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1. 发明申请

US20130046116A1 INTEGRATED COPOLYETHER GLYCOL MANUFACTURING PROCESS 审中-公开
标题翻译：一体化聚乙二醇制造工艺
公开(公告)号：US20130046116A1
公开(公告)日：2013-02-21
申请号：US13514801
申请日：2010-01-12
申请人： Robert B. Osborne , Qun Sun , Yanhui Sun , Gregg M. Sisler , Roy N. Eissmann , Robert D. Orlandi
发明人： Robert B. Osborne , Qun Sun , Yanhui Sun , Gregg M. Sisler , Roy N. Eissmann , Robert D. Orlandi
IPC分类号： C07C41/26 , C07C43/13
CPC分类号： C08G65/20 , C08G65/2678 , C08G65/2684 , C08G65/2696 , C08G65/30
摘要： The present invention relates to an improved, fully-integrated continuous process of enhanced process operability for manufacturing copolyether glycols having enhanced physical properties by polymerization of a reaction mixture comprising tetrahydrofuran and at least one alkylene oxide in the presence of an acid catalyst and at least one compound containing reactive hydrogen atoms. The copolyether glycols manufactured by the present process have enhanced physical properties of increased alkylene oxide incorporation, average molecular weight and polydispersity, as well as reduced crystallinity, color, oligomeric cyclic ether content, and linear oligomer having an average molecular weight of up to about 400 dalton content.
摘要翻译：本发明涉及一种改进的，完全一体化的连续方法，其增强了制备具有增强的物理性能的共聚醚二醇的工艺可操作性，所述共聚醚二醇在酸催化剂存在下通过聚合包含四氢呋喃和至少一种烯化氧的反应混合物和至少一种含有活性氢原子的化合物。通过本方法制备的共聚醚二醇具有增加的烯化氧掺入，平均分子量和多分散性以及降低的结晶度，颜色，低聚环醚含量和平均分子量高达约400的线性低聚物的物理性能达尔顿内容

2. 发明申请

US20130053583A1 DEPOLYMERIZATION OF OLIGOMERIC CYCLIC ETHERS 有权
标题翻译：低分子环化聚合物的分解
公开(公告)号：US20130053583A1
公开(公告)日：2013-02-28
申请号：US13514786
申请日：2009-12-11
申请人： Robert B. Osborne , Paul S. Pearlman , Yanhui Sun
发明人： Robert B. Osborne , Paul S. Pearlman , Yanhui Sun
IPC分类号： C07D307/08
CPC分类号： C07D307/08 , C08G65/20 , C08G65/32 , C08G2650/10 , C08G2650/12 , C08G2650/34
摘要： The present invention provides a method for depolymerization of a mixture comprising oligomeric cyclic ethers resulting from copolymerization of at least one tetrahydrofuran and at least one other cyclic ether to recover tetrahydrofuran monomer.
摘要翻译：本发明提供了包含由至少一种四氢呋喃和至少一种其它环醚的共聚产生的低聚环醚的混合物的解聚方法，以回收四氢呋喃单体。

3. 发明授权

US08809491B2 Depolymerization of oligomeric cyclic ethers 有权
标题翻译：低聚环醚的解聚
公开(公告)号：US08809491B2
公开(公告)日：2014-08-19
申请号：US13514786
申请日：2009-12-11
申请人： Robert B. Osborne , Paul S. Pearlman , Yanhui Sun
发明人： Robert B. Osborne , Paul S. Pearlman , Yanhui Sun
IPC分类号： C08F6/00 , C08G65/20 , C07D307/08 , C08G65/32
CPC分类号： C07D307/08 , C08G65/20 , C08G65/32 , C08G2650/10 , C08G2650/12 , C08G2650/34
摘要： The present invention provides a method for depolymerization of a mixture comprising oligomeric cyclic ethers resulting from copolymerization of at least one tetrahydrofuran and at least one other cyclic ether to recover tetrahydrofuran monomer.
摘要翻译：本发明提供了包含由至少一种四氢呋喃和至少一种其它环醚的共聚产生的低聚环醚的混合物的解聚方法，以回收四氢呋喃单体。

4. 发明授权

US4874884A Promoter synergism in pentenenitrile hydrocyanation 失效
标题翻译：戊烯腈氢氰化促进剂的促进作用
公开(公告)号：US4874884A
公开(公告)日：1989-10-17
申请号：US310411
申请日：1989-02-14
申请人： Ronald J. McKinney , Robert B. Osborne
发明人： Ronald J. McKinney , Robert B. Osborne
IPC分类号： C07C253/10
CPC分类号： C07C253/10
摘要： Process for producing adiponitrile by the zerovalent nickel catalyzed hydrocyanation of pentenenitriles is improved by using a synergistic combination of promoters selected in accordance with the reaction kinetics of the synthesis.
摘要翻译：通过使用根据合成的反应动力学选择的助催化剂的协同组合，通过五价镍催化的氢化氰化腈制备己腈的方法得到改善。

5. 发明授权

US09040754B2 Product recovery process in the filtration of polyether polyols 有权
标题翻译：产品回收过程中过滤聚醚多元醇
公开(公告)号：US09040754B2
公开(公告)日：2015-05-26
申请号：US14233018
申请日：2012-07-17
申请人： Robert B. Osborne , Willard L. Quon
发明人： Robert B. Osborne , Willard L. Quon
IPC分类号： C07C41/34 , C07C41/46 , C08G65/20 , C08G65/30
CPC分类号： C07C41/34 , C07C41/46 , C08G65/20 , C08G65/30
摘要： An improved method for recovering a purified polyether polyol comprising the steps of providing an aqueous solution of a polyether polyol containing an alkali metal catalyst residual formed from a transesterification process, contacting the aqueous solution with a stoichiometric excess of magnesium sulfate to form a second aqueous solution, removing water from said second aqueous solution at a temperature above the melt temperature of said polyether polyol to produce a dehydrated slurry containing a molten polyether polyol phase essentially free of residual alkali metal and a precipitated solid phase comprising sulfate and/or sulfite salts of the alkali metal catalyst, magnesium hydroxide, and excess magnesium sulfate and/or sulfide, passing the dehydrated slurry of through a filtration system comprising a filtration press to separate the molten polyether polyol phase from the precipitated solid phase, wherein the filtration press is treated with a filter aid that is essentially free of transition metal oxide content, separating the molten polyether polyol phase substantially free of water, residual alkali metal catalyst and transition metal contaminants from the precipitated solid phase and recovering polyether polyol from the separated polyether polyol phase.
摘要翻译：一种用于回收纯化的聚醚多元醇的改进方法，包括以下步骤：提供含有由酯交换方法形成的碱金属催化剂残余物的聚醚多元醇水溶液，使该水溶液与化学计量过量的硫酸镁接触以形成第二水溶液在高于所述聚醚多元醇的熔融温度的温度下从所述第二水溶液中除去水，以产生含有基本上不含残余碱金属的熔融聚醚多元醇相的脱水浆料和包含硫酸盐和/或亚硫酸盐的沉淀固相碱金属催化剂，氢氧化镁和过量的硫酸镁和/或硫化物，使脱水的浆料通过包括过滤机的过滤系统，以将熔融的聚醚多元醇相与沉淀的固相分离，其中过滤机用基本上免费的助滤剂o f过渡金属氧化物含量，从沉淀的固相中分离基本上不含水的熔融聚醚多元醇相，残留的碱金属催化剂和过渡金属污染物，并从分离的聚醚多元醇相回收聚醚多元醇。

6. 发明申请

US20140303405A1 PRODUCT RECOVERY PROCESS IN THE FILTRATION OF POLYETHER POLYOLS 有权
标题翻译：聚醚多元醇过滤中的产物回收过程
公开(公告)号：US20140303405A1
公开(公告)日：2014-10-09
申请号：US14233018
申请日：2012-07-17
申请人： Robert B. Osborne , Willard L. Quon
发明人： Robert B. Osborne , Willard L. Quon
IPC分类号： C07C41/34
CPC分类号： C07C41/34 , C07C41/46 , C08G65/20 , C08G65/30
摘要： An improved method for recovering a purified polyether polyol comprising the steps of providing an aqueous solution of a polyether polyol containing an alkali metal catalyst residual formed from a transesterification process, contacting the aqueous solution with a stoichiometric excess of magnesium sulfate to form a second aqueous solution, removing water from said second aqueous solution at a temperature above the melt temperature of said polyether polyol to produce a dehydrated slurry containing a molten polyether polyol phase essentially free of residual alkali metal and a precipitated solid phase comprising sulfate and/or sulfite salts of the alkali metal catalyst, magnesium hydroxide, and excess magnesium sulfate and/or sulfide, passing the dehydrated slurry of through a filtration system comprising a filtration press to separate the molten polyether polyol phase from the precipitated solid phase, wherein the filtration press is treated with a filter aid that is essentially free of transition metal oxide content, separating the molten polyether polyol phase substantially free of water, residual alkali metal catalyst and transition metal contaminants from the precipitated solid phase and recovering polyether polyol from the separated polyether polyol phase.
摘要翻译：一种用于回收纯化的聚醚多元醇的改进方法，包括以下步骤：提供含有由酯交换方法形成的碱金属催化剂残余物的聚醚多元醇水溶液，使该水溶液与化学计量过量的硫酸镁接触以形成第二水溶液在高于所述聚醚多元醇的熔融温度的温度下从所述第二水溶液中除去水，以产生含有基本上不含残余碱金属的熔融聚醚多元醇相的脱水浆料和包含硫酸盐和/或亚硫酸盐的沉淀固相碱金属催化剂，氢氧化镁和过量的硫酸镁和/或硫化物，使脱水的浆料通过包括过滤机的过滤系统，以将熔融的聚醚多元醇相与沉淀的固相分离，其中过滤机用基本上免费的助滤剂o f过渡金属氧化物含量，从沉淀的固相中分离基本上不含水的熔融聚醚多元醇相，残留的碱金属催化剂和过渡金属污染物，并从分离的聚醚多元醇相回收聚醚多元醇。

7. 发明授权

US5284980A Block copolyethers via oxonium coupling of poly(tetramethylene ether) glycols 失效
标题翻译：通过聚（四亚甲基醚）二醇的氧杂偶联来嵌段共聚醚
公开(公告)号：US5284980A
公开(公告)日：1994-02-08
申请号：US965599
申请日：1992-10-26
申请人： Gerfried Pruckmayr , Robert B. Osborne
发明人： Gerfried Pruckmayr , Robert B. Osborne
IPC分类号： C08G18/66 , C08G18/65 , C08G65/20 , C08G65/28 , C08G65/32 , C08G65/331 , C08G65/34 , C07C41/09
CPC分类号： C08G65/34 , C08G65/20 , C08G65/3312
摘要： Treatment of poly(tetramethylene ether) glycols with acid catalysts at elevated temperatures leads to a chain coupling with rapid increase in molecular weight. Various alcohols including diols and triols can be incorporated into poly(tetramethylene ether) glycol backbone with modified properties and performance.
摘要翻译：在高温下用酸催化剂处理聚（四亚甲基醚）二醇导致分子量快速增加的链偶联。包括二醇和三醇的各种醇可以掺入具有改进的性能和性能的聚（四亚甲基醚）乙二醇骨架中。

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