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1. 发明授权

US11465123B2 Systems and methods for gas treatment 有权
公开(公告)号：US11465123B2
公开(公告)日：2022-10-11
申请号：US16749623
申请日：2020-01-22
申请人： BLUE-ZONE TECHNOLOGIES LTD.
发明人： Dusanka Filipovic , Laurence Whitby , Biljana Bicky Milin , Frederick Cashin
IPC分类号： B01D53/02 , B01J20/20 , A61M16/00 , B01D53/70 , B01J20/10 , B01J20/12 , B01J20/16 , B01J20/18 , B01J20/28 , B01J20/34 , C07C41/34 , F16K11/00 , G01N25/18 , G01N27/14 , A61M16/10
摘要： A system and process for the recovery of at least one halogenated hydrocarbon from a gas stream. The recovery includes adsorption by exposing the gas stream to an adsorbent with a lattice structure having pore diameters with an average pore opening of between about 5 and about 50 angstroms. The adsorbent is then regenerated by exposing the adsorbent to a purge gas under conditions which efficiently desorb the at least one adsorbed halogenated hydrocarbon from the adsorbent. The at least one halogenated hydrocarbon (and impurities or reaction products) can be condensed from the purge gas and subjected to fractional distillation to provide a recovered halogenated hydrocarbon.

2. 发明申请

US20200171458A1 SYSTEMS AND METHODS FOR GAS TREATMENT 审中-公开
公开(公告)号：US20200171458A1
公开(公告)日：2020-06-04
申请号：US16749623
申请日：2020-01-22
申请人： BLUE-ZONE TECHNOLOGIES LTD.
发明人： Dusanka FILIPOVIC , Laurence WHITBY , Biljana Bicky MILIN , Frederick CASHIN
IPC分类号： B01J20/20 , G01N27/14 , G01N25/18 , F16K11/00 , C07C41/34 , A61M16/00 , B01J20/34 , B01J20/28 , B01J20/18 , B01J20/16 , B01J20/12 , B01J20/10 , B01D53/70 , B01D53/02
摘要： A system and process for the recovery of at least one halogenated hydrocarbon from a gas stream. The recovery includes adsorption by exposing the gas stream to an adsorbent with a lattice structure having pore diameters with an average pore opening of between about 5 and about 50 angstroms. The adsorbent is then regenerated by exposing the adsorbent to a purge gas under conditions which efficiently desorb the at least one adsorbed halogenated hydrocarbon from the adsorbent. The at least one halogenated hydrocarbon (and impurities or reaction products) can be condensed from the purge gas and subjected to fractional distillation to provide a recovered halogenated hydrocarbon.

3. 发明授权

US09981896B2 Conversion of methane to dimethyl ether 有权
公开(公告)号：US09981896B2
公开(公告)日：2018-05-29
申请号：US15612312
申请日：2017-06-02
申请人： RES USA, LLC
发明人： Harold A. Wright , Mark K. Robertson , Weibin Jiang
IPC分类号： C07C41/09 , C07C41/34 , C01B3/38
CPC分类号： C07C41/09 , C01B3/38 , C01B3/44 , C01B3/505 , C01B2203/0238 , C01B2203/0405 , C01B2203/041 , C01B2203/06 , C01B2203/1058 , C01B2203/1241 , C01B2203/148 , C07C41/01 , C07C41/34 , C07C43/043
摘要： Herein disclosed is a method of producing dimethyl ether (DME) comprising introducing one or more feed streams comprising methane and carbon dioxide into a reformer to generate synthesis gas; and converting synthesis gas to DME in one step. In some cases, the reformer comprises a Ni catalyst. In some cases, the reformer is a pressurized fluidized bed dry reforming reactor. In some cases, the reformer comprises a hydrogen membrane. The hydrogen membrane removes hydrogen contained in the synthesis gas and shifts reforming reactions toward completion.

4. 发明授权

US09873645B2 Method for producing hydrocarbon products 有权
公开(公告)号：US09873645B2
公开(公告)日：2018-01-23
申请号：US14916161
申请日：2014-09-03
申请人： Linde Aktiengesellschaft
发明人： Stefanie Walter , Helmut Fritz , Gunther Schmidt
IPC分类号： C07C4/04 , C10G45/58 , C10G65/04 , C10G69/06 , C10G70/04 , C10G9/36 , C07C5/13 , C07C5/333 , C07C7/148 , C07C5/03 , C07C41/06 , C07C41/34
CPC分类号： C07C4/04 , C07C5/03 , C07C5/13 , C07C5/333 , C07C7/14891 , C07C41/06 , C07C41/34 , C10G9/36 , C10G45/58 , C10G65/04 , C10G69/06 , C10G70/041 , C10G2300/104 , C10G2300/20 , C10G2300/4081 , C07C11/167 , C07C11/08
摘要： The invention relates to a method for producing hydrocarbon products which comprises preparing a hydrocarbon stream (C4) which predominantly comprises branched and unbranched hydrocarbons each having four carbon atoms. A first and a second partial stream (i-C4, n-C4) are obtained from this stream (C4), the first partial stream (i-C4) predominantly comprising branched hydrocarbons with four carbon atoms and the second partial stream (n-C4) predominantly comprising unbranched hydrocarbons with four carbon atoms. The method further comprises the steam cracking of at least part of the first partial stream (i-C4) at a first, higher cracking severity and at least part of the second partial stream (n-C4), at a second, lower, cracking severity.

5. 发明授权

US09856197B2 Systems and methods for manufacture of dimethyl ether (DME) from natural gas and flare gas feedstock 有权
公开(公告)号：US09856197B2
公开(公告)日：2018-01-02
申请号：US15447050
申请日：2017-03-01
申请人： Pioneer Energy Inc.
发明人： Robert M Zubrin , Boris Nizamov , Thomas L Henshaw , Adam M Kortan , James Siebarth , Colin Apke , Mark Berggren
IPC分类号： C07C41/00 , C07C41/01 , C07C41/09 , C07C41/34 , C07C41/40 , C07C41/42 , C01B3/00 , C01B3/02 , C01B3/32 , C01B3/34 , C01B3/36 , C01B3/38
CPC分类号： C07C41/42 , B01J8/02 , B01J2208/025 , C01B3/36 , C01B3/386 , C01B2203/0261 , C01B2203/06 , C01B2203/1241 , C01B2203/1258 , C07C29/1518 , C07C41/09 , C07C41/34 , Y02P20/129 , C07C43/043 , C07C31/04
摘要： Disclosed is a method that reforms flare gas or other raw natural gas source, using air without steam, to directly produce dimethyl ether (DME), a direct diesel substitute. The method first reforms an air-natural gas mixture at ambient atmospheric pressures, and then compresses the resulting CO-hydrogen-nitrogen gas mixture to 100-2,000 psi, and feeds it through a combined reactor which reacts the gas mixture directly into DME. The nitrogen is returned to the atmosphere. DME is an excellent diesel fuel, and can be used to displace significantly costlier and dirtier petroleum-based diesel fuel, while solving a critical problem with flaring or other wasted natural gas. For example, the roughly 120 billion cubic feet per year that was flared in North Dakota in 2014 could be converted into over 3 million tons of DME using the disclosed method.

6. 发明授权

US09758460B2 Process for recovery of pure components from product mixture of one step dimethyl ether synthesis reactor 有权
公开(公告)号：US09758460B2
公开(公告)日：2017-09-12
申请号：US15164743
申请日：2016-05-25
申请人： Council of Scientific & Industrial Research
发明人： Sunil Kumar , Nanoti Shrikant Madhusudan , Garg Madhukar Onkarnath
IPC分类号： C07C41/42 , C07C43/04 , C07C41/34 , C07C41/38 , C07C41/40
CPC分类号： C07C41/42 , C07C41/34 , C07C41/38 , C07C41/40 , C07C43/043
摘要： A process separates pure components from a product mixture produced by a one-step dimethyl ether synthesis reactor. The product mixture is scrubbed with pure dimethyl ether followed by scrubbing with aqueous methanol solvent in two absorption columns to reduce CO2 level and to minimize methanol and dimethyl ether loss with the recovered unconverted synthetic gas. The pure water or aqueous methanol is mixed with the vapor stream of CO2 separation distillation. Dimethyl ether, methanol and water mixture are separated. A scheme for separation of methanol and water mixture minimizes the size, energy and cost of separation. The process can be cost-effective, energy-efficient, environment-friendly and readily-miniaturized.

7. 发明授权

US09643906B2 Systems and methods for manufacture of dimethyl ether (DME) from natural gas and flare gas feedstock 有权
公开(公告)号：US09643906B2
公开(公告)日：2017-05-09
申请号：US14953268
申请日：2015-11-27
申请人： Pioneer Energy Inc.
发明人： Robert M Zubrin , Boris Nizamov , Thomas L Henshaw , Adam M Kortan , James Siebarth , Colin Apke , Mark Berggren
IPC分类号： B01J8/00 , B01J8/02 , C07C41/00 , C07C41/01 , C07C41/09 , C07C41/34 , C07C41/40 , C07C41/42 , C07C43/00 , C07C43/02 , C07C43/03 , C07C43/04 , C01B3/38 , C07C29/151 , C01B3/36 , B01J19/00 , B01J19/24 , C07C29/10 , C07C29/152 , C07C31/04
CPC分类号： C07C41/42 , B01J8/02 , B01J2208/025 , C01B3/36 , C01B3/386 , C01B2203/0261 , C01B2203/06 , C01B2203/1241 , C01B2203/1258 , C07C29/1518 , C07C41/09 , C07C41/34 , Y02P20/129 , C07C43/043 , C07C31/04
摘要： A unique design for a mobile system that reforms flare gas or natural gas, using air without steam, to directly produce dimethyl ether (DME), a diesel substitute, is disclosed. The system first reforms the air-methane mixture at ambient atmospheric pressures, and then compresses the resulting CO-hydrogen-nitrogen gas mixture to up to 600 psi, and feeds it through a combined reactor which reacts the gas mixture directly into dimethyl ether. The nitrogen is returned by the system back to the atmosphere. DME is an excellent diesel fuel, and can be used to displace significantly costlier and dirtier petroleum-based diesel fuel, while solving a critical problem with flaring. For example, the over 120 billion cubic feet per year that is currently flared in North Dakota could be converted into over 3 million tons of DME.

8. 发明授权

US09505690B2 Systems and methods for recovering dimethyl ether from gas mixtures and liquid mixtures 有权
标题翻译：从气体混合物和液体混合物中回收二甲醚的系统和方法
公开(公告)号：US09505690B2
公开(公告)日：2016-11-29
申请号：US14278368
申请日：2014-05-15
申请人： SHELL OIL COMPANY
发明人： Hendrik Adriaan Kooijman
IPC分类号： C07C41/38 , C07C41/34 , B01D53/14 , B01D53/18
CPC分类号： C07C41/34 , B01D53/1487 , B01D53/18 , B01D2252/103 , B01D2256/24 , B01D2257/704 , C10G21/02 , C10G21/06 , C10G21/08 , C07C43/043
摘要： An apparatus includes an airtight shell and an absorption column arranged inside the shell. The absorption column has a multiple stage component, and a single stage component arranged below the multiple stage component with respect to gravity. A gap is arranged between the multiple stage component and the single stage component. The apparatus also includes a gas input in fluid communication with the absorption column for receiving a gas mixture, and a liquid input is in fluid communication with the absorption column for receiving a liquid mixture. A liquid-liquid separator is arranged below the absorption column with respect to gravity. The gas input is arranged below the single stage component. The liquid input is arranged above the single stage component and below the multiple stage component. A method is described for using the apparatus to remove DME from gas and liquid mixtures.
摘要翻译：一种装置包括一个气密的外壳和一个设置在外壳内的吸收塔。吸收塔具有多级部件，以及相对于重力布置在多级部件下方的单级部件。在多级部件和单级部件之间布置间隙。该设备还包括与吸收塔流体连通以接收气体混合物的气体输入，并且液体输入与吸收塔流体连通以接收液体混合物。相对于重力，液 - 液分离器布置在吸收塔的下方。气体输入设置在单级部件下方。液体输入设置在单级部件上方并在多级部件下方。描述了使用该装置从气体和液体混合物中除去DME的方法。

9. 发明授权

US09353039B2 Process for the production of polyether polyols 有权
标题翻译：制备聚醚多元醇的方法
公开(公告)号：US09353039B2
公开(公告)日：2016-05-31
申请号：US14402126
申请日：2013-04-25
申请人： Huntsman International LLC
发明人： Rene Den Heeten , Paul Anton Termorshuizen
IPC分类号： C07C41/44 , C07C41/34 , C08G65/30
CPC分类号： C07C41/44 , C07C41/34 , C08G65/30
摘要： A method to provide polyether polyols comprises the steps of •providing a crude polyether polyol mixture comprising polyether polyol and a base catalyst; •neutralizing said base catalyst; •removing, in a first dehydration step, at least part of the water from the neutralized polyether polyol; •redissolving at least part of the salt crystals obtained by removal of at least part of the water; •removing, in a second dehydration step, at least part of the water from the neutralized polyether polyol mixture, thereby providing salt crystals; •removing the salt crystals from the neutralized polyether polyol, thereby providing the polyether polyol mixture.
摘要翻译：提供聚醚多元醇的方法包括以下步骤：提供包含聚醚多元醇和碱催化剂的粗聚醚多元醇混合物; •中和所述碱催化剂; 在第一脱水步骤中，从中和的聚醚多元醇中除去至少一部分水; •重新溶解至少部分通过除去至少部分水而获得的盐晶体; 在第二脱水步骤中，从中和的聚醚多元醇混合物中除去至少一部分水，由此提供盐晶; •从中和的聚醚多元醇中除去盐晶体，从而提供聚醚多元醇混合物。

10. 发明授权

US09207220B1 Fully automated analytical method for determination of chloroethers in water and urine sample 有权
公开(公告)号：US09207220B1
公开(公告)日：2015-12-08
申请号：US14846564
申请日：2015-09-04
申请人： KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS , King Abdulaziz City for Science and Technology
发明人： Basheer Chanbasha , Mousa Yaser Amayreh
IPC分类号： C07C43/00 , G01N30/72 , C07C41/34 , G01N30/02 , C07C43/13
CPC分类号： G01N30/7206 , C07C41/34 , C07C43/137 , G01N30/08 , G01N30/88 , G01N35/109 , G01N2030/025 , G01N2030/8804
摘要： A fully automated flow assisted-solid-phase microextraction (FA-SPME) is developed for the determination of chloroethers in aqueous samples. A CTC CombiPAL autosampler coupled with gas chromatography-mass spectrometry (GC-MS) is used to automate the extraction process. In this method, the SPME fiber is exposed to a sample in direct immersion. After exposure, the fiber is desorbed at the injection port of GC-MS.

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