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1. 发明授权

US4226628A Cuprous copper and/or silver halophosphate glasses 失效
标题翻译：铜铜和/或卤代磷酸银眼镜
公开(公告)号：US4226628A
公开(公告)日：1980-10-07
申请号：US61901
申请日：1979-07-30
申请人： Roger F. Bartholomew , William G. Dorfeld , James A. Murphy , Joseph E. Pierson , Stanley D. Stookey , Paul A. Tick
发明人： Roger F. Bartholomew , William G. Dorfeld , James A. Murphy , Joseph E. Pierson , Stanley D. Stookey , Paul A. Tick
IPC分类号： C03C3/23 , C03C3/247 , H01M6/18 , C03C3/16
CPC分类号： H01M6/18 , C03C3/23 , C03C3/247
摘要： This invention is related to the production of glasses having compositions within the copper and/or silver-halide-phosphate field, wherein at least one halide is present selected from the group of fluoride, chloride, bromide, and iodide, such glasses exhibiting softening points below about 400.degree. C., coefficients of thermal expansion (25.degree.-300.degree. C.) in excess of about 180.times.10.sup.-7 /.degree.C., high electrical conductivity, and electrochromic behavior. The copper-containing glasses may also demonstrate thermochromic properties.
摘要翻译：本发明涉及在铜和/或卤化银 - 磷酸盐领域中具有组成的玻璃的制备，其中至少一种卤化物存在选自氟化物，氯化物，溴化物和碘化物，这种玻璃表现出软化点低于约400℃，热膨胀系数（25-300℃）超过约180×10 -7 /℃，高导电性和电致变色行为。含铜玻璃也可以显示出热致变色性质。

2. 发明授权

US3948629A Hydration of silicate glasses in aqueous solutions 失效
标题翻译：在水溶液中水化硅酸盐玻璃
公开(公告)号：US3948629A
公开(公告)日：1976-04-06
申请号：US465243
申请日：1974-04-29
申请人： Roger F. Bartholomew , Larry E. Campbell , Stanley S. Lewek , Joseph E. Pierson , Stanley D. Stookey
发明人： Roger F. Bartholomew , Larry E. Campbell , Stanley S. Lewek , Joseph E. Pierson , Stanley D. Stookey
IPC分类号： C03C3/076 , C03C23/00 , C03C17/00
CPC分类号： C03C23/00
摘要： The present invention relates to a method for hydrating fine-dimensioned alkali metal-containing silicate glass bodies so as to impart the property of thermoplasticity thereto. More particularly, this invention contemplates contacting fine-dimensioned alkali metal silicate glass bodies with an aqueous solution at elevated temperatures and pressures to develop at least a surface layer thereon having a water content ranging up to about 36% by weight, said aqueous solution having a pH less than 6 as measured at room temperature. The hydrated bodies can approach certain properties of high-polymer organic plastics and exhibit the capability of being thermoplastically formed at relatively low temperatures.
摘要翻译：本发明涉及一种水合精细尺寸的含碱金属的硅酸盐玻璃体以赋予其热塑性的特性的方法。更具体地说，本发明考虑在高温和高压下将精细尺寸的碱金属硅酸盐玻璃体与水溶液接触，以至少在其上含有至多约36重量％水含量的表面层，所述水溶液具有 pH小于6，在室温下测得。水合体可以接近高分子有机塑料的某些性能，并具有在较低温度下热塑性形成的能力。

3. 发明授权

US5696785A Impurity getters in laser enclosures 失效
标题翻译：激光外壳中的杂质吸气剂
公开(公告)号：US5696785A
公开(公告)日：1997-12-09
申请号：US320549
申请日：1994-10-11
申请人： Roger F. Bartholomew , Margaret K. Faber , Julia A. Sharps , Kenneth E. Zaun
发明人： Roger F. Bartholomew , Margaret K. Faber , Julia A. Sharps , Kenneth E. Zaun
IPC分类号： H01S3/08 , B01D53/28 , B01J20/18 , H01L33/48 , H01M2/04 , H01M2/12 , H01S3/02 , H01S3/03 , H01S3/06 , H01S3/094 , H01S3/14 , H01S5/022 , H01S3/22 , H01S3/223
CPC分类号： H01L33/483 , H01S5/02204 , H01S5/02284
摘要： A getter for immobilizing water and organic molecules which may be present as impurities in an enclosure for a high power laser. The getter is formulated from selected zeolite compositions having a pore or channel size suitable for immobilizing water and a size range of organic molecules up to about 40 microns. A binder is used to provide a getter having sufficient strength to allow use of the getter in a laser enclosure in a telecommunications application. The binder also provides a substantially dust free getter body to maintain the cleanliness of the interior of the laser enclosure. Getters which immobilize only organics or only water are contemplated.
摘要翻译：用于固定水和有机分子的吸气剂，其可以作为高功率激光器的外壳中的杂质存在。吸气剂由具有适合于固定水的孔或通道尺寸的选定沸石组合物和高达约40微米的有机分子的尺寸范围配制。粘合剂用于提供具有足够强度的吸气剂以允许在电信应用中的激光外壳中使用吸气剂。粘合剂还提供了基本上无粉尘的吸气体，以保持激光外壳内部的清洁度。预期仅限有机物或仅限于水的吸气剂。

4. 发明授权

US5151117A Solution doping of porous preforms 失效
标题翻译：多孔预制件的溶液掺杂
公开(公告)号：US5151117A
公开(公告)日：1992-09-29
申请号：US715348
申请日：1991-06-14
申请人： Roger F. Bartholomew , Andrea L. Sadd
发明人： Roger F. Bartholomew , Andrea L. Sadd
IPC分类号： C03B8/04 , C03B8/00 , C03B20/00 , C03B37/014 , C03C3/06 , C03C13/04 , C03C23/00 , G02B6/00
CPC分类号： C03C23/0095 , C03B37/01433 , C03B2201/34 , C03B2207/85 , Y10S65/901
摘要： Disclosed is a method of forming a doped glass body. The glass body is formed by adding a dopant to a glass preform, at least part of which has interconnective pores. The porous preform is immersed in a solution of a salt of the dopant dissolved in an organic solvent having no OH groups. The solvent is removed, and the porous glass preform is heat treated to consolidate it into a non-porous glassy body containing the dopant dispersed throughout at least a portion of the body. An OH-free solvent is selected because of its beneficial effect on the preform during the drying step. Whereas OH-containing solvents such as water and alcohol caused cracking and/or flaking of the outer surface of the porous preform following the drying step, an undamaged surface is formed by the present invention.

5. 发明授权

US06356699B1 Rare earth doped optical glasses 失效
标题翻译：稀土掺杂光学眼镜
公开(公告)号：US06356699B1
公开(公告)日：2002-03-12
申请号：US09130800
申请日：1998-08-07
申请人： Roger F. Bartholomew , Heather D. Boek , Michelle D. Pierson , Carlton M. Truesdale
发明人： Roger F. Bartholomew , Heather D. Boek , Michelle D. Pierson , Carlton M. Truesdale
IPC分类号： G02B600
CPC分类号： C03C4/0071 , C03C3/095 , H01S3/1603 , H01S3/17 , H01S3/176
摘要： A glass component in an optical system, which may be a lazing or an optical amplifying medium, comprising a silicate base glass doped with at least two Group III B elements, the glass, and a method of preventing clustering of a rare earth metal ion in the glass.
摘要翻译：光学系统中的玻璃组分，其可以是釉料或光学放大介质，其包含掺杂有至少两种IIIB族元素的玻璃基底玻璃，所述玻璃以及防止稀土金属离子聚集的方法玻璃。

6. 发明授权

US4133665A Hydration of silicate glasses in alcohol-water solutions 失效
标题翻译：水溶液中的硅酸盐玻璃
公开(公告)号：US4133665A
公开(公告)日：1979-01-09
申请号：US829731
申请日：1977-09-01
申请人： Roger F. Bartholomew , William L. Haynes , Leon M. Sanford
发明人： Roger F. Bartholomew , William L. Haynes , Leon M. Sanford
IPC分类号： C03C21/00 , C03C23/00 , C03C15/00 , C03B21/00
CPC分类号： C03C21/002 , C03C23/00 , Y10T428/315
摘要： The present invention is concerned with the production of sodium and/or potassium hydrosilicate glass bodies. The basis of the invention resides in the hydration of anhydrous sodium and/or potassium silicate glass bodies in aqueous alcohol solutions to impart enhanced mechanical strength and thermoplastic properties thereto. The hydrating process, which permits close control to be maintained over the water content absorbed in the glass, can be carried out in liquid solutions of water and relatively short chain, i.e. up to about five carbon atoms, aliphatic alcohols or in gaseous atmospheres of such solutions. An ion exchange reaction of Li.sup.+ ions or protons with Na.sup.+ and/or K.sup.+ ions can be promoted at temperatures above the transformation range of the hydrated glass, and an exchange of K.sup.+ ions for Na.sup.+ and/or Li.sup.+ ions at temperatures below the transformation range. The invention also contemplates treating sodium and/or potassium hydrosilicate glass bodies, produced through the previous hydration of sodium and/or potassium silicate glass bodies, in a gaseous or liquid alcohol or water-alcohol mixture to impart increased strength and impact resistance thereto and alter the absorbed water content therein. The aforementioned ion exchange reactions are also applicable here.
摘要翻译：本发明涉及生产水合硅酸钠和/或钾的玻璃体。本发明的基础是在醇水溶液中水合无水的钠和/或硅酸钾玻璃体以赋予其机械强度和热塑性能。允许对玻璃中吸收的水分含量进行密切控制的水合方法可以在水和相对短链的溶液中进行，例如高达约5个碳原子，脂族醇或在气体气氛中解决方案 Li +离子或质子与Na +和/或K +离子的离子交换反应可以在高于水合玻璃的转变范围的温度下被促进，并且在低于转变范围的温度下交换Na +和/或Li +离子的K +离子。本发明还考虑处理通过先前水合钠和/或硅酸钾玻璃体而在气态或液态醇或水 - 醇混合物中产生的硅酸钠和/或钾硅酸盐玻璃，以赋予其增强的强度和抗冲击性，并改变其中吸收的水分含量。上述离子交换反应也适用于此。

7. 发明授权

US5770473A Packaging of high power semiconductor lasers 失效
公开(公告)号：US5770473A
公开(公告)日：1998-06-23
申请号：US833548
申请日：1997-04-07
申请人： Douglas W. Hall , Paul A. Jakobson , Julia Alyson Sharps , Roger F. Bartholomew
发明人： Douglas W. Hall , Paul A. Jakobson , Julia Alyson Sharps , Roger F. Bartholomew
IPC分类号： H01L33/48 , H01S5/00 , H01S5/022 , H01L21/00
CPC分类号： H01L33/483 , H01S5/0021 , H01S5/0287 , H01L2924/0002 , H01S5/02204 , H01S5/02224
摘要： A package for a high power semiconductor laser comprising a hermetically sealed container filled with a dry gaseous medium containing oxygen. The presence of oxygen in the laser atmosphere is counter to standard practice in the art which teaches the use of an atmosphere of a dry inert gas. The package also includes a getter for organic impurities, e.g., a getter composed of a porous silica or a zeolite. The hydrogen content of the materials used to form the package are reduced by baking at an elevated temperature for an extended period of time, e.g., at 150.degree. C. for 200 hours.

8. 发明授权

US4099978A High refractive index hydrated glasses 失效
$High refractive index hydrated glasses$
标题翻译：高折射率水合眼镜
公开(公告)号：US4099978A
公开(公告)日：1978-07-11
申请号：US843798
申请日：1977-10-20
申请人： Roger F. Bartholomew , Che-Kuang Wu
发明人： Roger F. Bartholomew , Che-Kuang Wu
IPC分类号： C03C3/102 , C03C4/00 , C03C13/04 , C03C23/00 , C03C3/10 , C03C3/30
CPC分类号： C03C3/102 , C03C23/00 , Y10S501/903
摘要： The present invention is directed to the preparation of hydrated glasses in the Na.sub.2 O-K.sub.2 O-PbO-SiO.sub.2 base composition system containing an amount of BaO and/or Y.sub.2 O.sub.3 and/or ZnO and/or ZrO.sub.2 effective to cause the hydrated glass to be essentially colorless. Such glasses are transparent, exhibit refractive indices higher than 1.60, and which demonstrate intrinsic thermoplastic properties thereby enabling such to be readily molded into optical quality components at relatively low temperatures. The operable glasses in the anhydrous state consist essentially, in mole percent on the oxide basis, of 8-18% Na.sub.2 O, 2-6% K.sub.2 O, 10-23% Na.sub.2 O + K.sub.2 O, >15 but
摘要翻译：本发明涉及在含有一定量的BaO和/或Y 2 O 3和/或ZnO和/或ZrO 2的Na 2 O-K 2 O-PbO-SiO 2基础组合物体系中制备水合玻璃，其有效地使水合玻璃基本上无色。这种玻璃是透明的，具有高于1.60的折射率，并且其表现出内在的热塑性质，因此能够在相对低的温度下容易地模制成光学质量的组分。无水状态的可操作的玻璃基本上以氧化物的摩尔％计含有8-18％的Na2O，2-6％的K2O，10-23％的Na2O + K2O，> 15但是<21％的PbO，55-67 ％SiO 2，PbO:SiO 2的摩尔比在0.225-0.3之间，有效量的BaO和/或Y 2 O 3和/或ZnO和/或ZrO 2直到5％BaO，5％Y 2 O 3，8％ZnO的指定最大值，5％ZrO 2，BaO + Y 2 O 3 + ZnO + ZrO 2不超过10％。

9. 发明授权

US4026692A Press molding optical articles from acid hydrated glasses 失效
标题翻译：从酸性水晶眼镜压制成型光学制品
公开(公告)号：US4026692A
公开(公告)日：1977-05-31
申请号：US640735
申请日：1975-12-15
申请人： Roger F. Bartholomew
发明人： Roger F. Bartholomew
IPC分类号： C03B11/08 , C03B23/03 , C03C3/078 , C03C3/085 , C03C3/102 , C03C3/105 , C03C23/00 , C03C15/00 , C03B9/14
CPC分类号： C03B23/0302 , C03B11/08 , C03C23/00 , C03C3/078 , C03C3/085 , C03C3/102 , C03C3/105 , Y10S501/90
摘要： A glass article having relatively high degrees of surface smoothness, durability, and light transmissivity can be made by forming a glass comprising, in mole percent on an oxide basis, 70-80% SiO.sub.2, 8-18% Na.sub.2 O and/or K.sub.2 O, and 5 to 10% of ZnO and/or PbO; hydrating the glass under acidic conditions to include a water content of up to 12% by weight while reducing the alkali content; reacting the hydrated glass with a HF-containing solution to remove up to 30 weight % of the glass; dehydrating the glass, if necessary, to reduce the total water content to a range of 3 to 7 weight percent; and pressure molding the glass under conditions sufficient to impart an optical quality surface smoothness of a die to the glass surface.
摘要翻译：具有相对高的表面平滑度，耐久性和透光性的玻璃制品可以通过形成以氧化物为基准的摩尔百分数为70-80％的SiO 2，8-18％的Na 2 O和/或K 2 O的玻璃，以及 5〜10％的ZnO和/或PbO; 在酸性条件下水合玻璃以包含最高达12重量％的水含量，同时降低碱含量; 使水合玻璃与含HF溶液反应，以除去多达30重量％的玻璃; 如果需要，将玻璃脱水以将总含水量降低至3至7重量％的范围; 并在足以使模具的光学质量表面平滑度赋予玻璃表面的条件下对玻璃进行加压成型。

10. 发明授权

US5629952A Packaging of high power semiconductor lasers 失效
标题翻译：大功率半导体激光器的封装
公开(公告)号：US5629952A
公开(公告)日：1997-05-13
申请号：US481008
申请日：1995-06-07
申请人： Roger F. Bartholomew , Paul A. Jakobson , Douglas W. Hall , Julia A. Sharps
发明人： Roger F. Bartholomew , Paul A. Jakobson , Douglas W. Hall , Julia A. Sharps
IPC分类号： H01L33/48 , H01S5/00 , H01S5/022 , H01S3/00 , H01L23/36
CPC分类号： H01L33/483 , H01S5/0021 , H01S5/0287 , H01L2924/0002 , H01S5/02204 , H01S5/02224
摘要： A package for a high power semiconductor laser comprising a hermetically sealed container filled with a dry gaseous medium containing oxygen. The presence of oxygen in the laser atmosphere is counter to standard practice in the art which teaches the use of an atmosphere of a dry inert gas. The package also includes a getter for organic impurities, e.g., a getter composed of a porous silica or a zeolite. The hydrogen content of the materials used to form the package are reduced by baking at an elevated temperature for an extended period of time, e.g., at 150.degree. C. for 200 hours.
摘要翻译：一种用于大功率半导体激光器的封装，包括填充有含氧的干燥气态介质的密封容器。在激光气氛中存在氧与本领域的标准做法相反，该方法教导了使用干燥惰性气体的气氛。该包装还包括有机杂质的吸气剂，例如由多孔二氧化硅或沸石组成的吸气剂。用于形成包装的材料的氢含量通过在升高的温度下长时间烘烤（例如在150℃下）减少200小时。

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