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1. 发明授权

US6071606A Hydrophilic film and method for forming same on substrate 失效
标题翻译：亲水膜及其在基材上的形成方法
公开(公告)号：US6071606A
公开(公告)日：2000-06-06
申请号：US917617
申请日：1997-08-26
申请人： Seiji Yamazaki , Kensuke Makita , Yasuaki Kai , Satoko Sugawara , Takashi Seino
发明人： Seiji Yamazaki , Kensuke Makita , Yasuaki Kai , Satoko Sugawara , Takashi Seino
IPC分类号： C03C17/00 , C03C17/25 , C03C17/34 , C23C18/12 , C23C26/00 , B32B17/00
CPC分类号： C23C26/00 , C03C17/007 , C03C17/256 , C03C17/3411 , C03C17/3417 , C23C18/1216 , C23C18/1225 , C23C18/1254 , C03C2217/23 , C03C2217/45 , C03C2217/475 , C03C2217/478 , C03C2218/113 , Y10T428/252
摘要： The invention relates to a hydrophilic film formed on a substrate. This film has a hydrophilic outermost layer having a matrix phase containing titania and a disperse phase constituted of at least one compound of silica and alumina. The matrix phase may further contain an amorphous metal oxide. With this, the outermost layer becomes superior in abrasion resistance. The at least one compound of the disperse phase may be a non-spherical colloidal silica. With this, the outermost layer becomes substantially improved in scratch resistance. The outermost layer is formed on the substrate by a method including sequential steps of (a) providing a sol mixture including a first sol containing a precursor of the titania and a second sol containing the at least one compound; (b) coating the substrate with the sol mixture, thereby to form thereon a precursory film; and (c) baking the precursory film into the outermost layer.
摘要翻译：本发明涉及形成在基材上的亲水膜。该膜具有含有二氧化钛的基质相和由至少一种二氧化硅和氧化铝的化合物构成的分散相的亲水性最外层。基质相可以进一步含有无定形金属氧化物。由此，最外层的耐磨性变得优异。分散相的至少一种化合物可以是非球形胶体二氧化硅。由此，最外层的耐擦伤性显着提高。通过包括以下步骤的方法在基材上形成最外层：（a）提供包含含有二氧化钛前体的第一溶胶和含有至少一种化合物的第二溶胶的溶胶混合物; （b）用溶胶混合物涂覆基材，从而在其上形成前体膜; 和（c）将前体膜烘烤到最外层中。

2. 发明授权

US5510141A Coating composition and method for forming thin film on substrate using same 失效
标题翻译：涂料组合物和使用其在基材上形成薄膜的方法
公开(公告)号：US5510141A
公开(公告)日：1996-04-23
申请号：US378729
申请日：1995-01-26
申请人： Kensuke Makita , Yasuo Moriguchi , Junichi Okuda
发明人： Kensuke Makita , Yasuo Moriguchi , Junichi Okuda
IPC分类号： B05D1/28 , C03C17/25 , B05D5/06
CPC分类号： B05D1/28 , C03C17/25 , C03C2218/113 , C03C2218/118 , C03C2218/322
摘要： The invention relates to a method for applying a coating composition to a substrate with a reverse roller coater so as to form a thin film on the substrate and then for baking the thin film so as to transform the thin film into a metal oxide film. The coating composition comprises: 0.1-10 wt % of at least one organic metal compound on a metal oxide basis; and at least one organic solvent. The at least one organic metal compound is selected from the group consisting of metal alkoxides, metal acetyl-acetonates and metallic soaps. The coating composition is adjusted to have a viscosity within a range from 0.1 to 100 centipoises. In this method, a reverse roller of the coater is rotated at a rotation speed within a range from 2 to 55 m/min. and the substrate is moved at a moving speed within a range from 1 to 30 m/min. while the coating composition is applied to the substrate. Furthermore, the rotation speed of the reverse roller is adjusted to be higher than the moving speed of the substrate. According to the invention, it is possible to form an optical metal oxide film which has a uniform thickness of up to about 10 .mu.m (more particularly up to about 1 .mu.m).
摘要翻译：本发明涉及一种用反辊涂布机将涂料组合物涂布在基材上的方法，以便在基材上形成薄膜，然后烘烤该薄膜，以将该薄膜转变成金属氧化物膜。所述涂料组合物包含：0.1-10重量％的至少一种金属氧化物上的有机金属化合物; 和至少一种有机溶剂。所述至少一种有机金属化合物选自金属醇盐，金属乙酰丙酮酸盐和金属皂。将涂料组合物调节至粘度在0.1至100厘泊的范围内。在该方法中，涂布机的反转辊以2〜55m /分钟的范围内的转速旋转。并且以1〜30m / min的范围内的移动速度移动基板。同时将涂料组合物施加到基材上。此外，将反转辊的旋转速度调整为高于基板的移动速度。根据本发明，可以形成具有高达约10μm的均匀厚度（更特别地至多约1μm）的光学金属氧化物膜。

3. 发明授权

US5496621A Glass pane with reflectance reducing coating and combiner of head-up display system 失效
标题翻译：具有反射率降低涂层的玻璃板和平视显示系统的组合器
公开(公告)号：US5496621A
公开(公告)日：1996-03-05
申请号：US228522
申请日：1994-04-15
申请人： Kensuke Makita , Atsushi Takamatsu , Katsuto Tanaka
发明人： Kensuke Makita , Atsushi Takamatsu , Katsuto Tanaka
IPC分类号： G02B5/28 , G02B27/00 , G02B27/01 , G02B1/10
CPC分类号： G02B5/286 , B32B17/10036 , B32B17/10174 , B32B17/10761 , G02B27/0101 , G02B2027/0118 , G02B2027/012 , G02B2027/0194 , Y10S428/913 , Y10T428/24942 , Y10T428/24975 , Y10T428/265 , Y10T428/3163
摘要： The invention relates to a transparent coating on a transparent glass pane which may be a laminated glass pane such as an automobile windshield. The present invention provides a two-layer coating including a first layer which is a transparent oxide film in direct contact with the major surface of the glass substrate and a second layer which is a transparent oxide film. The first layer has a thickness of 70-230 nm and a refractive index of 1.80-2.10 and includes a major portion and a minor portion which is exposed and adapted to be used as a combiner of a head-up display system. The second layer is formed on the major portion of the first layer so as to expose the minor portion of the first layer. The second layer has a thickness of 110-130 nm and a refractive index of 1.40-1.50. An additional film is optionally formed on the minor portion of the first layer so as to fully or partly cover the minor portion. The additional layer is adapted to be used as a wavelength-selective combiner of the head-up display system. The two-layer coating except the minor portion is adapted to be used as a reflectance reducing coating. To reduce the reflectance of perpendicularly incident light the two-layer coating can be modified into a three-layer coating by interposing another oxide film.
摘要翻译：本发明涉及透明玻璃板上的透明涂层，其可以是诸如汽车挡风玻璃的层压玻璃板。本发明提供一种双层涂层，其包括与玻璃基板的主表面直接接触的透明氧化膜的第一层和作为透明氧化膜的第二层。第一层具有70-230nm的厚度和1.80-2.10的折射率，并且包括暴露并适于用作平视显示系统的组合器的主要部分和次要部分。第二层形成在第一层的主要部分上，以露出第一层的次要部分。第二层的厚度为110-130nm，折射率为1.40-1.50。可选地，在第一层的次要部分上形成附加的膜，以便完全或部分地覆盖次要部分。附加层适于用作平视显示系统的波长选择组合器。除了次要部分之外的两层涂层适合用作反射率降低涂层。为了降低垂直入射光的反射率，可以通过插入另一氧化膜将双层涂层改性成三层涂层。

4. 发明授权

US5338350A Ink composition for forming thin film 失效
标题翻译：用于形成薄膜的油墨组合物
公开(公告)号：US5338350A
公开(公告)日：1994-08-16
申请号：US85786
申请日：1993-07-06
申请人： Katsuto Tanaka , Kensuke Makita , Yasuo Moriguchi
发明人： Katsuto Tanaka , Kensuke Makita , Yasuo Moriguchi
IPC分类号： B60J1/00 , C03C17/02 , C03C17/25 , C04B41/82 , C09D11/00 , C09D101/18 , G02B27/02
CPC分类号： C03C17/25 , C03C2217/23 , C03C2218/113
摘要： An ink composition for forming a thin metal oxide film contains a glass component, a viscosity-increasing agent and a solvent. The glass component is one of a halogen-containing metal alkoxide, a mixture of the halogen-containing metal alkoxide and another metal alkoxide, and a mixture of the halogen-containing metal alkoxide and a metal oxide sol. The viscosity-increasing agent is nitrocellulose H60 according to Japanese Industrial Standard K6703. The solvent is at least one of ethylcarbitol and butylcarbitol. The formed thin metal oxide film is superior in transparency, abrasion resistance and scratch resistance.
摘要翻译：用于形成薄金属氧化物膜的油墨组合物含有玻璃成分，增粘剂和溶剂。玻璃成分是含卤素的金属醇盐，含卤素金属醇盐和另一种金属醇盐的混合物，含卤素金属醇盐和金属氧化物溶胶的混合物之一。粘度增加剂是日本工业标准K6703的硝基纤维素H60。溶剂是乙基卡必醇和丁基卡必醇中的至少一种。所形成的薄金属氧化物膜的透明性，耐磨性和耐刮擦性优异。

5. 发明授权

US5318830A Glass pane with reflectance reducing coating 失效
标题翻译：具有反射率降低涂层的玻璃板
公开(公告)号：US5318830A
公开(公告)日：1994-06-07
申请号：US872033
申请日：1992-04-23
申请人： Atsushi Takamatsu , Kensuke Makita
发明人： Atsushi Takamatsu , Kensuke Makita
IPC分类号： B32B17/10 , G02B1/11 , G02B1/100
CPC分类号： C03C17/3417 , B32B17/10036 , B32B17/10174 , B32B17/10761 , G02B1/115 , C03C2217/212 , C03C2217/213 , C03C2217/22 , C03C2217/23 , C03C2217/734 , C03C2218/355 , Y10S428/913 , Y10T428/24942 , Y10T428/24975 , Y10T428/265 , Y10T428/3163
摘要： The invention relates to a transparent coating on a transparent glass pane which may be a laminated glass pane such as an automobile windshield. The invention provides a two-layer coating made up of a first oxide film, e.g. a TiO.sub.2 -SiO.sub.2 mixed oxide film, which is in contact with the glass pane and has a thickness of 70-100 nm and a refractive index of 1.80-1.90 and an outer second oxide film, e.g. a SiO.sub.2 film, which has a thickness of 110-130 nm and a refractive index of 1.40-1.50. With respect to visible light obliquely incident on the coating side of the glass pane at an angle of 50-70 degrees with the normal, the reflectance of the coated glass pane becomes lower than that of the glass pane without coating by 4.5-6.5%. To reduce the reflectance of perpendicularly incident light the two-layer coating can be modified into a three-layer coating by interposing another oxide film, e.g. a TiO.sub.2 film, having a thickness of 130-160 nm and a refractive index of 2.05-2.30 between the above described first and second oxide films. The three-layer coating is nearly equivalent to the two-layer coating in the ability to reduce the reflectance of obliquely incident light.
摘要翻译：本发明涉及透明玻璃板上的透明涂层，其可以是诸如汽车挡风玻璃的层压玻璃板。本发明提供了由第一氧化膜，例如，与玻璃板接触并且具有70-100nm的厚度和1.80-1.90的折射率和外部的第二氧化物膜的TiO 2 -SiO 2混合氧化物膜。 SiO 2膜，其厚度为110-130nm，折射率为1.40-1.50。对于以正常方式倾斜入射到玻璃板的涂层侧的可见光，与玻璃板的反射率相比，涂层的玻璃板的反射率低于4.5-6.5％。为了降低垂直入射光的反射率，可以通过插入另一氧化膜，例如，将两层涂层改性成三层涂层。在上述第一和第二氧化物膜之间具有130-160nm的厚度和2.05-2.30的折射率的TiO 2膜。三层涂层几乎等同于双层涂层，以降低倾斜入射光的反射率。

6. 发明授权

US5289315A Head-up display system including a uniformly reflecting layer and a selectively reflecting layer 失效
标题翻译：平视显示系统，包括均匀反射层和选择性反射层
公开(公告)号：US5289315A
公开(公告)日：1994-02-22
申请号：US872027
申请日：1992-04-23
申请人： Kensuke Makita , Katsuto Tanaka , Atsushi Takamatsu
发明人： Kensuke Makita , Katsuto Tanaka , Atsushi Takamatsu
IPC分类号： B60J1/02 , B60K35/00 , C03C17/34 , G02B1/10 , G02B5/28 , G02B27/00 , G02B27/01 , G02B27/14
CPC分类号： G02B5/0833 , C03C17/3417 , G02B27/0101 , G02B2027/0194 , G02B5/28
摘要： The present invention relates to a head-up display system which includes an element thereof. The element is attached to, for example, an automobile windshield so as to project light rays carrying images of display information onto the element from a luminous source in a car. The element includes first and second reflection layers. The first layer is directly attached to the windshield and has a relatively uniform reflectance throughout visible light spectrum. The second layer is directly formed on the first layer and has a selective reflection against incident visible light of wavelengths in the range from about 500 nm to about 600 nm. Thus, the light rays from the luminous source are displayed on the first and second layers in different colors.
摘要翻译：本发明涉及一种包括其元件的平视显示系统。该元件例如附接到汽车挡风玻璃上，以便将来自汽车的光源的显示信息的图像的光线投射到元件上。元件包括第一和第二反射层。第一层直接连接到挡风玻璃上，并且在可见光光谱范围内具有相对均匀的反射率。第二层直接形成在第一层上，并且对波长在约500nm至约600nm范围内的入射可见光具有选择性反射。因此，来自光源的光线以不同的颜色显示在第一和第二层上。

7. 发明授权

US5268198A Water-repellent metal oxide film coated on glass substrate and method of forming same 失效
标题翻译：涂覆在玻璃基板上的防水金属氧化物膜及其形成方法
公开(公告)号：US5268198A
公开(公告)日：1993-12-07
申请号：US865449
申请日：1992-04-09
申请人： Seiji Yamasaki , Kensuke Makita , Hiroshi Inaba
发明人： Seiji Yamasaki , Kensuke Makita , Hiroshi Inaba
IPC分类号： C03C17/42 , C03C17/00 , C03C17/25 , B05D3/02
CPC分类号： C03C17/25 , C03C17/009 , C03C2217/29 , C03C2218/113
摘要： The disclosure relates to a metal oxide film formed on a glass substrate by the sol-gel process using an alcohol solution of at least one metal alkoxide or acetylacetonato. To afford water repellency to the oxide film, carbon fluoride is dispersed in the metal oxide matrix by thermal decomposition of a fluoroalkylsilane compound, e.g. CF.sub.3 (CF.sub.2).sub.3 CH.sub.2 CH.sub.2 Si(OCH.sub.3).sub.3. An organic polymer, e.g. polyethylene glycol, is dissolved in the metal alkoxide or acetylacetonato solution, and the solution is applied to the glass substrate to form a sol film. By heating at a temperature not higher than 200.degree. C. the sol film turns into a porous gel film. Next, the porous gel film is impregnated with an alcohol solution of the fluoroalkylsilane compound and then heated at a temperature not lower than 500.degree. C. The obtained oxide film is good in durability and abrasion resistance, and on this film the contact angle of water drop becomes greater than 90 degrees.
摘要翻译：本发明涉及通过使用至少一种金属醇盐或乙酰丙酮的醇溶液的溶胶 - 凝胶法在玻璃基板上形成的金属氧化物膜。为了提供对氧化膜的拒水性，碳氟化物通过氟烷基硅烷化合物的热分解分散在金属氧化物基质中。 CF 3（CF 2）3 CH 2 CH 2 Si（OCH 3）3。有机聚合物，例如聚乙二醇溶解在金属醇盐或乙酰丙酮溶液中，并将溶液施加到玻璃基板上以形成溶胶膜。通过在不高于200℃的温度下加热，溶胶膜变成多孔凝胶膜。接着，用氟烷基硅烷化合物的醇溶液浸渍多孔凝胶膜，然后在不低于500℃的温度下加热。所得到的氧化膜具有良好的耐久性和耐磨性，在该膜上，水的接触角下降变得大于90度。

8. 发明授权

US5009933A Method and apparatus for coating thin liquid film on plate surface 失效
标题翻译：在薄板表面涂覆薄膜的方法和装置
公开(公告)号：US5009933A
公开(公告)日：1991-04-23
申请号：US397672
申请日：1989-08-23
申请人： Naohiko Matsuda , Kensuke Makita
发明人： Naohiko Matsuda , Kensuke Makita
IPC分类号： B05C3/18
CPC分类号： B05C3/18
摘要： A method and apparatus for coating a plate with a thin liquid film. In the method, a thin liquid film is coated on a surface of a substrate such as a glass plate by using an incomplete liquid tank having an opening of a shape similar to the shape of the substrate surface on one side thereof. The tank communicates with a flow streamlining channel by an aperture in a lower section of the tank. First the substrate and the incomplete tank are brought into tight contact with each other such that the side opening of the tank is closed by the substrate, whereby the tank is completed. Next, a coating liquid such as a metal alkoxide solution is fed into the tank to thereby wet the substrate surface. Preferably the coating liquid is allowed to overflow the tank to remove a surface layer of the liquid. Then the liquid is extracted from the tank through the streamlining channel so as to lower the liquid level in the tank at a predetermined rate while keeping both the tank and the substrate stationary. By this method a submicron coating film of uniform thickness can easily be formed even on a large-sized substrate, and it is easy to form a coating film on only a selected area of the substrate surface without using any masking.
摘要翻译：一种涂有薄液膜的板的方法和装置。在该方法中，通过使用具有与其一面上的基板表面的形状类似的开口的不完全液体罐将薄液膜涂布在诸如玻璃板的基板的表面上。储罐通过槽的下部的孔与流动流线通道连通。首先，使基板和不完全的槽彼此紧密接触，使得罐的侧开口被基板封闭，从而完成储罐。接下来，将诸如金属醇盐溶液的涂布液供给到罐中，从而使基板表面湿润。优选地，允许涂覆液体溢出罐以除去液体的表面层。然后通过流线通道将液体从罐中提取出来，以便以同时保持罐和基板两者均匀的方式以预定的速率降低罐中的液面。通过这种方法，即使在大尺寸基板上也能够容易地形成均匀厚度的亚微米涂膜，并且容易仅在基板表面的选定区域形成涂膜，而不使用任何掩模。

9. 发明授权

US4397666A Method of producing glass from metal alkoxide solution 失效
标题翻译：从金属醇盐溶液中生产玻璃的方法
公开(公告)号：US4397666A
公开(公告)日：1983-08-09
申请号：US315494
申请日：1981-10-27
申请人： Michiharu Mishima , Yuji Yamamoto , Kensuke Makita , Sumio Sakka , Kanichi Kamiya
发明人： Michiharu Mishima , Yuji Yamamoto , Kensuke Makita , Sumio Sakka , Kanichi Kamiya
IPC分类号： C01B33/152 , B05D7/00 , B32B17/00 , C03B8/02 , C03B19/12 , C03B37/01 , C03C1/00 , C03C3/04 , C03C3/06 , C03C17/02 , C04B41/50 , C04B41/86 , C03B19/06 , C03B20/00
CPC分类号： C04B41/009 , C03B19/12 , C03B37/011 , C03C1/008 , C03C3/04 , C03C3/06 , C04B41/5022 , C04B41/86 , C03C2201/02 , C03C2201/40 , C03C2201/42 , C03C2203/26 , C03C2203/30 , Y02P40/57 , Y10S65/901
摘要： In producing silica glass, which may contain additional metal(s) such as Ti or Zr, from a solution of a silicon alkoxide, mixed with alkoxide(s) of the additional metal(s) where necessary, in water and a hydrophilic organic solvent by shaping the solution into a desired form such as a coating film on a substrate, self-supporting film, fiber or lump when the solution exhibits a suitably high viscosity and sufficiently heating the shaped solution, a water-soluble organic polymeric substance is added to the solution as a viscosity adjusting agent to soon increase the viscosity of the solution to the desirable level. Therefore, shaping of the solution can be performed without awaiting the progress of hydrolysis of the alkoxide in the solution, and the glass can be obtained with improved uniformity of its properties. A cellulose ether is preferred as the viscosity adjusting agent, and hydroxypropyl cellulose is particularly preferable.
摘要翻译：在可能含有另外的金属如Ti或Zr的二氧化硅玻璃中，从需要的金属醇盐与硅烷醇盐的溶液在水和亲水性有机溶剂中混合通过将溶液成型为所需形状，例如基材上的涂膜，自支撑膜，纤维或块状物，当溶液表现出适当高的粘度并充分加热成型溶液时，将水溶性有机聚合物质加入该溶液作为粘度调节剂，将溶液粘度迅速提高至理想水平。因此，可以在不等待溶液中的醇盐的水解进行的情况下进行溶液的成形，并且可以获得具有改善的性能均匀性的玻璃。优选纤维素醚作为粘度调节剂，特别优选羟丙基纤维素。

10. 发明授权

US07802450B2 Organic-inorganic hybrid glassy materials and their production processes 有权
标题翻译：有机 - 无机混合玻璃材料及其生产工艺
公开(公告)号：US07802450B2
公开(公告)日：2010-09-28
申请号：US10800010
申请日：2004-03-15
申请人： Minoru Kuniyoshi , Naoya Hayakawa , Kensuke Makita , Toshinobu Yoko , Masahide Takahashi
发明人： Minoru Kuniyoshi , Naoya Hayakawa , Kensuke Makita , Toshinobu Yoko , Masahide Takahashi
IPC分类号： C03B8/00
CPC分类号： C03C3/06 , C08G79/00
摘要： In a production process of an organic-inorganic hybrid glassy material, the invention relates to a process for producing an organic-inorganic hybrid glassy material, characterized in that the process comprises at least the three steps of producing a gel body by a sol-gel method; melting by heating; and aging, and it relates to an organic-inorganic hybrid glassy material produced by this process.
摘要翻译：在有机 - 无机混合玻璃材料的制造方法中，本发明涉及一种有机 - 无机混合玻璃材料的制造方法，其特征在于，该方法至少包括通过溶胶 - 凝胶制备凝胶体的三个步骤方法; 通过加热熔化; 和老化，并且涉及通过该方法生产的有机 - 无机混合玻璃状材料。

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