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1. 发明授权

US3867346A Process for the production of liquid epoxy-novolak resins and product thereof 失效
标题翻译：液态环氧树脂及其制品的生产工艺
公开(公告)号：US3867346A
公开(公告)日：1975-02-18
申请号：US39509273
申请日：1973-09-07
申请人： SIR SOC ITALIANA RESINE SPA
发明人： VARGIU SILVIO , PITZALIS MARIO , CRESPOLINI GIANCARLO
IPC分类号： C07D301/28 , C08G8/00 , C08G8/36 , C08G59/00 , C08G59/08 , C08G5/18
CPC分类号： C08G59/08
摘要： Process for the production of liquid epoxy-novolak resins having high contents of epoxy groups by (a) mixing and homogenizing a novolak phenolic resin having a molecular weight of about 220 to 300 and with about 2.2 to 2.9 phenolic hydroxyl groups per molecule and an epihalohydrin (about 5 to 10 moles of epihalohydrin are used per mole equivalent of phenolic hydroxyl groups in the novolak phenolic resin), (b) contacting the homogenized mixture with kieselguhr at temperatures of about 20* to 40* C and separating the kieselguhr, (c) adding an inorganic base in the course of at least 1 hour at temperatures of about 80* to 115* C (the total quantity of base to be used being so chosen that the ratio of the number of phenolic hydroxyl groups in the novolak resin to the number of equivalents of base is about 0.78:1 to 0.75:1) and (d) separating the liquid epoxynovolak resin from the reaction mixture obtained.
摘要翻译：通过（a）将分子量为约220至300的酚醛清漆酚醛树脂和每分子约2.2至2.9个酚羟基和表卤代醇混合并均化，生产具有高含量环氧基团的液体环氧酚醛清漆树脂的方法（酚醛清漆酚醛树脂中每摩尔当量酚羟基使用约5至10摩尔表卤代醇），（b）将均化的混合物与硅藻土在约20至40℃的温度下接触并分离硅藻土（c ）在约80-115℃的温度下在至少1小时的过程中加入无机碱（所使用的碱的总量被选择为使酚醛清漆树脂中的酚羟基的数量与碱的当量数为约0.78:1至0.75:1）和（d）从获得的反应混合物中分离液体环氧 - 酚醛清漆树脂。

2. 发明授权

US3705117A Process for the manufacture of light building elements 失效
公开(公告)号：US3705117A
公开(公告)日：1972-12-05
申请号：US3705117D
申请日：1970-12-14
申请人： SIR SOC ITALIANA RESINE SPA
发明人： VARGIU SILVIO , PITZALIS MARIO , ABRUZZI PIERLUIGI
IPC分类号： C04B38/08 , C04B20/10 , C08F47/08
CPC分类号： C04B20/1037 , Y10S264/07 , C04B16/08
摘要： LIGHTWEIGHT CONCRETE BUILDING ELEMENTS ARE MADE BY A PROCESS IN WHICH THE ACTION OF EPOXY BINDERS FOR THE POLYSTYRENE GRANULES IS ASSISTED BY THE PRESENCE OF AN ORGANIC SOLVENT, PREFERABLY BENZENE, TOLUENE OR XYLENE.

3. 发明授权

US3896080A Liquid hardeners for liquid epoxy resins, manufacturing method and use 失效
标题翻译：液体环氧树脂用液体硬化剂，制造方法和用途
公开(公告)号：US3896080A
公开(公告)日：1975-07-22
申请号：US39900673
申请日：1973-09-20
申请人： SIR SOC ITALIANA RESINE SPA
发明人： VARGIU SILVIO , BERTI RENATO , PITZALIS MARIO
IPC分类号： C08G59/00 , C07G99/00 , C08G73/00 , C08G73/02 , C08L63/00 , C08L63/02 , C08G30/14
CPC分类号： C08L63/00 , C08L2666/20
摘要： Liquid hardeners for liquid epoxy resins comprising the products of condensation at high temperature of an aromatic polyamine with at least one hydroxy compound selected from the group consisting of polyalkylene glycols, furan alcohols and their polymers and with at least one acidic compound selected from the group consisting of phenols or carboxylic acids. Said liquid hardeners are prepared by heating a mixture of an aromatic polyamine and at least one of the above-mentioned hydroxy compounds for about 60 to 120 minutes to about 90* to 130*C and heating the product obtained with at least one of the above-mentioned acidic compounds for about 1 to 5 hours to about 70* to 170*C.

4. 发明授权

US3876615A Process for the preparation of glycidyl ethers of bisphenols 失效
标题翻译：制备双酚的甘氨酸酯的方法
公开(公告)号：US3876615A
公开(公告)日：1975-04-08
申请号：US31391872
申请日：1972-12-11
申请人： SIR SOC ITALIANA RESINE SPA
发明人： VARGIU SILVIO , PITZALIS MARIO , CRESPOLINI GIANCARLO
IPC分类号： C08G59/00 , C07D301/28 , C08G59/04 , C08G59/06 , C08G59/14 , C08G30/04
CPC分类号： C08G59/04
摘要： Modified liquid epoxy resins of improved viscosity are obtained by reacting bisphenol-A or other diphenols with epichlorohydrin in the presence of polyglycols.

5. 发明授权

US3674732A Rosin modified phenolic resins and method of preparing same 失效
标题翻译：罗辛改性酚醛树脂及其制备方法
公开(公告)号：US3674732A
公开(公告)日：1972-07-04
申请号：US3674732D
申请日：1969-12-10
申请人： SIR SOC ITALIANA RESINE SPA
发明人： PITZALIS MARIO , VARGIU SILVIO , NISTRI UGO
IPC分类号： C08G8/28 , C09D11/10 , C09D161/10 , C08G5/22
CPC分类号： C08G8/34 , C08G8/12 , C08G8/38 , C09D11/102 , C09D11/103
摘要： A method of preparing phenolic resins suitable for the production of inks, characterized in that p-cumyl phenol, formaldehyde, a polyhydroxy alcohol and rosin are polymerized at a temperature of from 130* C. to 270* C. in the presence of a catalyst selected from salts of zinc, calcium, magnesium or manganese with organic or inorganic acids having a dissociation constant (or initial dissociation constant) of less than 1.8 X 10 5, the molar ratio of p-cumyl phenol to formaldehyde being between 1:2.5 and 1:4 and the quantity of rosin from 150 to 200 parts by weight per 100 parts by weight of the phenol.

6. 发明授权

US3860561A Process for the production of epoxy-novolak resins and products thereof 失效
标题翻译：用于生产环氧 - 诺瓦克树脂及其制品的方法
公开(公告)号：US3860561A
公开(公告)日：1975-01-14
申请号：US38722773
申请日：1973-08-09
申请人： SIR SOC ITALIANA RESINE SPA
发明人： VARGIU SILVIO , GIOVANNI SESTO S , PITZALIS MARIO , CRESPOLINI GIANCARLO
IPC分类号： C08G8/00 , C08G8/36 , C08G59/00 , C08G59/08 , C09D163/00 , C08G5/18
CPC分类号： C08G59/08
摘要： Process for the production of solid epoxy-novolak resins having a high content of epoxy groups by adding an inorganic base, preferably sodium hydroxide, in a quantity of about 2 to 10 wt. % of total quantity of base to be used to a fused novolak phenolic resin having an average molecular weight of about 500 to 650 and containing about 5 to 6 phenolic hydroxyl groups per molecule at about 80* to 100*C, the total quantity of base to be used corresponding to about 0.9 to 1.1 equivalents of base per mole equivalent of phenolic hydroxyl groups in the novolak phenolic resin, adding a epihalohydrin to the reaction mixture obtained in the course of at least about 2 hours at temperatures of about 80* to 100*C in a quantity of about 3 to 6 moles per mole equivalent of phenolic hydroxyl groups in the novolak phenolic resin, adding the remainder of the inorganic base to the reaction mixture obtained in the course of at least about 3 hours at temperatures of about 85* to 110*C, and separating the solid epoxy-novolak resin from the reaction mixture obtained.
摘要翻译：通过加入约2-10重量％的无机碱，优选氢氧化钠，生产具有高含量环氧基团的固体环氧 - 酚醛清漆树脂的方法。平均分子量为约500〜650，约80〜100℃，每分子含有约5〜6个酚羟基的熔融酚醛清漆酚醛树脂所用碱的总量的百分比，碱的总量在酚醛清漆酚醛树脂中相对于每摩尔当量酚羟基约0.9-1.1当量碱，在约80℃至100℃的温度下在至少约2小时内获得的反应混合物中加入表卤代醇在酚醛清漆酚醛树脂中每摩尔当量酚羟基约3至6摩尔的量的C C，将剩余的无机碱加入到在约85℃的温度下在至少约3小时的过程中获得的反应混合物 DEG至110℃，并从得到的反应混合物中分离固体环氧 - 酚醛清漆树脂。

7. 发明授权

US3705116A Process for the manufacture of light building elements 失效
标题翻译：轻型建筑元件的制造工艺
公开(公告)号：US3705116A
公开(公告)日：1972-12-05
申请号：US3705116D
申请日：1970-12-10
申请人： SIR SOC ITALIANA RESINE SPA
发明人： VARGIU SILVIO , PITZALIS MARIO , ABRUZZI PIERLUIGI
IPC分类号： C04B38/08 , C04B16/10 , C04B20/10 , C04B28/02 , C08G59/14 , C08J9/236 , C08F47/08
CPC分类号： C08J9/236 , C04B20/1037 , C04B28/02 , C08G59/145 , C08J2325/06 , Y10S264/07 , C04B16/08 , C04B24/28 , C04B20/1018
摘要： LIGHTWEIGHT CONCRETE BUILDING ELEMENTS ARE MADE BY A PROCESS IN WHICH THE POLYSTYRENE GRANULES USED ARE ASSOCIATED WITH A BINDER CONTAINING BOTH A POLYEPOXY COMPOUND AND A MONOEPOXY COMPOUND.

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