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    • 1. 发明授权
    • Dehydroxylation and purification of calcium fluoride materials using a halogen containing plasma
    • 使用含卤素等离子体对氟化钙材料进行脱羟基化和纯化
    • US06982001B2
    • 2006-01-03
    • US10856633
    • 2004-05-28
    • Robert A. BellmanDana C. BookbinderKishor P. GadkareeCynthia B. Giroux
    • Robert A. BellmanDana C. BookbinderKishor P. GadkareeCynthia B. Giroux
    • C30B11/00C30B11/12
    • C01B9/08C01F11/22C30B11/00C30B29/12
    • The invention is directed to a process of purifying metal fluoride materials used to make metal fluoride single crystals suitable for making optical elements used in the transmission of wavelengths below 200 nm, and in particular to a process of purifying such materials by the use of a halogen containing plasma to convert metal oxygenates contaminating the feedstocks used in the preparation of the crystals to metal fluorides. The invention also is directed to a process of growing a metal fluoride single crystal using a crystal growth furnace to carry out the foregoing purification procedure followed by the steps of melting the purified material and cooling it using s selected time and temperature cycle to from a metal fluoride single crystal. The plasmas used in practicing the invention can be derived from a variety of halogenated materials including, for example, fluorocarbons, chlorocarbons, boron trihalides, chlorine, fluorine, xenon difluoride and other gaseous or easily volatilized halogenated substances known in the art.
    • 本发明涉及一种净化金属氟化物材料的方法,所述金属氟化物材料用于制备适于制造用于波长低于200nm的透射体的光学元件的金属氟化物单晶,并且特别涉及一种通过使用卤素 将等离子体转化成金属氧化物,将用于制备晶体的原料污染成金属氟化物。 本发明还涉及使用晶体生长炉生长金属氟化物单晶的方法,以执行上述纯化程序,然后是将精制材料熔化并使用选定的时间和温度循环冷却至金属 氟化物单晶。 用于实施本发明的等离子体可以衍生自各种卤化物质,包括例如碳氟化合物,氯代烃,三卤化硼,氯,氟,氙二氟化物以及本领域已知的其它气态或易挥发的卤化物质。
    • 5. 发明授权
    • Method of making activated carbon composites from supported
crosslinkable resins
    • 由负载的可交联树脂制备活性炭复合材料的方法
    • US5776385A
    • 1998-07-07
    • US806892
    • 1997-02-25
    • Kishor P. GadkareeJoseph F. Mach
    • Kishor P. GadkareeJoseph F. Mach
    • B01J20/20C04B35/83C01B31/00
    • B01J20/20C04B35/83
    • A method for making an activated carbon composite which involves providing a crosslinkable resin and a support material which is wettable by the resin. The support material can be cotton, chopped wood, sisal, non-fugitive material, and combinations of these. The support is contacted with the resin; and the resin and support material are dried. The resin and support material are then shaped, the resin is cured, and the resin and any carbonizable material are carbonized. The carbon is then activated to produce the product composite. An activated carbon composite produced by the above described method in which the carbon is in the form of a continuous structure reinforced by and uniformly distributed throughout non-fugitive support material.
    • 一种制备活性炭复合物的方法,其包括提供可交联树脂和可被树脂润湿的载体材料。 支撑材料可以是棉花,切碎的木材,剑麻,非易失性材料,以及它们的组合。 支撑体与树脂接触; 并干燥树脂和载体材料。 然后树脂和支撑材料成型,树脂固化,并且树脂和任何可碳化的材料被碳化。 然后将碳活化以产生产物复合物。 通过上述方法制备的活性炭复合材料,其中碳是连续结构形式,并且通过非逸散性支撑材料均匀分布并均匀分布。
    • 6. 发明授权
    • System and method for adsorbing contaminants and regenerating the
adsorber
    • 用于吸附污染物和再生吸附剂的系统和方法
    • US5658372A
    • 1997-08-19
    • US500078
    • 1995-07-10
    • Kishor P. Gadkaree
    • Kishor P. Gadkaree
    • B01D53/04
    • B01D53/02B01D2253/102B01D2253/308B01D2253/342B01D2253/3425B01D2257/108B01D2257/504B01D2257/70B01D2257/7022B01D2257/7027B01D2259/40086B01D2259/41Y02C10/08
    • A system for adsorbing a plurality of contaminants from a workstream composed of a first stage open-ended activated carbon monolith adsorber, a second stage open ended activated carbon monolith adsorber downstream of the first stage. The first stage activated carbon has an average pore size that is larger than the average pore size of the second stage activated carbon. A method for removing more than one contaminant from a workstream which involves passing a workstream containing more than one contaminant through a first open ended activated carbon monolith adsorber having a pore size suitable for adsorbing the major portion of the larger size contaminant and for allowing the smaller size contaminant to pass through the monolith, to cause adsorption of the major portion of the larger size contaminant by the activated carbon, while allowing the smaller size contaminant to pass through the first monolith, and thereafter passing the effluent from the first adsorber through a second open ended activated carbon monolith adsorber having a pore size suitable for adsorbing the smaller size contaminant to cause adsorption of the major portion of the smaller size contaminant by the second monolith activated carbon. The adsorbed contaminants can then be desorbed by passing a regenerating stream(s) through the respective monoliths.
    • 一种用于从由第一级开放式活性炭整料吸附器,第二级开放式活性炭整体式吸附器组成的工作流中吸附多种污染物的系统。 第一级活性炭的平均孔径大于第二级活性炭的平均孔径。 一种用于从工作流中除去多于一种污染物的方法,其涉及使含有多于一种污染物的工作流通过具有适于吸附较大尺寸污染物的主要部分的孔径的第一开放式活性炭整料吸附器,并允许较小的 尺寸的污染物通过整料,以引起活性炭对较大尺寸污染物的主要部分的吸附,同时允许较小尺寸的污染物通过第一整料,然后使来自第一吸附器的流出物通过第二 开放式活性炭整体式吸附器具有适于吸附较小尺寸污染物的孔径,以引起较小尺寸污染物主要部分被第二整体活性炭吸附。 然后可以通过将再生流通过相应的整料来解吸吸附的污染物。