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1. 发明授权

US5891574A Polyazacycloalkanes, tri-, tetra- or penta-azamacrocyclic complexes, processs for the production of these substituted or unsubstituted polyazacycloalkanes grafted to a support and uses of polyazacycloalkanes and the aforementioned complexes 失效
标题翻译：多氮杂环烷烃，三，四或五氮杂十环配合物，用于制备接枝到载体上的这些取代或未取代的多氮杂环烷烃的方法和多氮杂环烷烃和上述络合物的用途
公开(公告)号：US5891574A
公开(公告)日：1999-04-06
申请号：US646330
申请日：1997-04-25
申请人： Roger Guilard , Herve Chollet , Philippe Guiberteau , Panayotis Cocolios
发明人： Roger Guilard , Herve Chollet , Philippe Guiberteau , Panayotis Cocolios
IPC分类号： B01D53/04 , B01D53/14 , B01J45/00 , C08F12/32 , G21F9/12 , B32B5/16 , C07D255/02
CPC分类号： G21F9/12 , B01D53/1493 , B01J45/00 , C08F12/32 , B01D2253/106 , B01D2259/4583 , Y10T428/2991 , Y10T428/2993 , Y10T428/2998
摘要： The invention relates to polyazacycloalkanes having 3, 4 or 5 nitrogen atoms, tri-, tetra- or penta-azamacrocyclic transition metal complexes and processes for the production of said polyazacycloalkanes.The object of the invention is to form polyazacycloalkanes able to trap metal cations and in particular U, Pu, Am, Ce, Eu, Al, Gd, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ag, Cd, Sn, Au, Mg or Pb or complexes able to trap in particular oxygen in a gaseous mixture.The invention more particularly applies to the treatment of liquid effluents from nuclear power stations.
摘要翻译：本发明涉及具有3,4或5个氮原子的多氮杂环烷烃，三 - ，四 - 或五 - 氮杂十八烷基过渡金属络合物和用于生产所述多氮杂环烷烃的方法。本发明的目的是形成能够捕获金属阳离子，特别是U，Pu，Am，Ce，Eu，Al，Gd，Cr，Mn，Fe，Co，Ni，Cu，Zn，Ag，Cd，Sn的多氮杂环烷烃，Au，Mg或Pb或能够在气体混合物中捕获特别是氧的络合物。本发明更特别适用于从核电站处理液体流出物。

2. 发明授权

US06265483B1 Polyazacycloalkanes, tri, tetra- or penta-azamacrocyclic complexes, processes for the production of these substituted or unsubstituted polyazacycloalkanes grafted to a support and uses of polyazacycloalkanes and the aforementioned complexes 失效
标题翻译：多氮杂环烷烃，三，四或五氮杂十环配合物，用于制备接枝到载体上的这些取代或未取代的多氮杂环烷烃的方法和多氮杂环烷烃和上述络合物的用途
公开(公告)号：US06265483B1
公开(公告)日：2001-07-24
申请号：US09190144
申请日：1998-11-12
申请人： Roger Guilard , Hervé Chollet , Philippe Guiberteau , Panayotis Cocolios
发明人： Roger Guilard , Hervé Chollet , Philippe Guiberteau , Panayotis Cocolios
IPC分类号： C07D25502
CPC分类号： G21F9/12 , B01D53/1493 , B01D2253/106 , B01D2259/4583 , B01J45/00 , C08F12/32 , Y10T428/2991 , Y10T428/2993 , Y10T428/2998
摘要： The invention relates to polyazacycloalkanes having 3, 4 or 5 nitrogen atoms, tri-, tetra- or penta-azamacrocyclic transition metal complexes and processes for the production of said polyazacycloalkanes. The object of the invention is to form polyazacycloalkanes able to trap metal cations and in particular U, Pu, Am, Ce, Eu, Al, Gd, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ag, Cd, Sn, Au, Mg or Pb or complexes able to trap in particular oxygen in a gaseous mixture. The invention more particularly applies to the treatment of liquid effluents from nuclear power stations.
摘要翻译：本发明涉及具有3,4或5个氮原子的多氮杂环烷烃，三，四或五氮杂十八烷基过渡金属络合物以及用于制备所述多氮杂环烷烃的方法。本发明的目的是形成能够捕获金属阳离子的多氮杂环烷烃，特别是U，Pu，Am，Ce，Eu，Al，Gd，Cr，Mn，Fe，Co，Ni，Cu，Zn，Ag，Cd，Sn，Au，Mg或Pb或能够特别吸留氧的络合物气体混合物。本发明更特别适用于处理来自核电站的液体流出物。

3. 发明授权

US06410143B1 POLYAZACYCLOALKANES, TRI-, TETRA- OR PENTA-AZAMACROCYCLIC COMPLEXES, PROCESSES FOR THE PRODUCTION OF THESE SUBSTITUTED OR UNSUBSTITUTED POLYAZACYCLOALKANES GRAFTED TO A SUPPORT AND USES OF POLYAZACYCLOALKANES AND THE AFOREMENTIONED COMPLEXES 失效
标题翻译：聚氮杂环戊烷，三异氰酸酯，四环戊基或三甲基环烷基复合物，生产这些取代或未取代的聚氨基甲酸酯的方法，用于支持和使用聚氨基甲酸酯和已制备的复合物
公开(公告)号：US06410143B1
公开(公告)日：2002-06-25
申请号：US09667506
申请日：2000-09-22
申请人： Roger Guilard , Hervé Chollet , Philippe Guiberteau , Panayotis Cocolios
发明人： Roger Guilard , Hervé Chollet , Philippe Guiberteau , Panayotis Cocolios
IPC分类号： B32B516
CPC分类号： G21F9/12 , B01D53/1493 , B01D2253/106 , B01D2259/4583 , B01J45/00 , C08F12/32 , Y10T428/2991 , Y10T428/2993 , Y10T428/2998
摘要： The invention relates to polyazacycloalkanes having 3, 4 or 5 nitrogen atoms, tri-, tetra- or penta-azamacrocyclic transition metal complexes and processes for the production of said polyazacycloalkanes. The object of the invention is to form polyazacycloalkanes able to trap metal cations and in particular U, Pu, Am, Ce, Eu, Al, Gd, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ag, Cd, Sn, Au, Mg or Pb or complexes able to trap in particular oxygen in a gaseous mixture. The invention more particularly applies to the treatment of liquid effluents from nuclear power stations.
摘要翻译：本发明涉及具有3,4或5个氮原子的多氮杂环烷烃，三，四或五氮杂十八烷基过渡金属络合物以及用于制备所述多氮杂环烷烃的方法。本发明的目的是形成能够捕获金属阳离子的多氮杂环烷烃，特别是U，Pu，Am，Ce，Eu，Al，Gd，Cr，Mn，Fe，Co，Ni，Cu，Zn，Ag，Cd，Sn，Au，Mg或Pb或能够特别吸留氧的络合物气体混合物。本发明更特别适用于处理来自核电站的液体流出物。

4. 发明授权

US06310202B1 Nitric oxide carriers based on polyazamacrocycle complexes 失效
标题翻译：基于多氮杂环络合物的一氧化氮载体
公开(公告)号：US06310202B1
公开(公告)日：2001-10-30
申请号：US09423363
申请日：2000-01-11
申请人： Alain Tabard , Olivier Siri , Panayotis Cocolios , Roger Guilard
发明人： Alain Tabard , Olivier Siri , Panayotis Cocolios , Roger Guilard
IPC分类号： C07D25502
CPC分类号： C07F15/045 , C07F15/025
摘要： Novel compounds capable of carrying and releasing nitrogen oxide (NO) in a biological medium, their use for implementing a therapeutic treatment method or a diagnostic method applied to a human or animal body, and for making medicines useful for treating or preventing disorders affecting the human or animal cardiovascular, nervous, immune, renal or pulmonary system, specifically, an organometallic complex of nitrogen oxide, wherein the cationic part is of the formula (I) in which x=0 or 1; x′=2 or 3; y=0, 2 or 3; z=0 or 1; with the condition that, if y=0 (or z=0) then z=0 (or y=0; respectively); R is a group chosen from the group formed by: a hydrogen atom, —(CH2)2COOH and R1, R2, R3 and R4 are groups chosen from the group formed by: a hydrogen atom and alkyl groups comprising from 1 to 4 carbon atoms; and M2+ is a divalent cation Fe++ or Co++.
摘要翻译：能够在生物培养基中携带和释放氮氧化物（NO）的新型化合物，其用于实施治疗方法或应用于人体或动物体的诊断方法，以及用于制备治疗或预防影响人类的病症的药物或动物心血管，神经，免疫，肾或肺系统，特别是氮氧化物的有机金属络合物，其中阳离子部分为式（I），其中x = 0或1; x'= 2或3; y = 0 2或3; z = 0或1;条件是，如果y = 0（或z = 0），则z = 0（或分别为y = 0）; R为选自以下的基团：氢原子， - （CH 2）2 COOH和R 1，R 2，R 3和R 4是选自由氢原子和含有1至4个碳原子的烷基形成的基团; 和M2 +是二价阳离子Fe ++或Co ++。

5. 发明申请

US20100059446A1 MATERIAL COMPRISING POLYAZACYCLOALKANES, GRAFTED ON POLYPROPYLENE FIBRES, ITS PROCESS OF PREPARATION, AND PROCESS FOR REMOVING METAL CATIONS FROM A LIQUID 有权
标题翻译：包含在聚丙烯纤维上制备聚丙烯酰胺的材料，其制备方法以及从液体中除去金属的方法
公开(公告)号：US20100059446A1
公开(公告)日：2010-03-11
申请号：US12523330
申请日：2008-01-14
申请人： Frederic Rascalou , Franck Denat , Roger Guilard , Jean-Louis Babouhot , Herve Chollet , Michel Meyer
发明人： Frederic Rascalou , Franck Denat , Roger Guilard , Jean-Louis Babouhot , Herve Chollet , Michel Meyer
IPC分类号： C08F271/02 , C08J3/28 , C02F1/42
CPC分类号： D06M14/10 , C08F8/30 , D06M14/28 , C08F10/06
摘要： Material composed of a polyazacycloalkane grafted on polypropylene fibres.Process for the preparation of this material.Process for removing metal cations present in a liquid by bringing this liquid into contact with the said material.
摘要翻译：由在聚丙烯纤维上接枝的多氮杂环烷烃组成的材料。制备该材料的方法。通过使该液体与所述材料接触来除去存在于液体中的金属阳离子的方法。

6. 发明授权

US07312327B2 Method of preparing nitrogen macrocycles 失效
标题翻译：制备氮大环的方法
公开(公告)号：US07312327B2
公开(公告)日：2007-12-25
申请号：US10490948
申请日：2002-09-27
申请人： Frederic Boschetti , Franck Denat , Roger Guilard , Henry Ledon , Herve Chollet , Jean-Louis Babouhot
发明人： Frederic Boschetti , Franck Denat , Roger Guilard , Henry Ledon , Herve Chollet , Jean-Louis Babouhot
IPC分类号： C07D257/02
CPC分类号： C07D487/08 , C07D257/02
摘要： The invention relates to a method of preparing nitrogen macrocycles having formula (I). The inventive method comprises a step involving the reaction of compounds (II) and (III) in order to form a compound having formula (IV). Said compound is subsequently made to react with a compound having formula (V) in order to form a compound having formula (VI). The latter compound is then subjected to an acid treatment
摘要翻译：本发明涉及制备具有式（I）的氮大环化合物的方法。本发明的方法包括涉及化合物（II）和（III）的反应以形成具有式（IV）的化合物的步骤。随后使所述化合物与具有式（V）的化合物反应，以形成具有式（VI）的化合物。然后将后一种化合物进行酸处理

7. 发明授权

US08975395B2 Materials for the solid/liquid extraction of heavy metal ions, containing supported N-functionalized polyazacycloalkanes 有权
标题翻译：用于固体/液体提取重金属离子的材料，含有负载的N-官能化的多氮杂环烷烃
公开(公告)号：US08975395B2
公开(公告)日：2015-03-10
申请号：US12735980
申请日：2009-02-20
申请人： Michel Meyer , Arnaud Bucaille , Francois Cuenot , Franck Denat , Frédéric Boschetti , Roger Guilard
发明人： Michel Meyer , Arnaud Bucaille , Francois Cuenot , Franck Denat , Frédéric Boschetti , Roger Guilard
IPC分类号： C07D257/02 , B01J20/22 , B01J20/26 , C07F7/08
CPC分类号： C07F7/0836 , C07B2200/11
摘要： The present invention relates to a material notably adapted for the extraction of metal cations in an aqueous medium, comprising a solid support on which are attached polyazacycloalkane compounds having a ring including at least 4 nitrogen atoms, and wherein the nitrogen atoms of the ring are substituted with coordinating groups, which each are independently: a coordinating group of formula: —(CH2)n—C(═O)—NR1R2 or else a both coordinating and binding group, fitting the formula: —(CH2)p—C(═O)—NR3-(A)-[support]. The invention also relates to methods for preparing the aforementioned materials and to different uses thereof, notably for the extraction of Pb2+ cations in an aqueous medium.
摘要翻译：本发明涉及一种特别适用于在含水介质中萃取金属阳离子的材料，其中包括一种固体载体，其中连接有多环氮杂环烷烃化合物，该化合物具有包含至少4个氮原子的环，并且其中该环的氮原子被取代配位基团，各自独立地是： - （CH 2）n -C（= O）-NR 1 R 2的配位基团，或者是配位和结合基团，配合下式： - （CH 2）p -C（= O）-NR 3 - （A） - [支持]。本发明还涉及制备上述材料及其不同用途的方法，特别是用于在水性介质中萃取Pb 2+阳离子。

8. 发明授权

US06524372B1 Silica gel incorporating polyazacycloalkane structural units 有权
标题翻译：掺有多氮杂环烷结构单元的硅胶
公开(公告)号：US06524372B1
公开(公告)日：2003-02-25
申请号：US09600954
申请日：2000-07-25
申请人： Robert Corriu , Catherine Reye , Ahmad Mehdi , Gérard Dubois , Claude Chuit , Franck Denat , Bruno Roux-Fouillet , Roger Guilard , Gilles Lagrange , Stéphane Brandes
发明人： Robert Corriu , Catherine Reye , Ahmad Mehdi , Gérard Dubois , Claude Chuit , Franck Denat , Bruno Roux-Fouillet , Roger Guilard , Gilles Lagrange , Stéphane Brandes
IPC分类号： B01D5302
CPC分类号： C07F7/0896 , B01D53/02 , B01D2253/20 , B01D2253/202 , B01D2256/12 , B01D2257/104 , C01B13/0262 , C01B15/013 , C01B21/0455 , C01B2210/0045 , C01B2210/0046 , C07F7/1804
摘要： A novel compound which can be used in the field of separation and purification of gases is disclosed. The compound can be incorporated into a silica gel incorporating polyazacycloalkane structural units for separating a predetermined gas from a mixture of gases. The mixture of gases is brought into contact with a metallated hybrid gel under conditions which make possible the absorption of the gas to be separated, followed by a phase of desorption of the attached gas, and the recovery of the gas.
摘要翻译：公开了一种可用于气体分离和纯化领域的新型化合物。该化合物可以并入含有用于从气体混合物中分离预定气体的多氮杂环烷结构单元的硅胶中。使气体混合物与金属化混合凝胶接触，使得可能吸收待分离的气体，随后附着气体的解吸相和气体的回收。

9. 发明授权

US08247392B2 Materials for selective trapping of carbon monoxide 有权
标题翻译：用于选择性捕获一氧化碳的材料
公开(公告)号：US08247392B2
公开(公告)日：2012-08-21
申请号：US10485935
申请日：2002-07-19
申请人： François Jerome , Géraud Dubois , Stéphane Brandes , Gabriel Canard , Jean-Michel Barbe , Roger Guilard , Bruno Roux-Fouillet , Henry Ledon
发明人： François Jerome , Géraud Dubois , Stéphane Brandes , Gabriel Canard , Jean-Michel Barbe , Roger Guilard , Bruno Roux-Fouillet , Henry Ledon
IPC分类号： C07D487/22
CPC分类号： C07D487/22 , B01D53/02 , B01D2257/502 , B01J20/103 , B01J20/223 , B01J20/28083 , B01J20/3204 , B01J20/3217 , B01J20/3219 , B01J20/3257 , B01J20/3259 , B01J20/3261 , B01J20/3265 , C01B3/56 , C01B13/0262 , C01B2203/042 , C01B2203/047 , C01B2210/005 , C07F7/1804 , C07F15/025 , C07F15/065
摘要： Compounds of formula (I) are disclosed. The tetrapyrole ring in formula (I) can be substituted with a metal cation (M); R1, R2, R3 and R4 separately represent a hydrogen atom, a C1-4 alkyl or alkyloxy radical, or a phenyl radical optionally substituted by vinyl, hydroxy, nitro, amino, bromo, chloro, fluoro, iodo, benzyloxy, or hydroxymethyl radicals; R5, R6, R7 and R8 separately represent a hydrogen atom or a C1-4 alkyl radical; Ra, Rb and Rc separately represent a hydrogen atom, a C1-4 alkyl or alkyloxy radical optionally substituted by a halogen, or a phenyl radical optionally substituted by vinyl, hydroxy, nitro, amino, bromo, chloro, fluoro, iodo, benzyloxy, or hydroxymethyl radicals, wherein at least one of Ra, Rb, and Rc is a phenyl radical. Compounds of formula (I) bound to a silica, a sol-gel material or a mesoporous silica are useful for selective trapping of carbon monoxide.
摘要翻译：公开了式（I）的化合物。式（I）中的四氟环可以被金属阳离子（M）取代; R1，R2，R3和R4分别表示氢原子，C1-4烷基或烷氧基，或任选被乙烯基，羟基，硝基，氨基，溴，氯，氟，碘，苄氧基或羟甲基取代的苯基 ; R5，R6，R7和R8分别表示氢原子或C1-4烷基; Ra，Rb和Rc分别表示氢原子，任选被卤素取代的C 1-4烷基或烷氧基，或任选被乙烯基，羟基，硝基，氨基，溴，氯，氟，碘，苄氧基，或羟甲基，其中Ra，Rb和Rc中的至少一个是苯基。与二氧化硅，溶胶 - 凝胶材料或介孔二氧化硅结合的式（I）化合物可用于选择性捕获一氧化碳。

10. 发明申请

US20110079557A1 MATERIALS FOR THE SOLID/LIQUID EXTRACTION OF HEAVY METAL IONS, CONTAINING SUPPORTED N-FUNCTIONALIZED POLYAZACYLOALKANES 有权
标题翻译：用于固体/液体提取重金属离子的材料，含有支持的N-官能化聚山梨醇
公开(公告)号：US20110079557A1
公开(公告)日：2011-04-07
申请号：US12735980
申请日：2009-02-20
申请人： Michel Meyer , Arnaud Bucaille , Francois Cuenot , Franck Denat , Frédéric Boschetti , Roger Guilard
发明人： Michel Meyer , Arnaud Bucaille , Francois Cuenot , Franck Denat , Frédéric Boschetti , Roger Guilard
IPC分类号： C07F7/18 , C02F1/26 , C02F1/62 , B01D11/02
CPC分类号： C07F7/0836 , C07B2200/11
摘要： The present invention relates to a material notably adapted for the extraction of metal cations in an aqueous medium, comprising a solid support on which are attached polyazacycloalkane compounds having a ring including at least 4 nitrogen atoms, and wherein the nitrogen atoms of the ring are substituted with coordinating groups, which each are independently: a coordinating group of formula: —(CH2)n—C(═O)—NR1R2 or else a both coordinating and binding group, fitting the formula: —(CH2)p—C(═O)—NR3-(A)-[support]. The invention also relates to methods for preparing the aforementioned materials and to different uses thereof, notably for the extraction of Pb2+ cations in an aqueous medium.
摘要翻译：本发明涉及一种特别适用于在含水介质中萃取金属阳离子的材料，其中包括一种固体载体，其中连接有多环氮杂环烷烃化合物，该化合物具有包含至少4个氮原子的环，并且其中该环的氮原子被取代配位基团，各自独立地是： - （CH 2）n -C（= O）-NR 1 R 2的配位基团，或者是配位和结合基团，配合下式： - （CH 2）p -C（= O）-NR 3 - （A） - [支持]。本发明还涉及制备上述材料及其不同用途的方法，特别是用于在水性介质中萃取Pb 2+阳离子。

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