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1. 发明申请

US20050169830A1 Macroscopic ordered assembly of carbon nanotubes 审中-公开
标题翻译：宏观有序的碳纳米管组装
公开(公告)号：US20050169830A1
公开(公告)日：2005-08-04
申请号：US10759356
申请日：2004-01-16
申请人： Smalley Richard , Daniel Colbert , Kenneth Smith , Deron Walters , Michael Casavant , Chad Huffman , Boris Yakobson , Robert Hauge , Rajesh Saini , Wan-Ting Chiang , Xiao Qin
发明人： Smalley Richard , Daniel Colbert , Kenneth Smith , Deron Walters , Michael Casavant , Chad Huffman , Boris Yakobson , Robert Hauge , Rajesh Saini , Wan-Ting Chiang , Xiao Qin
IPC分类号： C01B31/02 , H01J1/304 , H01J9/02 , D01F9/12 , H05F3/00
CPC分类号： B82Y40/00 , B82Y10/00 , B82Y30/00 , C01B32/168 , C01B2202/02 , C01B2202/08 , H01J2201/30469 , Y10S977/75 , Y10S977/845 , Y10S977/847 , Y10T156/10
摘要： The present invention is directed to the creation of macroscopic materials and objects comprising aligned nanotube segments. The invention entails aligning single-wall carbon nanotube (SWNT) segments that are suspended in a fluid medium and then removing the aligned segments from suspension in a way that macroscopic, ordered assemblies of SWNT are formed. The invention is further directed to controlling the natural proclivity of nanotube segments to self assemble into ordered structures by modifying the environment of the nanotubes and the history of that environment prior to and during the process. The materials and objects are “macroscopic” in that they are large enough to be seen without the aid of a microscope or of the dimensions of such objects. These macroscopic, ordered SWNT materials and objects have the remarkable physical, electrical, and chemical properties that SWNT exhibit on the microscopic scale because they are comprised of nanotubes, each of which is aligned in the same direction and in contact with its nearest neighbors. An ordered assembly of closest SWNT also serves as a template for growth of more and larger ordered assemblies. An ordered assembly further serves as a foundation for post processing treatments that modify the assembly internally to specifically enhance selected material properties such as shear strength, tensile strength, compressive strength, toughness, electrical conductivity, and thermal conductivity.
摘要翻译：本发明涉及包括对准的纳米管段的宏观材料和物体的产生。本发明需要将悬浮在流体介质中的单壁碳纳米管（SWNT）段对准，然后以形成SWNT的宏观有序组件的方式从悬浮液中除去对准的段。本发明进一步涉及通过在过程之前和过程中修改纳米管的环境和该环境的历史来控制纳米管段的自然倾向自我组装成有序结构。材料和物体是“宏观的”，因为它们足够大以便在没有显微镜或这些物体的尺寸的情况下被看到。这些宏观有序的SWNT材料和物体具有显着的物理，电学和化学性质，SWNT在微观尺度上显示，因为它们由纳米管组成，其中每个纳米管沿相同方向排列并与其最近的邻近物接触。最近的SWNT的有序组件也可以作为增加更多和更大订单组件的模板。订购的组件还用作后处理处理的基础，其在内部改变组件以特异性地增强选定的材料性能，例如剪切强度，抗拉强度，抗压强度，韧性，导电性和导热性。

2. 发明申请

US20080210370A1 MACROSCOPIC ORDERED ASSEMBLY OF CARBON NANOTUBES 审中-公开
标题翻译：碳纳米管的大型订购总成
公开(公告)号：US20080210370A1
公开(公告)日：2008-09-04
申请号：US11840033
申请日：2007-08-16
申请人： Richard E. Smalley , Daniel T. Colbert , Ken A. Smith , Deron A. Walters , Michael J. Casavant , Chad B. Huffman , Boris I. Yakobson , Robert H. Hauge , Rajesh Kumar Saini , Wan-Ting Chiang , Xiao Chuan Qin
发明人： Richard E. Smalley , Daniel T. Colbert , Ken A. Smith , Deron A. Walters , Michael J. Casavant , Chad B. Huffman , Boris I. Yakobson , Robert H. Hauge , Rajesh Kumar Saini , Wan-Ting Chiang , Xiao Chuan Qin
IPC分类号： C01B31/02 , B32B37/00 , B05D3/00 , B01J19/00 , B03C1/32
CPC分类号： B82Y40/00 , B82Y10/00 , B82Y30/00 , C01B32/168 , C01B2202/02 , C01B2202/08 , H01J2201/30469 , Y10S977/75 , Y10S977/845 , Y10S977/847 , Y10T156/10
摘要： The present invention is directed to the creation of macroscopic materials and objects comprising aligned nanotube segments. The invention entails aligning single-wall carbon nanotube (SWNT) segments that are suspended in a fluid medium and then removing the aligned segments from suspension in a way that macroscopic, ordered assemblies of SWNT are formed. The invention is further directed to controlling the natural proclivity or nanotube segments to self assemble into or ordered structures by modifying the environment of the nanotubes and the history of that environment prior to and during the process. The materials and objects are “macroscopic” in that they are large enough to be seen without the aid of a microscope or of the dimensions of such objects. These macroscopic ordered SWNT materials and objects have the remarkable physical, electrical, and chemical properties that SWNT exhibit on the microscopic scale because they are comprised of nanotubes, each of which is aligned in the same direction and in contact with its nearest neighbors. An ordered assembly of closest SWNT also serves as a template for growth of more and larger ordered assemblies. An ordered assembly further serves as a foundation for post processing treatments that modify the assembly internally to specifically enhance selected material properties such as shear strength, tensile strength, compressive strength, toughness, electrical conductivity, and thermal conductivity.
摘要翻译：本发明涉及包括对准的纳米管段的宏观材料和物体的产生。本发明需要将悬浮在流体介质中的单壁碳纳米管（SWNT）段对准，然后以形成SWNT的宏观有序组件的方式从悬浮液中除去对准的段。本发明进一步涉及通过在工艺之前和期间修改纳米管的环境和该环境的历史来控制天然倾向或纳米管段自组装成或有序的结构。材料和物体是“宏观的”，因为它们足够大以便在没有显微镜或这些物体的尺寸的情况下被看到。这些宏观有序的SWNT材料和物体具有卓越的物理，电学和化学性质，SWNT在微观尺度上显示，因为它们由纳米管组成，其中每个纳米管沿相同方向对齐并与其最近的邻近物接触。最近的SWNT的有序组件也可以作为增加更多和更大订单组件的模板。订购的组件还用作后处理处理的基础，其在内部改变组件以特异性地增强选定的材料性能，例如剪切强度，抗拉强度，抗压强度，韧性，导电性和导热性。

3. 发明授权

US07090819B2 Gas-phase process for purifying single-wall carbon nanotubes and compositions thereof 有权
公开(公告)号：US07090819B2
公开(公告)日：2006-08-15
申请号：US10071166
申请日：2002-02-08
申请人： Richard E. Smalley , Robert H. Hauge , Wan-Ting Chiang , Yuemei Yang , Kenneth A. Smith , Wilber Carter Kittrell , Zhenning Gu
发明人： Richard E. Smalley , Robert H. Hauge , Wan-Ting Chiang , Yuemei Yang , Kenneth A. Smith , Wilber Carter Kittrell , Zhenning Gu
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/17 , C01B2202/02 , D01F9/1278 , D01F11/121
摘要： The present invention relates to an all gas-phase process for the purification of single-wall carbon nanotubes and the purified single-wall carbon nanotube material. Known methods of single-wall carbon nanotube production result in a single-wall carbon nanotube product that contains single-wall carbon nanotubes in addition to impurities including residual metal catalyst particles and amounts of small amorphous carbon sheets that surround the catalyst particles and appear on the sides of the single-wall carbon nanotubes and “ropes” of single-wall carbon nanotubes. The purification process removes the extraneous carbon as well as metal-containing residual catalyst particles. The process comprises oxidation of the single-wall carbon nanotube material, reduction and reaction of a halogen-containing gas with the metal-containing species. The oxidation step may be done dry or in the presence of water vapor. The present invention provides a scalable means for producing high-purity single-wall carbon nanotube material.

4. 发明授权

US06752977B2 Process for purifying single-wall carbon nanotubes and compositions thereof 有权
标题翻译：单壁碳纳米管纯化方法及其组合物
公开(公告)号：US06752977B2
公开(公告)日：2004-06-22
申请号：US10068907
申请日：2002-02-08
申请人： Richard E. Smalley , Robert H. Hauge , Wan-Ting Chiang
发明人： Richard E. Smalley , Robert H. Hauge , Wan-Ting Chiang
IPC分类号： D01F912
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/17 , C01B2202/02 , D01F9/1278 , D01F11/121 , Y10S977/75 , Y10S977/845
摘要： The present invention relates to a process for the purification of single-wall carbon nanotubes and the purified single-wall carbon nanotube material. Known methods of single-wall carbon nanotube production result in a single-wall carbon nanotube product that contains single-wall carbon nanotubes in addition to impurities including residual metal catalyst particles and amounts of small amorphous carbon sheets that surround the catalyst particles and appear on the sides of the single-wall carbon nanotubes and “ropes” of single-wall carbon nanotubes. The purification process removes the extraneous carbon as well as metal-containing residual catalyst particles. The process employs steps including a gas-phase oxidation of the amorphous carbon and subsequent liquid-phase reaction of a halogen-containing acid with the metal-containing species. Optionally, the single-wall carbon nanotube material may be annealed dry or in the presence of moisture. The present invention provides a scalable means for producing high-purity single-wall carbon nanotube material.
摘要翻译：本发明涉及纯化单壁碳纳米管和纯化的单壁碳纳米管材料的方法。单壁碳纳米管生产的已知方法导致单壁碳纳米管产物，除了包含残留金属催化剂颗粒的杂质和围绕催化剂颗粒的小的无定形碳片的含量之外，还包含单壁碳纳米管，并出现在单壁碳纳米管的侧面和单壁碳纳米管的“绳索”。净化过程除去外来碳以及含金属的残留催化剂颗粒。该方法采用包括无定形碳的气相氧化和随后的含卤素酸与含金属物质的液相反应的步骤。任选地，单壁碳纳米管材料可以是干燥的或在水分存在下退火的。本发明提供了用于生产高纯度单壁碳纳米管材料的可伸缩手段。

5. 发明申请

US20130030266A1 PSYCHOLOGICAL STRESS INDEX MEASURING SYSTEM AND ANALYSIS METHOD 审中-公开
标题翻译：心理压力指标测量系统及分析方法
公开(公告)号：US20130030266A1
公开(公告)日：2013-01-31
申请号：US13193879
申请日：2011-07-29
申请人： Jiann-Shing SHIEH , Maysam F. Abbod , Wan-Ting Chiang , Si-Hui Yang
发明人： Jiann-Shing SHIEH , Maysam F. Abbod , Wan-Ting Chiang , Si-Hui Yang
IPC分类号： A61B5/1455
CPC分类号： A61B5/14551
摘要： A psychological stress index measuring system and its analysis method comprise a pulse generator, a transmission-based photo sensor, a signal converter & amplifier, a filter and a processing platform. At first, the transmission-based photo sensor fixed on a user depends on a light transmitting mechanism to detect analog SpO2 (oxyhemoglobin saturation by pulse oximetry) signals. Then, it will be processed and transformed to digital signals and further exported to the processing platform for extraction of PPGA & HBI. Finally, it will pass a median filter, normalization, and development of Psychological Stress Index which is based on the normalized PPGA & HBI as one convenient method to evaluate psychological health.
摘要翻译：心理应激指数测量系统及其分析方法包括脉冲发生器，基于透射的光电传感器，信号转换器和放大器，滤波器和处理平台。首先，固定在用户上的基于透射的光电传感器取决于透光机构以通过脉搏血氧饱和度信号检测模拟SpO2（氧合血红蛋白饱和度）。然后将其处理并转换为数字信号，并进一步输出到PPGA和HBI的提取处理平台。最后，它将通过基于归一化PPGA和HBI的心理应激指数的中值滤波，归一化和发展，作为评估心理健康的一种方便方法。

6. 发明授权

US06790425B1 Macroscopic ordered assembly of carbon nanotubes 有权
标题翻译：宏观有序的碳纳米管组装
公开(公告)号：US06790425B1
公开(公告)日：2004-09-14
申请号：US09890030
申请日：2001-07-24
申请人： Richard E. Smalley , Daniel T. Colbert , Ken A. Smith , Deron A. Walters , Michael J. Casavant , Chad B. Huffman , Boris I. Yakobson , Robert H. Hague , Rajesh Kumar Saini , Wan-Ting Chiang
发明人： Richard E. Smalley , Daniel T. Colbert , Ken A. Smith , Deron A. Walters , Michael J. Casavant , Chad B. Huffman , Boris I. Yakobson , Robert H. Hague , Rajesh Kumar Saini , Wan-Ting Chiang
IPC分类号： D01F912
CPC分类号： B82Y40/00 , B82Y10/00 , B82Y30/00 , C01B32/168 , C01B2202/02 , C01B2202/08 , H01J2201/30469 , Y10S977/75 , Y10S977/845 , Y10S977/847 , Y10T156/10
摘要： The present invention is directed to the creation of macroscopic materials and objects comprising aligned nanotube segments. The invention entails aligning single-wall carbon nanotube (SWNT) segments that are suspended in a fluid medium and then removing the aligned segments from suspension in a way that macroscopic, ordered assemblies of SWNT are formed. The invention is further directed to controlling the natural proclivity of nanotube segments to self assemble into ordered structures by modifying the environment of the nanotubes and the history of that environment prior to and during the process. The materials and objects are “macroscopic” in that they are large enough to be seen without the aid of a microscope or of the dimensions of such objects. These macroscopic, ordered SWNT materials and objects have the remarkable physical, electrical, and chemical properties that SWNT exhibit on the microscopic scale because they are comprised nanotubes, each of which is aligned in the same direction and in contact with its nearest neighbors. An ordered assembly of closest SWNT also serves as a template for growth of more and larger ordered assemblies. An ordered assembly further serves as a foundation for post processing treatments that modify the assembly internally to specifically enhance selected material properties such as shear strength, tensile strength, compressive strength, toughness, electrical conductivity, and thermal conductivity.
摘要翻译：本发明涉及包括对准的纳米管段的宏观材料和物体的产生。本发明需要将悬浮在流体介质中的单壁碳纳米管（SWNT）段对准，然后以形成SWNT的宏观有序组件的方式从悬浮液中除去对准的段。本发明进一步涉及通过在过程之前和过程中修改纳米管的环境和该环境的历史来控制纳米管段的自然倾向自我组装成有序结构。材料和物体是“宏观的”，因为它们足够大以便在没有显微镜或这些物体的尺寸的情况下被看到。这些宏观有序的SWNT材料和物体具有显着的物理，电学和化学性质，SWNT在微观尺度上显示，因为它们包含纳米管，每个纳米管沿相同方向排列并与其最近的邻近物接触。最近的SWNT的有序组件也可以作为增加更多和更大订单组件的模板。订购的组件还用作后处理处理的基础，其在内部改变组件以特异性地增强选定的材料性能，例如剪切强度，抗拉强度，抗压强度，韧性，导电性和导热性。

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