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1. 发明授权

US6071606A Hydrophilic film and method for forming same on substrate 失效
标题翻译：亲水膜及其在基材上的形成方法
公开(公告)号：US6071606A
公开(公告)日：2000-06-06
申请号：US917617
申请日：1997-08-26
申请人： Seiji Yamazaki , Kensuke Makita , Yasuaki Kai , Satoko Sugawara , Takashi Seino
发明人： Seiji Yamazaki , Kensuke Makita , Yasuaki Kai , Satoko Sugawara , Takashi Seino
IPC分类号： C03C17/00 , C03C17/25 , C03C17/34 , C23C18/12 , C23C26/00 , B32B17/00
CPC分类号： C23C26/00 , C03C17/007 , C03C17/256 , C03C17/3411 , C03C17/3417 , C23C18/1216 , C23C18/1225 , C23C18/1254 , C03C2217/23 , C03C2217/45 , C03C2217/475 , C03C2217/478 , C03C2218/113 , Y10T428/252
摘要： The invention relates to a hydrophilic film formed on a substrate. This film has a hydrophilic outermost layer having a matrix phase containing titania and a disperse phase constituted of at least one compound of silica and alumina. The matrix phase may further contain an amorphous metal oxide. With this, the outermost layer becomes superior in abrasion resistance. The at least one compound of the disperse phase may be a non-spherical colloidal silica. With this, the outermost layer becomes substantially improved in scratch resistance. The outermost layer is formed on the substrate by a method including sequential steps of (a) providing a sol mixture including a first sol containing a precursor of the titania and a second sol containing the at least one compound; (b) coating the substrate with the sol mixture, thereby to form thereon a precursory film; and (c) baking the precursory film into the outermost layer.
摘要翻译：本发明涉及形成在基材上的亲水膜。该膜具有含有二氧化钛的基质相和由至少一种二氧化硅和氧化铝的化合物构成的分散相的亲水性最外层。基质相可以进一步含有无定形金属氧化物。由此，最外层的耐磨性变得优异。分散相的至少一种化合物可以是非球形胶体二氧化硅。由此，最外层的耐擦伤性显着提高。通过包括以下步骤的方法在基材上形成最外层：（a）提供包含含有二氧化钛前体的第一溶胶和含有至少一种化合物的第二溶胶的溶胶混合物; （b）用溶胶混合物涂覆基材，从而在其上形成前体膜; 和（c）将前体膜烘烤到最外层中。

2. 发明授权

US6045903A Hydrophilic article and method for producing same 失效
标题翻译：亲水制品及其制造方法
公开(公告)号：US6045903A
公开(公告)日：2000-04-04
申请号：US92857
申请日：1998-06-08
申请人： Takashi Seino , Yasuaki Kai , Satoko Sugawara
发明人： Takashi Seino , Yasuaki Kai , Satoko Sugawara
IPC分类号： C09D1/00 , C03C17/00 , C03C17/23 , C03C17/25 , C03C17/34 , C09D5/00 , B32B5/16 , B05D5/06
CPC分类号： C03C17/3417 , C03C17/007 , C03C17/25 , C03C2217/23 , C03C2217/45 , C03C2217/478 , C03C2218/113 , Y10T428/259
摘要： The invention relates to a hydrophilic article having (a) a substrate; and (b) a hydrophilic film formed on the substrate. This film has a hydrophilic outermost layer containing (1) a titania; (2) an amorphous oxide in an amount of from 5 to 25 wt % based on the total weight of the outermost layer; and (3) silica particles having a particle diameter of from 3 to 20 nm. A combination of the titania and the amorphous oxide constitutes the hydrophilic outermost layer's matrix phase (continuous phase), and the silica particles constitute the disperse phase distributed over the matrix phase. The hydrophilic outermost layer is superior in abrasion resistance and duration of hydrophilicity. The hydrophilic article is produced by a method including sequential steps of (a) providing a sol mixture comprising a first sol containing a precursor of the titania, a second sol containing a precursor of the amorphous oxide, and a silica colloidal solution containing the silica particles; (b) applying the sol mixture to the substrate, thereby to form thereon a precursory film; and (c) baking the precursory film into the outermost layer.
摘要翻译：本发明涉及一种具有（a）底物的亲水制品; 和（b）在基材上形成的亲水膜。该膜具有含有（1）二氧化钛的亲水性最外层; （2）基于最外层的总重量为5〜25重量％的无定形氧化物; 和（3）粒径为3〜20nm的二氧化硅粒子。二氧化钛和无定形氧化物的组合构成亲水性最外层的基质相（连续相），二氧化硅颗粒构成分散相分布在基体相上。亲水性最外层的耐磨性和亲水性的持久性优异。亲水制品通过以下步骤制备：（a）提供包含含有二氧化钛前体的第一溶胶的溶胶混合物，含有无定形氧化物前体的第二溶胶和含有二氧化硅颗粒的二氧化硅胶体溶液 ; （b）将溶胶混合物施加到基材上，由此在其上形成前体膜; 和（c）将前体膜烘烤到最外层中。

3. 发明授权

US6110269A Coating liquid for forming hydrophilic film and method for producing same 失效
标题翻译：用于形成亲水膜的涂布液及其制造方法
公开(公告)号：US6110269A
公开(公告)日：2000-08-29
申请号：US12728
申请日：1998-01-23
申请人： Satoko Sugawara , Toshikazu Nishide , Takashi Seino , Yasuaki Kai
发明人： Satoko Sugawara , Toshikazu Nishide , Takashi Seino , Yasuaki Kai
IPC分类号： C01G23/053 , C03C17/25 , C09D1/00 , B01J13/00 , C01B33/14 , C01G23/047 , C03G17/25
CPC分类号： C09D1/00 , B82Y30/00 , C01G23/053 , C03C17/256 , C01P2004/64 , C03C2217/212 , C03C2217/23 , C03C2217/71 , C03C2218/113
摘要： The invention relates to a coating liquid for forming a hydrophilic film. This coating liquid comprises a first sol which is a titania sol; and a second sol which is at least one of a silica sol and an alumina sol. This titania sol is prepared by a method comprising the sequential steps of (a) mixing a first solution containing a titanium alkoxide with a diol represented by at least one of the following general formulas (1) and (2), thereby to prepare a second solution containing a titanium complex formed by a reaction of the titanium alkoxide with the diol; and (b) hydrolyzing the titanium complex in the second solution, thereby to prepare the titania sol. The coating liquid is stable or sufficiently long in pot life, and the hydrophilic film has a long time duration in hydrophilicity and a superior abrasion resistance. ##STR1## wherein R.sub.1 is H or C.sub.p H.sub.2p+1 where p is from 1 to 5, R.sub.2 is C.sub.q H.sub.2q+1 where q is from 1 to 5, R.sub.3 is C.sub.r H.sub.2r where r is from 1 to 3, R.sub.4 is H or C.sub.x H.sub.2x+1 where x is from 1 to 5, and R.sub.5 is H or C.sub.y H.sub.2y+1 where y is from 1 to 5.
摘要翻译：本发明涉及一种用于形成亲水膜的涂布液。该涂布液包含作为二氧化钛溶胶的第一溶胶; 和二氧化硅溶胶和氧化铝溶胶中的至少一种的第二溶胶。该二氧化钛溶胶的制备方法包括以下顺序的步骤：（a）将含有钛醇盐的第一溶液与由以下通式（1）和（2）中的至少一个表示的二醇混合，从而制备第二种溶液，其含有通过钛醇盐与二醇的反应形成的钛络合物; 和（b）在第二溶液中水解钛络合物，从而制备二氧化钛溶胶。涂布液在适用期内稳定或足够长，并且亲水膜在亲水性和耐磨性方面具有长的持续时间。其中R1为H或CpH2p + 1，其中p为1至5，R2为CqH2q + 1，其中q为1至5，R3为CrH2r，其中r为1至3，R4为H或CxH2x + 1，其中x为 1〜5，R5为H或CyH2y + 1，其中y为1至5。

4. 发明申请

US20100210777A1 ALUMINA PARTICLE COMPOSITE, METHOD OF MANUFACTURING THE ALUMINA PARTICLE COMPOSITE, RESIN COMPOSITION AND METHOD OF MANUFACTURING THE RESIN COMPOSITION 审中-公开
标题翻译：氧化铝颗粒复合材料，制造氧化铝颗粒复合材料的方法，树脂组合物和制备树脂组合物的方法
公开(公告)号：US20100210777A1
公开(公告)日：2010-08-19
申请号：US12768378
申请日：2010-04-27
申请人： Takashi ODA , Yasuaki Kai , Tomohiro Itou , Takashi Seino , Hironobu Muramatsu
发明人： Takashi ODA , Yasuaki Kai , Tomohiro Itou , Takashi Seino , Hironobu Muramatsu
IPC分类号： C08K3/22
CPC分类号： C01F7/02 , B82Y30/00 , C01F7/021 , C01P2004/04 , C01P2004/10 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C01P2006/22 , C08K9/04 , C09C1/407
摘要： An alumina particle composite (1) includes an alumina particle (2) and an organic acid (3) chemically bonded to a surface of the alumina particle (2). Further, the alumina particle (2) has a short axis length of 1 to 10 nm, a long axis length of 20 to 400 nm, and an aspect ratio of 5 to 80, and is represented by Formula I, Al2O3.nH2O Formula I where n is 0 or more.
摘要翻译：氧化铝颗粒复合材料（1）包括氧化铝颗粒（2）和与氧化铝颗粒（2）的表面化学键合的有机酸（3）。此外，氧化铝颗粒（2）的短轴长度为1〜10nm，长轴长度为20〜400nm，纵横比为5〜80，由式I表示，Al 2 O 3·nH 2 O式I 其中n为0以上。

5. 发明申请

US20060058426A1 Alumina particle composite, method of manufacturing the alumina particle composite, resin composition and method of manufacturing the resin composition 审中-公开
标题翻译：氧化铝微粒复合体，氧化铝微粒复合体的制造方法，树脂组合物和树脂组合物的制造方法
公开(公告)号：US20060058426A1
公开(公告)日：2006-03-16
申请号：US11220402
申请日：2005-09-07
申请人： Takashi Oda , Yasuaki Kai , Tomohiro Itou , Takashi Seino , Hironobu Muramatsu
发明人： Takashi Oda , Yasuaki Kai , Tomohiro Itou , Takashi Seino , Hironobu Muramatsu
IPC分类号： C08K9/12 , C08K3/22
CPC分类号： C01F7/02 , B82Y30/00 , C01F7/021 , C01P2004/04 , C01P2004/10 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C01P2006/22 , C08K9/04 , C09C1/407
摘要： An alumina particle composite (1) includes an alumina particle (2) and an organic acid (3) chemically bonded to a surface of the alumina particle (2). Further, the alumina particle (2) has a short axis length of 1 to 10 nm, a long axis length of 20 to 400 nm, and an aspect ratio of 5 to 80, and is represented by Formula I, Al2O3.nH2O Formula I where n is 0 or more.
摘要翻译：氧化铝颗粒复合材料（1）包括氧化铝颗粒（2）和与氧化铝颗粒（2）的表面化学键合的有机酸（3）。此外，氧化铝颗粒（2）的短轴长度为1〜10nm，长轴长度为20〜400nm，纵横比为5〜80，由式

6. 发明授权

US06916545B2 Resin composition, thermoplastic resin laminate, and production methods thereof 失效
标题翻译：树脂组合物，热塑性树脂层合体及其制造方法
公开(公告)号：US06916545B2
公开(公告)日：2005-07-12
申请号：US10284178
申请日：2002-10-31
申请人： Shoichiro Yano , Takashi Sawaguchi , Masatoshi Chikazawa , Takashi Takei , Tomohiro Ito , Masao Nakajima , Takashi Seino , Yasuaki Kai , Shinkichi Torii , Kouichi Handa , Katsuhiko Suzuki , Kenji Uesugi
发明人： Shoichiro Yano , Takashi Sawaguchi , Masatoshi Chikazawa , Takashi Takei , Tomohiro Ito , Masao Nakajima , Takashi Seino , Yasuaki Kai , Shinkichi Torii , Kouichi Handa , Katsuhiko Suzuki , Kenji Uesugi
IPC分类号： B62D25/02 , B32B27/08 , B32B27/18 , B32B37/15 , B60J1/00 , B60J5/00 , B60K15/03 , B60R1/06 , B60R13/02 , B60R13/04 , B60R19/03 , B60S1/38 , B62D25/06 , B62D25/10 , B62D25/16 , B65D1/00 , C08K9/00 , C08L101/02 , C09D133/14 , C09J133/14
CPC分类号： B32B27/08 , B32B27/18 , B32B37/153 , B32B2605/08 , B60J5/00 , C09D133/14 , C09J133/14 , Y10T428/25 , Y10T428/28 , Y10T428/31681 , Y10T428/31909 , Y10T428/31931 , Y10T428/31938
摘要： A resin composition to be used as a material for a various part of an automotive vehicle. The resin composition comprises a copolymer (A) formed by copolymerization of a first unsaturated monomer (a) and a second mononer (b). The first unsaturated monomer has a functional group which is bondable by hydrogen bond to a hydroxyl group. The second monomer is copolymerizable with the first unsaturated monomer. A metal oxide (B) is dispersed in the copolymer and having hydroxyl groups and hydrophobic groups at surface of the metal oxide.
摘要翻译：用作机动车辆各部分的材料的树脂组合物。树脂组合物包含通过第一不饱和单体（a）和第二单体（b）的共聚形成的共聚物（A）。第一不饱和单体具有通过氢键与羟基键合的官能团。第二单体可与第一不饱和单体共聚。金属氧化物（B）分散在共聚物中，在金属氧化物的表面具有羟基和疏水基团。

7. 发明授权

US06903148B2 Resin composition and its production process and uses 失效
标题翻译：树脂成分及其生产工艺及用途
公开(公告)号：US06903148B2
公开(公告)日：2005-06-07
申请号：US10396476
申请日：2003-03-26
申请人： Katsuhiko Suzuki , Yasuaki Kai , Koichi Handa , Masao Nakajima , Takashi Seino , Shinkichi Torii , Tomohiro Ito , Kenji Uesugi , Masatoshi Chikazawa , Takashi Takei , Shoichiro Yano , Takashi Sawaguchi
发明人： Katsuhiko Suzuki , Yasuaki Kai , Koichi Handa , Masao Nakajima , Takashi Seino , Shinkichi Torii , Tomohiro Ito , Kenji Uesugi , Masatoshi Chikazawa , Takashi Takei , Shoichiro Yano , Takashi Sawaguchi
IPC分类号： B62D25/02 , B60J1/00 , B60K15/03 , B60R1/06 , B60R13/02 , B60R13/04 , B60R19/03 , B60S1/34 , B60S1/38 , B62D25/04 , B62D25/06 , B62D25/16 , C08K9/04 , C08K9/06 , C08L33/00 , C08L101/02 , F21S8/10 , F21V7/00 , F21V17/00 , C08K3/18
CPC分类号： C08K9/04
摘要： A resin composition of the present invention comprises a polymer having functional groups and a metal oxide surface modified to form functional groups at a surface of the metal oxide and dispersed uniformly in the polymer. The functional groups of the polymer and the functional groups of the metal oxide are ionically bondable to the metal oxide and the polymer, respectively, so that the polymer and the metal oxide are bonded by ionic bonds to each other.
摘要翻译：本发明的树脂组合物包含具有官能团的聚合物和金属氧化物表面改性以在金属氧化物的表面形成官能团并均匀分散在聚合物中。聚合物的官能团和金属氧化物的官能团分别与金属氧化物和聚合物离子键合，使得聚合物和金属氧化物通过离子键彼此键合。

8. 发明授权

US08722765B2 Alumina particle composite, method of manufacturing the alumina particle composite, resin composition and method of manufacturing the resin composition 失效
标题翻译：氧化铝微粒复合体，氧化铝微粒复合体的制造方法，树脂组合物和树脂组合物的制造方法
公开(公告)号：US08722765B2
公开(公告)日：2014-05-13
申请号：US13469302
申请日：2012-05-11
申请人： Takashi Oda , Yasuaki Kai , Tomohiro Ito , Takashi Seino , Hironobu Muramatsu
发明人： Takashi Oda , Yasuaki Kai , Tomohiro Ito , Takashi Seino , Hironobu Muramatsu
IPC分类号： C08K9/10 , C08K3/18 , C01F7/02
CPC分类号： C01F7/02 , B82Y30/00 , C01F7/021 , C01P2004/04 , C01P2004/10 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C01P2006/22 , C08K9/04 , C09C1/407
摘要： An alumina particle composite (1) includes an alumina particle (2) and an organic acid (3) chemically bonded to a surface of the alumina particle (2). Further, the alumina particle (2) has a short axis length of 1 to 10 nm, a long axis length of 20 to 400 nm, and an aspect ratio of 5 to 80, and is represented by Formula I, Al2O3·nH2O Formula I where n is 0 or more.
摘要翻译：氧化铝颗粒复合材料（1）包括氧化铝颗粒（2）和与氧化铝颗粒（2）的表面化学键合的有机酸（3）。此外，氧化铝颗粒（2）的短轴长度为1〜10nm，长轴长度为20〜400nm，纵横比为5〜80，由式I表示，Al 2 O 3·nH 2 O式I 其中n为0以上。

9. 发明申请

US20120289653A1 ALUMINA PARTICLE COMPOSITE, METHOD OF MANUFACTURING THE ALUMINA PARTICLE COMPOSITE, RESIN COMPOSITION AND METHOD OF MANUFACTURING THE RESIN COMPOSITION 失效
标题翻译：氧化铝颗粒复合材料，制造氧化铝颗粒复合材料的方法，树脂组合物和制备树脂组合物的方法
公开(公告)号：US20120289653A1
公开(公告)日：2012-11-15
申请号：US13469302
申请日：2012-05-11
申请人： Takashi Oda , Yasuaki Kai , Tomohiro Itou , Takashi Seino , Hironobu Muramatsu
发明人： Takashi Oda , Yasuaki Kai , Tomohiro Itou , Takashi Seino , Hironobu Muramatsu
IPC分类号： C08K3/22 , C08L33/12 , C08L69/00
CPC分类号： C01F7/02 , B82Y30/00 , C01F7/021 , C01P2004/04 , C01P2004/10 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C01P2006/22 , C08K9/04 , C09C1/407
摘要： An alumina particle composite (1) includes an alumina particle (2) and an organic acid (3) chemically bonded to a surface of the alumina particle (2). Further, the alumina particle (2) has a short axis length of 1 to 10 nm, a long axis length of 20 to 400 nm, and an aspect ratio of 5 to 80, and is represented by Formula I, Al2O3.nH2O Formula I where n is 0 or more.
摘要翻译：氧化铝颗粒复合材料（1）包括氧化铝颗粒（2）和与氧化铝颗粒（2）的表面化学键合的有机酸（3）。此外，氧化铝颗粒（2）的短轴长度为1〜10nm，长轴长度为20〜400nm，纵横比为5〜80，由式I表示，Al 2 O 3·nH 2 O式I 其中n为0以上。

10. 发明申请

US20080015329A1 Resin Composition, Method for Producing the Same, and Intermediate and Molded Article of the Same 审中-公开
标题翻译：树脂组合物，其制造方法及其中间和成型品
公开(公告)号：US20080015329A1
公开(公告)日：2008-01-17
申请号：US11631313
申请日：2005-06-28
申请人： Takashi Seino , Yasuaki Kai , Tomohiro Ito , Hironobu Muramatsu , Manabu Kawa , Minoru Soma
发明人： Takashi Seino , Yasuaki Kai , Tomohiro Ito , Hironobu Muramatsu , Manabu Kawa , Minoru Soma
IPC分类号： C08G64/08 , C08G64/18
CPC分类号： C08G64/08 , C08G64/42 , C08L101/10
摘要： A thermoplastic resin composition contains polycarbonate molecules to which inorganic oxide fine particles are bonded through connecting groups of an aliphatic ether type represented by a following general wherein M represents a tri- or tetravalent metal element capable of bonding to surfaces of the inorganic oxide fine particles; m is 0 or 1; n is an integer of 2 to 8 indicating the number of methylene groups in a chain; R1 represents an aliphatic group containing a straight chain formed by connecting 2 to 8 carbon atoms to each other, and both terminals of which are bonded to two oxygen atoms adjacent thereto; at least one of *1-, *2- and *3- is a bonding species capable of bonding to the surfaces of the inorganic oxide fine particles, and at least one of the *1-, *2- and *3- is bonded to the surfaces of the inorganic oxide fine particles; and *4- represents a bond with a polycarbonate molecule.
摘要翻译：热塑性树脂组合物包含聚碳酸酯分子，无机氧化物细颗粒通过由以下通式表示的脂族醚类的连接基团键合而成，其中M表示能与无机氧化物细颗粒的表面结合的三价或四价金属元素; m为0或1; n是2〜8的整数，表示链中的亚甲基数; R 1表示含有通过连接2〜8个碳原子而形成的直链的脂肪族基团，其两末端键合在与其相邻的两个氧原子上; * 1-，* 2-和* 3-中的至少一个是能够键合到无机氧化物细颗粒的表面的结合物质，并且* 1，* 2-和* 3-中的至少一个是粘合到无机氧化物细颗粒的表面上; 和* 4-代表与聚碳酸酯分子的键。

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