. The placement stage (32A) on which a wafer (W) is placed has a plurality of areas (32Aa, 32Ab) so that one of the plurality of heaters is embedded independently in each of the plurality of areas. The heater (35Aa) embedded in one area (32Aa) of adjacent areas has a part (35Aa2) extending in the other area (32Ab) of the adjacent areas, and the heater (35Ab) embedded in the other area (32Ab) of the adjacent areas has a part (35Ab2) extending in the one area (32Aa).
    • 处理装置具有防止由于嵌入式加热器的加热而产生裂缝的放置台。 其上放置晶片(W)的放置台(32A)具有多个区域(32Aa,32Ab),使得多个加热器中的一个独立地嵌入在多个区域中的每个区域中。 嵌入在相邻区域的一个区域(32Aa)中的加热器(35Aa)具有在相邻区域的另一区域(32Ab)中延伸的部分(35Aa2),并且嵌入在相邻区域的另一区域(32Ab)中的加热器 相邻区域具有在一个区域(32Aa)中延伸的部分(35Ab2)。