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    • 2. 发明授权
    • Method for adding hops in beer manufacture
    • 在啤酒制造中添加啤酒花的方法
    • US09580674B2
    • 2017-02-28
    • US14112149
    • 2012-03-08
    • Ludwig SchellerRudolf MichelPatrick Bahns
    • Ludwig SchellerRudolf MichelPatrick Bahns
    • C12C3/00B01F3/08B01F5/06B01F13/10C12C7/22C12C13/00
    • C12C3/00B01F3/0807B01F5/0661B01F13/103B01F2003/0849C12C7/22C12C13/00
    • The invention relates to a method for adding hops in beer manufacture, having the following process steps; a) separation of a sub-quantity (07a) of water and/or wort (07) and/or beer as an aqueous fluid, b) addition of hop extract (10) in liquid or pasty form to the separated aqueous fluid (07a), c) production of a macroemulsion (13) of the hop extract by emulsifying the hop extract (10) in the aqueous fluid (07a), d) increasing the pressure in the macroemulsion (13) of the hop extract to a feed pressure of in particular higher than 100 bar, e) production of a microemulsion (17) of the hop extract by feeding the pressurized macroemulsion (13) through a gap or a valve (16) or by feeding the pressurized macroemulsion against a baffle plate, f) at least partial return of the microemulsion (17) of the hop extract to the beer manufacturing process.
    • 本发明涉及啤酒加工啤酒花的方法,具有以下工艺步骤; a)以水和/或麦芽汁(07)和/或啤酒作为水性液体分离子量(07a)和/或啤酒; b)将液体或糊状形式的啤酒花提取物(10)加入到分离的含水流体(07a) ),c)通过在水性流体(07a)中乳化啤酒花提取物(10)来生产啤酒花提取物的粗乳液(13),d)将啤酒花提取物的粗乳液(13)中的压力增加到进料压力 特别是高于100巴,e)通过将加压的粗乳液(13)通过间隙或阀(16)供给或通过将加压的宏乳剂输送到挡板上来生产啤酒花提取物的微乳液(17),f )啤酒花提取物的微乳液(17)的至少部分返回到啤酒制造过程。
    • 3. 发明授权
    • Process for the production of sulfur containing organosilicon compounds
    • 含硫有机硅化合物生产工艺
    • US4129585A
    • 1978-12-12
    • US884212
    • 1978-03-07
    • Wolfgang BuderHans-Dieter PletkaRudolf MichelRudolf SchwarzGerhard Dusing
    • Wolfgang BuderHans-Dieter PletkaRudolf MichelRudolf SchwarzGerhard Dusing
    • C07F7/18C08K5/548C08K5/549C07F7/08C07F7/10
    • C08K5/548C07F7/1892C08K5/549
    • There is provided a process for the production of sulfur containing organosilicon compounds of the formula (I) Z -- Alk -- S.sub.x -- Alk -- Z, where Z is the grouping: ##STR1## in which R.sup.1 is an alkyl group having 1 to 5 carbon atoms, a cycloalkyl group with 5 to 8 carbon atoms, the benzyl group, phenyl or phenyl substituted with at least one methyl, ethyl or chloro group, R.sup.2 is alkoxy of 1 to 4 carbon atoms, methoxyethoxy, cycloalkoxy with 5 to 8 carbon atoms, phenoxy or benzyloxy, R.sup.3 and R.sup.4 are alkyl of 1 to 3 carbon atoms or hydrogen, Alk is divalent saturated hydrocarbon group having 1 to 5 carbon atoms or such a group interrupted by --O--, --S-- or --NH-- and x is a number from 2.0 to 6.0 comprising reacting an alkali metal alcoholate, preferably in alcoholic solution with a compound of the formula (II) Z -- Alk -- Hal, where Hal is chlorine, bromine or iodine with a hydrosulfide of the formula (III) MeSH, in which Me is ammonium, an alkali metal atom or an equivalent of an alkaline earth metal or zinc and with sulfur, preferably in the presence of at least one organic solvent, separating from the halide formed, and removing the organic solvent.
    • 提供了一种制备式(I)Z-Alk-Sx-Alk-Z的含硫有机硅化合物的方法,其中Z是分组:其中R 1是烷基 具有1至5个碳原子的环烷基,具有5至8个碳原子的环烷基,苄基,苯基或被至少一个甲基,乙基或氯基取代的苯基,R 2是1至4个碳原子的烷氧基,甲氧基乙氧基, 5至8个碳原子,苯氧基或苄氧基,R3和R4是1至3个碳原子的烷基或氢,Alk是具有1至5个碳原子的二价饱和烃基或被-O - , - S-或 - -NH-,x是2.0至6.0的数,包括使碱金属醇盐,优选在醇溶液中与式(II)化合物Z-Alk-Hal反应,其中Hal为氯,溴或碘,其中硫氢化物为 Me III,其中Me为铵,碱金属原子或碱性ea当量 第二金属或锌和硫,优选在至少一种有机溶剂的存在下,与形成的卤化物分离,并除去有机溶剂。
    • 4. 发明授权
    • Process for the production of sulfur containing organosilicon compounds
    • 含硫有机硅化合物生产工艺
    • US4072701A
    • 1978-02-07
    • US730726
    • 1976-09-24
    • Hans-Dieter PletkaRudolf Michel
    • Hans-Dieter PletkaRudolf Michel
    • C07F7/08C07F7/18C08K5/548C08K5/549
    • C08K5/548C07F7/1892C08K5/549
    • There is provided a process for the production of sulfur containing organosilicon compounds of the formula (I) Z--Alk--S.sub.x --Alk--Z, where Z is the grouping: ##STR1## in which R.sup.1 is an alkyl group having 1 to 8 carbon atoms, a cycloalkyl group with 5 to 8 carbon atoms, the benzyl group, phenyl or phenyl substituted with at least one methyl, ethyl or chloro group and R.sup.2 is alkoxy of 1 to 8 carbon atoms, methoxyethoxy, cycloalkoxy with 5 to 8 carbon atoms, phenoxy or benzyloxy, Alk is divalent saturated hydrocarbon group having 1 to 10 carbon atoms or such a group interrupted once or twice by --O--, --S-- or --NH-- and x is a number from 2.0 to 6.0 comprising reacting a compound of the formula (II) Y--Alk--Hal, where Y is: ##STR2## WHERE Hal is fluorine, chlorine, bromine or iodine with at least one compound of the formula R.sup.3 OH in which R.sup.3 is alkyl of 1 to 8 carbon atoms, methoxyethyl, cycloalkyl with 5 to 8 carbon atoms, phenyl or benzyl or in the case of forming (d) reacting a tris alkoxysilane with triethanolamine to form the corresponding silatrane and with a hydrosulfide of the formula (III) MeSH, in which Me is ammonium, an alkali metal atom or an equivalent of an alkaline earth metal and with sulfur, preferably in the presence of at least one organic solvent, separating from the halide formed, and removing the organic solvent.
    • 提供了制备式(I)的Z-Alk-Sx-Alk-Z的含硫有机硅化合物的方法,其中Z是分组:其中R 1是具有1个 8个碳原子的环烷基,具有5至8个碳原子的环烷基,苄基,苯基或被至少一个甲基,乙基或氯基取代的苯基,R 2是1至8个碳原子的烷氧基,甲氧基乙氧基,环烷氧基, 8个碳原子,苯氧基或苄氧基,Alk是具有1-10个碳原子的二价饱和烃基,或者被-O - , - S-或-NH-中断一次或两次的基团,x是2.0至6.0的数,包括 使式(II)Y-Alk-Hal的化合物与其中Y是:其中Hal是氟,氯,溴或碘与至少一种式R 3 OH的化合物反应,其中R 3是1至8的烷基 碳原子,甲氧基乙基,具有5至8个碳原子的环烷基,苯基或苄基,或在形成(d)使三烷氧基硅烷 e与三乙醇胺形成相应的硅藻土和与式(III)MeSH的氢硫化物,其中Me是铵,碱金属原子或碱当量的碱土金属和硫,优选在至少一种 有机溶剂,与形成的卤化物分离,除去有机溶剂。