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1. 发明授权

US06265337B1 High strength sintered body 有权
标题翻译：高强度烧结体
公开(公告)号：US06265337B1
公开(公告)日：2001-07-24
申请号：US09453391
申请日：1999-12-03
申请人： Satoru Kukino , Tomohiro Fukaya , Junichi Shiraishi , Tetsuo Nakai
发明人： Satoru Kukino , Tomohiro Fukaya , Junichi Shiraishi , Tetsuo Nakai
IPC分类号： C04B355831
CPC分类号： C04B35/62836 , C04B35/5831 , C04B35/62813 , C04B35/62828 , C04B35/62831 , C04B35/62897 , C04B35/6303 , C04B35/645 , C04B2235/3217 , C04B2235/3804 , C04B2235/3813 , C04B2235/3843 , C04B2235/386 , C04B2235/3865 , C04B2235/3886 , C04B2235/402 , C04B2235/404 , C04B2235/5436 , C04B2235/656 , C04B2235/762 , C04B2235/80 , C04B2235/96 , C22C26/00
摘要： A sintered body contains a high pressure form boron nitride in the range of 20 to 70% by volume, a first binding material surrounding the high pressure form boron nitride with a thickness in the range of 5 nm to 300 nm and a second binding material of the balance. The first binding material is composed of at least one of nitride and boride of Ti and Al. The second binding material is composed of at least one selected from the group consisting of nitride, carbide, carbonitride, boride and oxide of Al and transition metals belonging to the group 4a, 5a and 6a in the periodic table and mutual solid solution thereof. Supposing that X is the amount of Al contained per unit volume in the first binding material and Y is the amount of Al contained per unit volume in the second binding material, the ratio X/Y is not less than 1.
摘要翻译：烧结体包含20至70体积％范围内的高压形式氮化硼，围绕厚度在5nm至300nm范围内的高压形式氮化硼的第一结合材料和第二粘合材料余额。第一结合材料由Ti和Al的氮化物和硼化物中的至少一种组成。第二结合材料由选自氮化物，碳化物，碳氮化物，硼化物和Al的氧化物中的至少一种和属于元素周期表中第4a，5a和6a族的过渡金属及其相互固溶体组成。假设X是第一粘合材料中每单位体积含有的Al的量，Y是第二粘合材料中每单位体积含有的Al的量，X / Y的比率不小于1。

2. 发明授权

US6008153A High-pressure phase boron nitride base sinter 失效
标题翻译：高压相氮化硼基烧结矿
公开(公告)号：US6008153A
公开(公告)日：1999-12-28
申请号：US101742
申请日：1998-07-16
申请人： Satoru Kukino , Tetsuo Nakai , Junichi Shiraishi , Tomohiro Fukaya , Shinya Uesaka
发明人： Satoru Kukino , Tetsuo Nakai , Junichi Shiraishi , Tomohiro Fukaya , Shinya Uesaka
IPC分类号： C04B35/5831 , C04B35/5835
CPC分类号： C04B35/5831
摘要： A high-pressure phase boron nitride-based high-hardness high-strength sintered body for cutting tools represented by a milling tool and an end mill etc., which is improved in wear resistance and chipping resistance, is obtained. The high-pressure phase boron nitride-based sintered body according to the present invention comprises a plurality of grains (1) of high-pressure phase boron nitride and a binder phase (2, 3), and the content of the aforementioned grains (1) is at least 20.0 volume % and not more than 99.7 volume %. The aforementioned binder phase (2, 3) includes a first binder phase (2) enclosing the aforementioned grains (1) and a second binder phase (3) other than that. The first binder phase (2) consists of the form of at least either a nitride of at least one of Ti, TiAl, Zr and Hf or a solid solution thereof. The aforementioned second binder phase (3) includes a grain growth suppressive binder phase (4) between a plurality of the aforementioned grains (1) enclosed with the aforementioned first binder phase (2).
摘要翻译： PCT No.PCT / JP97 / 04410 Sec。 371日期：1998年7月16日 102（e）日期1998年7月16日PCT 1997年12月3日PCT PCT。出版物WO98 / 24736 日期1998年6月11日获得了耐磨性和耐崩裂性提高的用于切削工具的高压相氮化硼系高硬度高强度烧结体。根据本发明的高压相氮化硼基烧结体包括多个高压相氮化硼颗粒（1）和粘结相（2,3），并且上述颗粒（1）的含量）为20.0体积％以上且99.7体积％以下。上述粘合剂相（2,3）包括包围上述颗粒（1）的第一粘结相（2）和除此之外的第二粘结相（3）。第一粘合剂相（2）由至少一种Ti，TiAl，Zr和Hf的氮化物或其固溶体的形式组成。上述第二粘结相（3）包括在由上述第一粘结相（2）包围的多个上述颗粒（1）之间的晶粒生长抑制粘合剂相（4）。

3. 发明授权

US6001758A Hard and tough sintered body 失效
标题翻译：坚硬坚韧的烧结体
公开(公告)号：US6001758A
公开(公告)日：1999-12-14
申请号：US960773
申请日：1997-10-30
申请人： Tomohiro Fukaya , Tetsuo Nakai , Junichi Shiraishi , Satoru Kukino , Shinya Uesaka
发明人： Tomohiro Fukaya , Tetsuo Nakai , Junichi Shiraishi , Satoru Kukino , Shinya Uesaka
IPC分类号： C04B35/5831 , C04B35/5835
CPC分类号： C04B35/5831
摘要： A sintered body consists of high-pressure phase boron nitride, a residual binder phase and an unavoidable impurity, and contains high-pressure phase boron nitride powder which is previously coated with a binder before sintering. The coating binder consists of an element belonging to the group 4a, 5a or 6a of the periodic table or the like, and has an average thickness of 5 to 300 nm. Binder powder other than the coating binder consists of an element belonging to the group 4a, 5a or 6a of the periodic table or the like, and a contact ratio of high-pressure phase boron nitride particles in surface-to-surface contact with each other is at least 20% and less than 50%. The resulting high-pressure phase boron nitride-based hard and tough sintered body for a cutting tool is improved in wear resistance and chipping resistance.
摘要翻译：烧结体由高压相氮化硼，残余粘结相和不可避免的杂质组成，并且包含预先在烧结之前用粘合剂涂覆的高压相氮化硼粉末。涂层粘合剂由属于周期表等的4a，5a或6a族元素组成，平均厚度为5〜300nm。涂层粘合剂以外的粘合剂粉末由属于周期表等的4a，5a或6a族的元素组成，高压相氮化硼颗粒在表面与表面之间接触的接触比至少为20％且小于50％。所得到的用于切削工具的高压相氮化硼基硬坚韧烧结体的耐磨性和耐崩裂性提高。

4. 发明授权

US06635593B1 High strength sintered impact having excellent resistance to cratering 有权
标题翻译：高强度烧结冲击具有优异的耐火蚀性
公开(公告)号：US06635593B1
公开(公告)日：2003-10-21
申请号：US09913265
申请日：2001-08-10
申请人： Satoru Kukino , Tomohiro Fukaya , Junichi Shiraishi , Tetsuo Nakai
发明人： Satoru Kukino , Tomohiro Fukaya , Junichi Shiraishi , Tetsuo Nakai
IPC分类号： C04B355831
CPC分类号： C04B35/5831 , Y10T407/27
摘要： A sintered material containing high-pressure phase-type boron nitride and a binder is provided. The high-pressure phase-type boron nitride is contained in an amount of from 50% to 78% by volume, and the balance is a binder phase. The binder phase comprises at least one selected from the group consisting of nitride, carbide, carbonitride, and boride of Ti, nitride, boride and oxide of Al, carbide and boride of W, nitride, carbide, carbonitride and boride of Co, and carbide and boride of Ni, or a mutual solid solution thereof. The binder phase forms a binder phase which is continuous in a sintered material texture. The weight of metal components Al, W, Co and Ni which are present as compounds in the sintered material is from 3% to 20% based on the sintered material. The sintered material is excellent in crater resistance and capable of realizing a long tool life, even under the condition that the temperature of the cutting edge becomes high and the impact is large, as in high-speed interrupted cutting of hardened steel where the cutting speed V becomes at least 150 m/min.
摘要翻译：提供含有高压相型氮化硼和粘合剂的烧结材料。高压相型氮化硼的含量为50〜78体积％，余量为粘结相。粘结相包括选自Ti，氮化物，硼化物和Al的氧化物的氮化物，碳化物，碳氮化物和硼化物中的至少一种，W，氮化物，碳化物，碳氮化物和Co的硼化物的碳化物和硼化物，以及碳化物和Ni的硼化物或其相互固溶体。粘结相形成在烧结材料结构中连续的粘结相。烧结材料中作为化合物存在的金属成分Al，W，Co，Ni的重量相对于烧结体为3〜20％。该烧结材料即使在切削刃的温度高，冲击大的条件下也能够实现长的刀具寿命，因为在切削速度高的淬火钢的高速切断切削中 V变为至少150m / min。

5. 发明授权

US06316094B1 Cubic boron nitride sintered body 有权
标题翻译：立方氮化硼烧结体
公开(公告)号：US06316094B1
公开(公告)日：2001-11-13
申请号：US09357970
申请日：1999-07-21
申请人： Tomohiro Fukaya , Satoru Kukino , Junichi Shiraishi
发明人： Tomohiro Fukaya , Satoru Kukino , Junichi Shiraishi
IPC分类号： B24D300
CPC分类号： C04B35/5831 , C22C26/00 , C22C2026/005 , Y10T428/25 , Y10T428/26 , Y10T428/2991 , Y10T428/2993
摘要： A cBN sintered body superior in chipping resistance. The cBN sintered body is a sintered body in which cBN particles are bonded through a bonding phase. The bonding phase has a two-dimensionally continuous structure. The bonding phase comprises at least one kind selected from the group consisting of (a) carbide, nitride, carbonitride, or boride of a 4a-, 5a-, or 6a-group transition metal in the periodic table; (b) nitride, boride, or oxide of Al; (c) at least one kind of carbide, nitride, carbonitride, and boride of Fe, Co, or Ni; and (d) a mutual solid solution of those. The percentage of cBN content is 45 to 70% in volume. The bonding phase has the thickness of which the average value is 1.5 &mgr;m or less and the standard deviation is 0.9 &mgr;m or less with the cBN particles having an average particle size of 2 to 6 &mgr;m inclusive. The bonding phase has the thickness of which the average value is 1.0 &mgr;m or less and the standard deviation is 0.7 &mgr;m or less with the cBN particles having an average particle size of not less than 0.01 &mgr;m and less than 2.0 &mgr;m.
摘要翻译：耐破碎性优异的cBN烧结体。 cBN烧结体是通过结合相结合cBN粒子的烧结体。结合相具有二维连续结构。键合相包含选自元素周期表中的（a）碳化物，氮化物，碳氮化物或硼化物中的至少一种，其中该元素是4a-，5a-或6a-基过渡金属; （b）Al的氮化物，硼化物或氧化物; （c）Fe，Co或Ni中的至少一种碳化物，氮化物，碳氮化物和硼化物; 和（d）这些的相互坚实的解决方案。 cBN含量的百分比为45〜70％。结合相的平均值为1.5μm以下，标准偏差为0.9μm以下，cBN粒子的平均粒径为2〜6μm。结合相的平均值为1.0μm以下，标准偏差为0.7μm以下，cBN粒子的平均粒径为0.01μm以上且小于2.0μm。

6. 发明授权

US06337152B1 Cutting tool made of A12O3-coated cBN-based sintered material 有权
标题翻译：由A12O3涂层的cBN型烧结材料制成的切削刀具
公开(公告)号：US06337152B1
公开(公告)日：2002-01-08
申请号：US09492128
申请日：2000-01-27
申请人： Satoru Kukino , Junichi Shiraishi , Tetsuo Nakai
发明人： Satoru Kukino , Junichi Shiraishi , Tetsuo Nakai
IPC分类号： B32B3300
CPC分类号： C04B41/009 , C04B41/5031 , C04B41/52 , Y10T428/24975 , Y10T428/265 , C04B35/5831
摘要： A cutting tool according to the present invention is coated with one or more Al2O3 layers on at least a part of the surface of a cBN-based sintered material substrate taking part in cutting. The sintered material substrate is made of cBN in an amount of from 20% to 99% by volume and Al2O3 having an average crystalline particle diameter of not more than 1 &mgr;m in an amount of from not less than 1.0% to less than 10% by volume. The Al2O3 layer has a thickness (d) of from 0.5 &mgr;m to 50 &mgr;m. The average crystalline particle diameter (s) of Al2O3 is from 0.01 &mgr;m to 4 &mgr;m if the thickness (d) of the Al2O3 layer is from 0.5 &mgr;m to 25 &mgr;m or from not less than 0.01 &mgr;m to not more than 10 &mgr;m if the thickness (d) of the Al2O3 layer is from more than 25 &mgr;m to 50 &mgr;m.
摘要翻译：根据本发明的切削工具在参与切削的cBN型烧结材料基材的至少一部分表面上涂覆有一种或多种Al 2 O 3层。所述烧结体基板由体积为20〜99体积％的cBN，平均结晶粒径为1μm以下的Al 2 O 3，以不小于1.0％至小于10％的量由卷。 Al 2 O 3层的厚度（d）为0.5〜50μm。如果Al 2 O 3层的厚度（d）为0.5μm至25μm，则Al 2 O 3的平均结晶粒径为0.01μm至4μm，或者如果厚度为0.01μm至10μm以下，则Al 2 O 3的平均结晶粒径为0.01μm至4μm Al 2 O 3层的（d）为25μm〜50μm。

7. 发明授权

US06261329B1 Diamond sintered body having high strength and high wear resistance, and tool including the same 有权
标题翻译：具有高强度和高耐磨性的金刚石烧结体，以及包括该金刚石烧结体的工具
公开(公告)号：US06261329B1
公开(公告)日：2001-07-17
申请号：US09367248
申请日：1999-08-10
申请人： Yasunobu Ogata , Satoru Kukino , Yasuyuki Kanada , Junichi Shiraishi , Tetsuo Nakai
发明人： Yasunobu Ogata , Satoru Kukino , Yasuyuki Kanada , Junichi Shiraishi , Tetsuo Nakai
IPC分类号： C22C105
CPC分类号： C04B35/52 , C22C26/00 , Y10T428/12049
摘要： A diamond sintered body having high wear resistance, chipping resistance, shock resistance and thermal conductivity is provided. The diamond sintered body includes sintered diamond particles and a sintering aid as the remainder. The content of the sintered diamond particles is at least 80% by volume and less than 99% by volume. The sintered diamond particles have a particle size in the range from at least 0.1 &mgr;m to at most 70 &mgr;m. The sintered diamond particles next to each other are directly bonded. The sintering aid includes at least one kind selected from tungsten, iron, cobalt and nickel. The percentage of the tungsten in the sintered body is in the range from at least 0.01% by weight to at most 8% by weight.
摘要翻译：提供了具有高耐磨性，耐崩裂性，抗冲击性和导热性的金刚石烧结体。金刚石烧结体包括烧结金刚石颗粒和其余的烧结助剂。烧结金刚石颗粒的含量为至少80体积％且小于99体积％。烧结金刚石颗粒的粒度在至少0.1μm至至多70μm的范围内。彼此相邻的烧结金刚石颗粒直接结合。烧结助剂包括选自钨，铁，钴和镍中的至少一种。烧结体中钨的百分比在至少0.01重量％至至多8重量％的范围内。

8. 发明授权

US06737178B2 Coated PCBN cutting tools 有权
标题翻译：涂层PCBN切割工具
公开(公告)号：US06737178B2
公开(公告)日：2004-05-18
申请号：US09729149
申请日：2000-12-01
申请人： Michiko Ota , Tomohiro Fukaya , Junichi Shiraishi , Tetsuo Nakai , Hisanori Ohara , Haruyo Fukui
发明人： Michiko Ota , Tomohiro Fukaya , Junichi Shiraishi , Tetsuo Nakai , Hisanori Ohara , Haruyo Fukui
IPC分类号： B23B2714
CPC分类号： C04B41/009 , C04B41/52 , C04B41/89 , C23C30/005 , Y10T407/26 , Y10T407/27 , Y10T428/24364 , Y10T428/252 , Y10T428/265 , C04B41/4529 , C04B41/5068 , C04B41/5133 , C04B41/522 , C04B41/5061 , C04B41/524 , C04B35/5831
摘要： A coated sintered body can be used for a cutting tool for precision machining of hardened steel. The coated PCBN cutting tool includes a substrate which contains not less than 35 volume % and not more than 85 volume % of CBN, and a hard coated layer formed on the substrate. The hard coated layer comprises at least one compound layer consisting of at least one element selected from the group 4a, 5a, and 6a elements of the periodic table and Al, and at least one element selected from C, N and O. The thickness of the layer is not less than 0.3 &mgr;m and not more than 10 &mgr;m. The center-line mean roughness of the hard coated layer is not more than 0.1 &mgr;m.
摘要翻译：涂层烧结体可用于硬化钢精密加工的切削刀具。涂布的PCBN切割工具包括含有不小于35体积％且不大于85体积％的CBN的基底和形成在基底上的硬涂层。硬涂层包含至少一种由选自元素周期表4a，5a和6a元素中的至少一种元素和Al组成的化合物层，以及选自C，N和O中的至少一种元素。该层不小于0.3μm且不大于10μm。硬涂层的中心线平均粗糙度不大于0.1μm。

9. 发明授权

US6065377A Method of cutting hardened steel with high accuracy 有权
标题翻译：高精度切削淬火钢的方法
公开(公告)号：US6065377A
公开(公告)日：2000-05-23
申请号：US175968
申请日：1998-10-21
申请人： Takashi Harada , Tetsuo Nakai , Tomohiro Fukaya , Junichi Shiraishi
发明人： Takashi Harada , Tetsuo Nakai , Tomohiro Fukaya , Junichi Shiraishi
IPC分类号： B23B1/00 , B23B3/00
CPC分类号： B23B1/00 , Y10T407/26 , Y10T407/27 , Y10T82/10
摘要： A method of cutting hardened steel using a cBN sintered tool which can improve the surface roughness while maintaining high dimensional accuracy. The upper limit of the tool feed rate is set at such a value that a theoretical surface roughness calculated from the feed rate is between 2/3 and 1/1000 of the target surface roughness. The amount of change of the feed rate between the upper and lower limits of the tool feed rate is set to be between 0.002 and 0.05 mm/rev, and the amount of every feed rate change is set not to be equal to the original feed rate multiplied by an integer. The feed rate is changed forcibly for every number of workpieces for which the total cutting length is between 10 and 1000 meters.
摘要翻译：使用可以提高表面粗糙度同时保持高尺寸精度的cBN烧结工具来切割硬化钢的方法。刀具进给速度的上限被设定为从进给速度计算的理论表面粗糙度在目标表面粗糙度的2/3和1/1000之间的值。刀具进给速度的上限和下限之间的进给速率的变化量设定在0.002和0.05mm / rev之间，并且每个进给速率变化的量被设定为不等于原始进给速率乘以整数。对于总切割长度在10到1000米之间的每个工件数量，进给速率被强制变化。

10. 发明授权

US06358624B1 Polycrystal diamond tool 有权
标题翻译：多晶金刚石工具
公开(公告)号：US06358624B1
公开(公告)日：2002-03-19
申请号：US09571173
申请日：2000-05-16
申请人： Katsuhito Yoshida , Junichi Shiraishi , Tetsuo Nakai
发明人： Katsuhito Yoshida , Junichi Shiraishi , Tetsuo Nakai
IPC分类号： B22F700
CPC分类号： B22F7/06 , B22F2005/001 , C04B37/026 , C04B2237/083 , C04B2237/12 , C04B2237/123 , C04B2237/124 , C04B2237/125 , C04B2237/363 , C04B2237/401 , C04B2237/66 , C04B2237/704 , C04B2237/706 , C04B2237/72 , C04B2237/76 , C04B2237/82 , C23C30/005 , Y10T428/12007 , Y10T428/30
摘要： The present invention provides a diamond sintered compact tool. Which is excellent in economy as well as cutting edge strength. A diamond sintered compact cutting tool comprising a diamond sintered compact sintered at an ultra-high pressure and high temperature and a WC—Co cemented carbide substrate directly bonded to the diamond sintered compact during a step of sintering and brazed to a tool base through the WC—Co cemented carbide substrate, in which a ratio of the thickness of the WC—Co cemented carbide substrate to the thickness of the diamond sintered compact layer satisfies the relation of: 0.8≦WC—Co cemented carbide substrate/diamond sintered compact layer≦3.0 and the diamond sintered compact layer has a thickness of 0.05 mm to 0.5 mm, preferably 0.05 mm to 0.45 mm, more preferably 0.12 mm to 0.36 mm.
摘要翻译：本发明提供一种金刚石烧结压块工具。具有优异的经济性和切削刃强度。一种金刚石烧结致密切割工具，包括在超高压和高温下烧结的金刚石烧结体和在金刚石烧结体中直接接合的WC-Co硬质合金基体通过WC-Co硬质合金基体烧结并钎焊到工具基底的步骤，其中WC-Co硬质合金基体的厚度与金刚石烧结致密层的厚度之比满足以下关系：和金刚石烧结致密层的厚度为0.05mm〜0.5mm，优选为0.05mm〜0.45mm，更优选为0.12mm〜0.36mm。

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