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1. 发明授权

US07294326B2 Hydrocyanic acid consisting of formamide 有权
标题翻译：氢氰酸由甲酰胺组成
公开(公告)号：US07294326B2
公开(公告)日：2007-11-13
申请号：US10537820
申请日：2003-12-03
申请人： Peter Bassler , Wolfgang Siegel , Guenther Achhammer , Anton Negele , Helmuth Menig , Wilhelm Ruppel , Peter Zehner , Hermann Luyken , Volker Vogt
发明人： Peter Bassler , Wolfgang Siegel , Guenther Achhammer , Anton Negele , Helmuth Menig , Wilhelm Ruppel , Peter Zehner , Hermann Luyken , Volker Vogt
IPC分类号： C01C3/02
CPC分类号： C01C3/0204 , B01J12/007 , B01J15/005 , B01J19/02 , B01J19/2415 , B01J23/866 , B01J2219/00135 , B01J2219/0236
摘要： The present invention relates to a process for preparing hydrocyanic acid (HCN) by catalytic dehydration of gaseous formamide in a reactor which has an internal reactor surface made of a steel comprising iron and chromium and nickel, and also to a reactor for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide, which reactor has an internal reactor surface made of a steel comprising iron and chromium and nickel, and also to the use of the reactor of the present invention in a process for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide.
摘要翻译：本发明涉及一种通过在反应器中催化脱水气态甲酰胺制备氢氰酸（HCN）的方法，该反应器具有由含铁和铬和镍的钢制成的内部反应器表面，并且还涉及通过以下步骤制备氢氰酸的反应器气态甲酰胺的催化脱水，该反应器具有由包含铁和铬和镍的钢制成的内部反应器表面，以及本发明的反应器在通过气态甲酰胺的催化脱水制备氢氰酸的方法中的用途。

2. 发明授权

US07566800B2 Homogeneous isomerization of cis-2-pentene nitrile to form 3-pentene nitrile 失效
标题翻译：顺式-2-戊烯腈的均相异构化形成3-戊烯腈
公开(公告)号：US07566800B2
公开(公告)日：2009-07-28
申请号：US10586481
申请日：2005-01-27
申请人： Jens Scheidel , Christian Miller , Robert Baumann , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Wolfgang Siegel , Peter Bassler
发明人： Jens Scheidel , Christian Miller , Robert Baumann , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Wolfgang Siegel , Peter Bassler
IPC分类号： C07D291/00
CPC分类号： C07C253/30 , Y02P20/127 , C07C255/07
摘要： The invention relates to a method for isomerization of pentene nitrile in an educt flow, wherein isomerization is performed on a homogeneously dissolved catalyst.
摘要翻译：本发明涉及一种在流出物流中异戊烯腈的方法，其中异构化在均匀溶解的催化剂上进行。

3. 发明申请

US20060201798A1 Method for purifying hydrocyanic acid 失效
标题翻译：氢氰酸净化方法
公开(公告)号：US20060201798A1
公开(公告)日：2006-09-14
申请号：US10553537
申请日：2004-04-15
申请人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Miguel Flores , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Wolfgang Siegel , Dagmar Kunsmann-Keitel , Peter Bassler
发明人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Miguel Flores , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Wolfgang Siegel , Dagmar Kunsmann-Keitel , Peter Bassler
IPC分类号： C01C3/04
CPC分类号： C07C253/10 , B01J2219/0011 , C01C3/0295 , C07C255/04
摘要： A process for dewatering hydrocyanic acid by distillation, which comprises distilling crude hydrocyanic acid containing from 50 to 99.9% by weight of HCN, from 0.1 to 40% by weight of water, from 0 to 15% by weight of carbon oxides and optionally from 0.01 to 1% by weight of an involatile stablilizer, at a pressure of from 1 bar to 2.5 bar, a bottom temperature of from 100° C. to 130° C. and a top temperature of from 25° C. to 54° C., in the absence of a volatile stabilizer, in a distillation column to obtain a top draw stream containing purified, anhydrous hydrocyanic acid and carbon oxides and a bottom draw stream comprising water and, where appropriate, the involatile stabilizer.
摘要翻译：一种通过蒸馏使氢氰酸脱水的方法，该方法包括将含有50-99.9重量％HCN的粗制氢氰酸，0.1-40重量％的水，0-15重量％的碳氧化物和任选的0.01 至1重量％的非挥发性固化剂，压力为1巴至2.5巴，底部温度为100℃至130℃，顶部温度为25℃至54℃。在不存在挥发性稳定剂的情况下，在蒸馏塔中获得含有纯化的无水氢氰酸和碳氧化物的顶部牵引流和包含水的底部牵引流，以及适当时的非挥发性稳定剂。

4. 发明授权

US06479680B1 Method for reacting an organic compound with a hydroperoxide 有权
标题翻译：使有机化合物与氢过氧化物反应的方法
公开(公告)号：US06479680B1
公开(公告)日：2002-11-12
申请号：US09762290
申请日：2001-02-07
申请人： Peter Bassler , Wolfgang Harder , Peter Resch , Norbert Rieber , Wilhelm Ruppel , Joaquim Henrique Teles , Andreas Walch , Anne Wenzel , Peter Zehner
发明人： Peter Bassler , Wolfgang Harder , Peter Resch , Norbert Rieber , Wilhelm Ruppel , Joaquim Henrique Teles , Andreas Walch , Anne Wenzel , Peter Zehner
IPC分类号： C07D30112
CPC分类号： C07D301/12 , C07B33/00
摘要： A process for the reaction of an organic compound with a hydroperoxide comprises at least the steps (i) to (iii) below: (i) reaction of the hydroperoxide with the organic compound to give a mixture comprising the reacted organic compound and unreacted hydroperoxide, (ii) separation of the unreacted hydroperoxide from the mixture resulting from step (i), (iii) reaction of the hydroperoxide separated off in step (ii) with the organic compound.
摘要翻译：有机化合物与氢过氧化物反应的方法至少包括以下步骤（i）至（iii）：（i）氢过氧化物与有机化合物的反应，得到包含反应的有机化合物和未反应的氢过氧化物的混合物，（ii）从步骤（i），（iii）中得到的混合物中分离未反应的氢过氧化物，（iii）步骤（ii）中分离出的氢过氧化物与有机化合物的反应。

5. 发明授权

US07935229B2 Extraction of nickel (0) complexes from nitrile mixtures with reduced rag formation 有权
标题翻译：从腈混合物中提取镍（0）配合物，并减少破布形成
公开(公告)号：US07935229B2
公开(公告)日：2011-05-03
申请号：US11577231
申请日：2005-10-12
申请人： Petra Deckert , Peter Bassler , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Peter Pfab , Tobias Aechtner , Wolfgang Siegel
发明人： Petra Deckert , Peter Bassler , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Peter Pfab , Tobias Aechtner , Wolfgang Siegel
IPC分类号： B01D3/34 , B01D11/04 , B01J31/40 , B01J38/56 , C07C253/32
CPC分类号： B01J31/4053 , B01D11/0434 , B01J31/1845 , B01J31/185 , B01J31/24 , B01J31/403 , B01J2231/323 , B01J2531/847 , C07C253/10 , C07C253/32 , Y02P20/584 , C07C255/04
摘要： A process for extractively removing homogeneously dissolved catalysts from a reaction effluent of a hydrocyanation of unsaturated mononitriles to dinitriles with a hydrocarbon H, including performing the steps of a) concentrating the reaction effluent before step b) by distillation at pressures of from 0.1 to 5000 mbar and temperatures of from 10 to 150° C., b) adding a hydrocarbon H to the concentrated reaction effluent to obtain a stream I, and c) feeding stream I, without prior separation of the liquid phases, into an extraction apparatus and extracting it at a temperature T with the hydrocarbon H to obtain a stream II comprising the hydrocarbon H enriched with the catalyst and a stream III having a low catalyst content.
摘要翻译：一种从均匀溶解的催化剂中将不饱和单腈的氢化氰化为碳氢化合物的反应流出物的方法，包括以下步骤：a）在步骤b）之前将反应流出物浓缩至0.1至5000毫巴和10至150℃的温度，b）向浓缩的反应流出物中加入烃H以获得流I，和c）将料流I未经预先分离的液相进入萃取装置并萃取在与烃H的温度T下，获得包含富含催化剂的烃H的流II和具有低催化剂含量的流III。

6. 发明授权

US07462263B2 Method for purifying hydrocyanic acid 失效
标题翻译：氢氰酸净化方法
公开(公告)号：US07462263B2
公开(公告)日：2008-12-09
申请号：US10553537
申请日：2004-04-15
申请人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Miquel Angel Flores , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Wolfgang Siegel , Dagmar Pascale Kunsmann-Keitel , Peter Bassler
发明人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Miquel Angel Flores , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Wolfgang Siegel , Dagmar Pascale Kunsmann-Keitel , Peter Bassler
IPC分类号： B01D3/00 , C01C3/04 , C07C253/34
CPC分类号： C07C253/10 , B01J2219/0011 , C01C3/0295 , C07C255/04
摘要： A process for dewatering hydrocyanic acid by distillation, which includes distilling crude hydrocyanic acid containing from 50 to 99.9% by weight of HCN, from 0.1 to 40% by weight of water, from 0 to 15% by weight of carbon oxides and optionally from 0.01 to 1% by weight of an involatile stabilizer, at a pressure of from 1 bar to 2.5 bar, a bottom temperature of from 100° C. to 130° C. and a top temperature of from 25° C. to 54° C., in the absence of a volatile stabilizer, in a distillation column to obtain a top draw stream containing purified, anhydrous hydrocyanic acid and carbon oxides and a bottom draw stream including water and, optionally, the involatile stabilizer.
摘要翻译：一种通过蒸馏对氢氰酸进行脱水的方法，包括将含有50-99.9重量％HCN的粗制氢氰酸，0.1-40重量％的水，0-15重量％的碳氧化物和任选的0.01 至1重量％的非挥发性稳定剂，压力为1巴至2.5巴，底部温度为100℃至130℃，顶部温度为25℃至54℃。在没有挥发性稳定剂的情况下，在蒸馏塔中获得含有纯化的无水氢氰酸和碳氧化物的顶部牵引流和包含水和任选的非挥发性稳定剂的底部牵引流。

7. 发明申请

US20080281120A1 Method for Producing Linear Pentenenitrile 审中-公开
标题翻译：生产线性戊烯腈的方法
公开(公告)号：US20080281120A1
公开(公告)日：2008-11-13
申请号：US10586470
申请日：2005-01-27
申请人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Tobias Aechtner , Peter Pfab , Petra Deckert , Wolfgang Siegel , Peter Bassler
发明人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Tobias Aechtner , Peter Pfab , Petra Deckert , Wolfgang Siegel , Peter Bassler
IPC分类号： C07C255/00
CPC分类号： C07C253/30 , C07C253/10 , Y02P20/582 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile, characterized by the following process steps: (a) isomerizing a reactant stream which comprises 2-methyl-3-butenenitrile over at least one dissolved or dispersed isomerization catalyst to give a stream 1 which comprises the at least one isomerization catalyst, 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile, (b) distilling stream 1 to obtain a stream 2 as the top product which comprises 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile, and a stream 3 as the bottom product which comprises the at least one isomerization catalyst, (c) distilling stream 2 to obtain a stream 4 as the top product which, compared to stream 2, is enriched in (Z)-2-methyl-2-butenenitrile, based on the sum of all pentenenitriles in stream 2, and a stream 5 as the bottom product which, compared to stream 2, is enriched in 3-pentenenitrile and 2-methyl-3-butenenitrile, based on the sum of all pentenenitriles in stream 2, (d) distilling stream 5 to obtain a stream 6 as the bottom product which comprises 3-pentenenitrile and a stream 7 as the top product which comprises 2-methyl-3-butenenitrile.
摘要翻译：描述了制备3-戊烯腈的方法，其特征在于以下方法步骤：（a）在至少一种溶解或分散的异构化催化剂上异构化包含2-甲基-3-丁烯腈的反应物流，得到流1，其包含至少一种异构化催化剂，2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈，（b）蒸馏物流1，得到作为顶部产物的物流2，其包含2-甲基 -3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈，以及作为底部产物的料流3，其包含至少一种异构化催化剂，（c）蒸馏物流2以获得物流4，与流2相比，基于流2中的所有五烯丙烯的总和和作为底部产物的流5，与流2相比富含（Z）-2-甲基-2-丁烯腈的顶部产物与流2相比较，富含3-戊烯腈和2-甲基-3-丁烯腈，基于所有pentenenit （d）蒸馏流5以获得作为底部产物的料流6，其包含3-戊烯腈和作为顶部产物的料流7，其包含2-甲基-3-丁烯腈。

8. 发明申请

US20080083607A1 Extraction of Nickel (0) Complexes from Nitrile Mixtures with Reduced Rag Formation 有权
标题翻译：从腈混合物中提取镍（0）配合物，减少碎屑形成
公开(公告)号：US20080083607A1
公开(公告)日：2008-04-10
申请号：US11577231
申请日：2005-10-12
申请人： Petra Deckert , Peter Bassler , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Peter Pfab , Tobias Aechtner , Wolfgang Siegel
发明人： Petra Deckert , Peter Bassler , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Peter Pfab , Tobias Aechtner , Wolfgang Siegel
IPC分类号： B01D11/04
CPC分类号： B01J31/4053 , B01D11/0434 , B01J31/1845 , B01J31/185 , B01J31/24 , B01J31/403 , B01J2231/323 , B01J2531/847 , C07C253/10 , C07C253/32 , Y02P20/584 , C07C255/04
摘要： A process for extractively removing homogeneously dissolved catalysts from a reaction effluent of a hydrocyanation of unsaturated mononitriles to dinitriles, by extraction by means of a hydrocarbon H, which comprises a) adding a nonpolar aprotic liquid L to the reaction effluent to obtain a stream I, and b) extracting the stream I at a temperature T with the hydrocarbon H to obtain a stream II comprising the hydrocarbon H enriched with the catalyst and a stream III having a low catalyst content.
摘要翻译：一种通过烃H提取从不饱和单腈的氢化氰化反应流出物向二腈提取均匀溶解的催化剂的方法，该方法包括：a）向反应流出物中加入非极性非质子液体L以获得流I，和b）用烃H提取温度T下的物流I以获得包含富含催化剂的烃H的流II和具有低催化剂含量的流III。

9. 发明申请

US20070155980A1 Homogeneous isomerization of cis-2-pentene nitrile to form 3-pentene nitrile 失效
标题翻译：顺式-2-戊烯腈的均相异构化形成3-戊烯腈
公开(公告)号：US20070155980A1
公开(公告)日：2007-07-05
申请号：US10586481
申请日：2005-01-27
申请人： Jens Scheidel , Christian Miller , Robert Baumann , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Wolfgang Siegel , Peter Bassler
发明人： Jens Scheidel , Christian Miller , Robert Baumann , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Wolfgang Siegel , Peter Bassler
IPC分类号： C07C253/12
CPC分类号： C07C253/30 , Y02P20/127 , C07C255/07
摘要： A process is described for isomerizing pentenenitrile in a reactant stream, wherein the isomerization is effected over a homogeneously dissolved catalyst.
摘要翻译：描述了在反应物流中异构化戊烯腈的方法，其中异构化在均匀溶解的催化剂上进行。

10. 发明授权

US06828457B2 Method for reducing the content of an unsaturated amine in a mixture containing an amine and a nitrile 失效
标题翻译：减少含有胺和腈的混合物中不饱和胺含量的方法
公开(公告)号：US06828457B2
公开(公告)日：2004-12-07
申请号：US10432385
申请日：2003-05-21
申请人： Frank Ohlbach , Christoph Benisch , Hermann Luyken , Andreas Ansmann , Rolf-Hartmuth Fischer , Johann-Peter Melder , Peter Bassler , Stefan Maixner
发明人： Frank Ohlbach , Christoph Benisch , Hermann Luyken , Andreas Ansmann , Rolf-Hartmuth Fischer , Johann-Peter Melder , Peter Bassler , Stefan Maixner
IPC分类号： C07C25334
CPC分类号： C07C209/84 , C07C253/34
摘要： A process is provided for reducing the content of a monounsaturated aliphatic amine (III) in a mixture (IV) containing an aminonitrile (I) or a diamine (II), or mixtures thereof, and the amine (III), wherein a) the mixture (IV) is reacted with an anionic nucleophile (V), which contains a nucleophilic atom selected from the group comprising oxygen, nitrogen and sulfur, which is capable of taking up an H+ ion to form an acid with a pKa ranging from 7 to 11, measured in water at 25° C., and which has a relative nucleophilicity, measured in methyl perchlorate/methanol at 25° C., ranging from 3.4 to 4.7 when oxygen is the nucleophilic atom, ranging from 4.5 to 5.8 when nitrogen is the nucleophilic atom, and ranging from 5.5 to 6.8 when sulfur is the nucleophilic atom, in an amount ranging from 0.01 to 10 mol per mole of amine (III) in the mixture (IV), to give a mixture (VI), and b) the aminonitrile (I) or the diamine (II), or mixtures thereof, are distilled from the mixture (VI) at a temperature ranging from 50 to 170° C. and a pressure ranging from 0.5 to 100 kPa.
摘要翻译：提供了一种降低含有氨基腈（I）或二胺（II）或其混合物的混合物（IV）中的单不饱和脂族胺（III）和胺（III）的含量的方法，其中a）混合物（IV）与阴离子亲核试剂（V）反应，所述阴离子亲核试剂（V）含有选自氧，氮和硫的亲核原子，其能够吸收H +离子以形成pKa范围从 7至11，在25℃的水中测量，并且当氧是亲核原子时，在25℃的甲基高氯酸甲酯/甲醇中测量的范围为3.4至4.7，当氮气为4.5至5.8时，其具有相对的亲核性是亲核原子，当硫是亲核原子时，其摩尔数为5.5至6.8，其量为每摩尔混合物（IV）中的胺（III）为0.01至10摩尔，得到混合物（Ⅵ），和b）氨基腈（I）或二胺（II）或其混合物在温度下从混合物（VI）中蒸馏出 e范围为50至170℃，压力范围为0.5至100kPa。

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