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1. 发明授权

US06790425B1 Macroscopic ordered assembly of carbon nanotubes 有权
标题翻译：宏观有序的碳纳米管组装
公开(公告)号：US06790425B1
公开(公告)日：2004-09-14
申请号：US09890030
申请日：2001-07-24
申请人： Richard E. Smalley , Daniel T. Colbert , Ken A. Smith , Deron A. Walters , Michael J. Casavant , Chad B. Huffman , Boris I. Yakobson , Robert H. Hague , Rajesh Kumar Saini , Wan-Ting Chiang
发明人： Richard E. Smalley , Daniel T. Colbert , Ken A. Smith , Deron A. Walters , Michael J. Casavant , Chad B. Huffman , Boris I. Yakobson , Robert H. Hague , Rajesh Kumar Saini , Wan-Ting Chiang
IPC分类号： D01F912
CPC分类号： B82Y40/00 , B82Y10/00 , B82Y30/00 , C01B32/168 , C01B2202/02 , C01B2202/08 , H01J2201/30469 , Y10S977/75 , Y10S977/845 , Y10S977/847 , Y10T156/10
摘要： The present invention is directed to the creation of macroscopic materials and objects comprising aligned nanotube segments. The invention entails aligning single-wall carbon nanotube (SWNT) segments that are suspended in a fluid medium and then removing the aligned segments from suspension in a way that macroscopic, ordered assemblies of SWNT are formed. The invention is further directed to controlling the natural proclivity of nanotube segments to self assemble into ordered structures by modifying the environment of the nanotubes and the history of that environment prior to and during the process. The materials and objects are “macroscopic” in that they are large enough to be seen without the aid of a microscope or of the dimensions of such objects. These macroscopic, ordered SWNT materials and objects have the remarkable physical, electrical, and chemical properties that SWNT exhibit on the microscopic scale because they are comprised nanotubes, each of which is aligned in the same direction and in contact with its nearest neighbors. An ordered assembly of closest SWNT also serves as a template for growth of more and larger ordered assemblies. An ordered assembly further serves as a foundation for post processing treatments that modify the assembly internally to specifically enhance selected material properties such as shear strength, tensile strength, compressive strength, toughness, electrical conductivity, and thermal conductivity.
摘要翻译：本发明涉及包括对准的纳米管段的宏观材料和物体的产生。本发明需要将悬浮在流体介质中的单壁碳纳米管（SWNT）段对准，然后以形成SWNT的宏观有序组件的方式从悬浮液中除去对准的段。本发明进一步涉及通过在过程之前和过程中修改纳米管的环境和该环境的历史来控制纳米管段的自然倾向自我组装成有序结构。材料和物体是“宏观的”，因为它们足够大以便在没有显微镜或这些物体的尺寸的情况下被看到。这些宏观有序的SWNT材料和物体具有显着的物理，电学和化学性质，SWNT在微观尺度上显示，因为它们包含纳米管，每个纳米管沿相同方向排列并与其最近的邻近物接触。最近的SWNT的有序组件也可以作为增加更多和更大订单组件的模板。订购的组件还用作后处理处理的基础，其在内部改变组件以特异性地增强选定的材料性能，例如剪切强度，抗拉强度，抗压强度，韧性，导电性和导热性。

2. 发明申请

US20080210370A1 MACROSCOPIC ORDERED ASSEMBLY OF CARBON NANOTUBES 审中-公开
标题翻译：碳纳米管的大型订购总成
公开(公告)号：US20080210370A1
公开(公告)日：2008-09-04
申请号：US11840033
申请日：2007-08-16
申请人： Richard E. Smalley , Daniel T. Colbert , Ken A. Smith , Deron A. Walters , Michael J. Casavant , Chad B. Huffman , Boris I. Yakobson , Robert H. Hauge , Rajesh Kumar Saini , Wan-Ting Chiang , Xiao Chuan Qin
发明人： Richard E. Smalley , Daniel T. Colbert , Ken A. Smith , Deron A. Walters , Michael J. Casavant , Chad B. Huffman , Boris I. Yakobson , Robert H. Hauge , Rajesh Kumar Saini , Wan-Ting Chiang , Xiao Chuan Qin
IPC分类号： C01B31/02 , B32B37/00 , B05D3/00 , B01J19/00 , B03C1/32
CPC分类号： B82Y40/00 , B82Y10/00 , B82Y30/00 , C01B32/168 , C01B2202/02 , C01B2202/08 , H01J2201/30469 , Y10S977/75 , Y10S977/845 , Y10S977/847 , Y10T156/10
摘要： The present invention is directed to the creation of macroscopic materials and objects comprising aligned nanotube segments. The invention entails aligning single-wall carbon nanotube (SWNT) segments that are suspended in a fluid medium and then removing the aligned segments from suspension in a way that macroscopic, ordered assemblies of SWNT are formed. The invention is further directed to controlling the natural proclivity or nanotube segments to self assemble into or ordered structures by modifying the environment of the nanotubes and the history of that environment prior to and during the process. The materials and objects are “macroscopic” in that they are large enough to be seen without the aid of a microscope or of the dimensions of such objects. These macroscopic ordered SWNT materials and objects have the remarkable physical, electrical, and chemical properties that SWNT exhibit on the microscopic scale because they are comprised of nanotubes, each of which is aligned in the same direction and in contact with its nearest neighbors. An ordered assembly of closest SWNT also serves as a template for growth of more and larger ordered assemblies. An ordered assembly further serves as a foundation for post processing treatments that modify the assembly internally to specifically enhance selected material properties such as shear strength, tensile strength, compressive strength, toughness, electrical conductivity, and thermal conductivity.
摘要翻译：本发明涉及包括对准的纳米管段的宏观材料和物体的产生。本发明需要将悬浮在流体介质中的单壁碳纳米管（SWNT）段对准，然后以形成SWNT的宏观有序组件的方式从悬浮液中除去对准的段。本发明进一步涉及通过在工艺之前和期间修改纳米管的环境和该环境的历史来控制天然倾向或纳米管段自组装成或有序的结构。材料和物体是“宏观的”，因为它们足够大以便在没有显微镜或这些物体的尺寸的情况下被看到。这些宏观有序的SWNT材料和物体具有卓越的物理，电学和化学性质，SWNT在微观尺度上显示，因为它们由纳米管组成，其中每个纳米管沿相同方向对齐并与其最近的邻近物接触。最近的SWNT的有序组件也可以作为增加更多和更大订单组件的模板。订购的组件还用作后处理处理的基础，其在内部改变组件以特异性地增强选定的材料性能，例如剪切强度，抗拉强度，抗压强度，韧性，导电性和导热性。

3. 发明授权

US5581082A Combined scanning probe and scanning energy microscope 失效
标题翻译：组合扫描探头和扫描能量显微镜
公开(公告)号：US5581082A
公开(公告)日：1996-12-03
申请号：US412036
申请日：1995-03-28
申请人： Paul K. Hansma , Deron A. Walters , Paul E. Hillner
发明人： Paul K. Hansma , Deron A. Walters , Paul E. Hillner
IPC分类号： G01N21/64 , G01N21/27 , G01N37/00 , G01Q10/04 , G01Q30/02 , G01Q60/00 , G01Q70/08 , G02B21/00 , H01J37/28 , H01J37/26 , G01B5/28
CPC分类号： G02B21/0028 , B82Y35/00 , G01Q30/025 , B82Y20/00 , Y10S977/869
摘要： A combined scanning probe and scanning energy microscope, in which the same scanning system is used for both the scanning probe and scanning energy images. A sample is translated substantially along a horizontal plane either between or below the probe of a scanning probe microscope and the objective of a scanning energy microscope. The probe collects topographic or other information. The objective focuses a fixed beam of energy to a small spot on the sample, then collects energy from the same spot and transmits it to a detector. A vertical translator connected to the probe or sample support provides the vertical motion necessary to maintain them in close proximity. The images produced by the two microscopes are in substantial direct registration with each other. The invention is exemplified by a combined atomic force and confocal laser scanning microscope with a translated sample.
摘要翻译：组合的扫描探针和扫描能量显微镜，其中扫描探针和扫描能量图像都使用相同的扫描系统。在扫描探针显微镜的探针之间或扫描能量显微镜的目标之下或之下，样本基本上沿水平面平移。探头收集地形或其他信息。目标将固定的能量束聚焦到样品上的一个小点上，然后从相同的点收集能量并将其传输到检测器。连接到探头或样品支架的垂直转换器提供必要的垂直运动，以保持它们靠近。由两个显微镜产生的图像相互直接对准。本发明通过具有翻译样品的组合原子力和共聚焦激光扫描显微镜来举例说明。

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