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1. 发明授权

US06586540B1 Method for producing an ethylene copolymer 失效
标题翻译：乙烯共聚物的制造方法
公开(公告)号：US06586540B1
公开(公告)日：2003-07-01
申请号：US09889607
申请日：2001-07-19
申请人： Paulus De Lange , Volker Billert , Bernd Brunner , Werner Ritter , Andreas Deckers
发明人： Paulus De Lange , Volker Billert , Bernd Brunner , Werner Ritter , Andreas Deckers
IPC分类号： C08F21016
CPC分类号： C08F210/16 , C08F2/002 , C08F210/14 , C08F2500/12 , C08F2500/07 , C08F210/08
摘要： The invention relates to a method for the production of copolymer based on ethylene by continuous copolymerization of ethylene and comonomer in a reactor in the presence of a catalyst. In this method, in a first step of the copolymerization, a mixture comprising ethylene and comonomer of such a composition that a copolymer-containing coating deposits in the reactor is metered into the reactor and/or generated in the reactor, and, in a second step, the concentration of the comonomer in the metered-in mixture and/or in the mixture generated in the reactor is reduced sufficiently and/or the concentration of the ethylene in the metered-in mixture and/or in the mixture generated in the reactor is increased sufficiently that the coating is removed from the reactor either partially or completely. The method has the advantage that the production of copolymer does not have to be interrupted during cleaning of the reactor.
摘要翻译：本发明涉及在反应器中在催化剂存在下通过乙烯和共聚单体的连续共聚制备基于乙烯的共聚物的方法。在该方法中，在共聚的第一步骤中，将含有共聚物的涂层沉积在反应器中的组合物的乙烯和共聚单体的混合物计量加入反应器和/或在反应器中产生，并且在第二步中步骤中，在计量混合物中和/或在反应器中产生的混合物中的共聚单体的浓度被充分降低和/或在计量混合物中和/或在反应器中产生的混合物中的乙烯浓度充分增加，使得涂层部分或完全从反应器中除去。该方法的优点在于，在反应器的清洗期间不必中断共聚物的制备。

2. 发明授权

US06608151B1 Method for producing supported chrome catalysts and the use thereof for the polymerization of olefins 有权
标题翻译：负载型铬催化剂的制备方法及其在烯烃聚合中的应用
公开(公告)号：US06608151B1
公开(公告)日：2003-08-19
申请号：US10070341
申请日：2002-02-28
申请人： Paulus de Lange , Guido Funk , Andreas Deckers , Peter Kölle
发明人： Paulus de Lange , Guido Funk , Andreas Deckers , Peter Kölle
IPC分类号： C08F424
CPC分类号： C08F10/02 , B01J23/26 , B01J37/0203 , C08F210/16 , C08F4/24 , C08F4/025 , C08F210/14 , C08F2500/12 , C08F2500/13
摘要： The invention relates to a method for producing supported chromium catalysts for the polymerisation of olefins by loading a xerogel support with chromium by adding to the xerogel support a volume of a 0.025 to 15% by weight solution of a chromium compound or a volume of a solution comprising from 0.025 to 7.8% by weight of Cr which is essentially converted into a chromium(VI) compound on heating in a water-free stream of gas under oxidizing conditions at temperatures in the range from 300 to 1100° C. for a period of from 10 to 1000 minutes in a solvent which comprises a maximum of 20% by weight of water, and subsequently evaporating the solvent, where the volume of the chromium salt solution employed is smaller than the pore volume of the xerogel support.
摘要翻译：本发明涉及通过向干凝胶载体中加入0.025至15重量％的铬化合物或一定体积的溶液的体积来生产用于使烯烃聚合的负载型铬催化剂的方法，包括0.025至7.8重量％的Cr，其在氧化条件下在300至1100℃的温度范围内在无水气体流中加热，基本上转化为铬（VI）化合物一段时间在包含最多20重量％的水的溶剂中10至1000分钟，然后蒸发溶剂，其中所用的铬盐溶液的体积小于干凝胶载体的孔体积。

3. 发明授权

US06645900B2 Optimized method for the production of catalyst supports based on silica gel and chromium catalysts supported on silica gel 有权
标题翻译：基于硅胶和载于硅胶上的铬催化剂生产催化剂载体的优化方法
公开(公告)号：US06645900B2
公开(公告)日：2003-11-11
申请号：US10087012
申请日：2002-02-28
申请人： Paulus de Lange , Guido Funk , Andreas Deckers , Peter Kölle
发明人： Paulus de Lange , Guido Funk , Andreas Deckers , Peter Kölle
IPC分类号： B01J29035
CPC分类号： C08F10/00 , B01J21/08 , B01J37/0072 , B01J37/036 , C08F4/02 , C08F4/24
摘要： The invention relates to a catalyst support and to a method for the production of the catalyst support comprising the following steps: a) production of a silicic acid hydrogel having a solids content of from 10 to 25% by weight (calculated as SiO2) whose particles are substantially spherical, b) extraction of the hydrogel particles with an alcohol until at least 60% of the water present in the hydrogel has been removed, c) drying of the resultant hydrogel until the residual alcohol content is less than 10% by weight (xerogel formation) at temperatures of ≧160° C. at atmospheric pressure using an inert entraining gas, d) setting of the desired particle size of the resultant xerogel, in which the hydrogel particles have a particle size of ≧8 mm before the extraction, and to a catalyst and to a method for the production of the catalyst by loading the catalyst support with a chromium compound. The invention also relates to a method for the production of polyolefins using the catalyst.
摘要翻译：本发明涉及一种催化剂载体和用于生产催化剂载体的方法，包括以下步骤：a）制备固体含量为10至25重量％（以SiO 2计）的硅酸水凝胶，其颗粒基本上是球形的，b）用醇萃取水凝胶颗粒，直到水凝胶中存在的至少60％的水已被除去，c）干燥所得的水凝胶，直到残余的醇含量低于10重量％干燥剂形成），在大气压下使用惰性夹带气体，在大气压力= 160℃的温度下，d）设定所得干燥剂的所需粒度，其中水凝胶颗粒的颗粒尺寸> 萃取和催化剂的制备方法，以及通过用铬化合物负载催化剂载体来生产催化剂的方法。本发明还涉及使用该催化剂生产聚烯烃的方法。

4. 发明授权

US06545093B1 High mixture-quality bi-modal polyethylene blends 失效
标题翻译：高混合质量的双模聚乙烯混合物
公开(公告)号：US06545093B1
公开(公告)日：2003-04-08
申请号：US09806584
申请日：2001-04-02
申请人： Paulus de Lange , Andreas Deckers , Thomas Kessler , Wolfgang Rohde , Thomas Blümel , Martin Lux
发明人： Paulus de Lange , Andreas Deckers , Thomas Kessler , Wolfgang Rohde , Thomas Blümel , Martin Lux
IPC分类号： C08L2304
CPC分类号： C08L23/0815 , C08L23/12 , C08L2205/02 , C08L2314/02 , C08L2666/04
摘要： Bimodal polyethylene blends are made from a high-molecular-weight ethylene copolymer and a low-molecular-weight ethylene homo- or copolymer and have a melt flow rate MFR 190/21.6 of from 6 to 14 g/10 min, a density of from 0.94 to 0.97 g/cm3, an environmental-stress-cracking resistance ESCR>150 h and a value of less than 3 when the quality of blending in the blend is measured to ISO 13949. A process prepares polyethylene blends of this type by melting and homogenization in a mixing apparatus and discharge via a gear pump. The blends are used to produce moldings, in particular hollow articles and pressure pipes.
摘要翻译：双峰聚乙烯共混物由高分子量乙烯共聚物和低分子量乙烯均聚物或共聚物制成，熔体流动速率MFR 190 / 21.6为6至14g / 10min，密度为 0.94〜0.97g / cm 3，环境耐应力开裂性ESCR> 150h，当共混物的共混质量测定为ISO 13949时，其值小于3。一种方法通过熔融和在混合装置中均匀化并通过齿轮泵排出。混合物用于生产模制品，特别是中空制品和压力管。

5. 发明授权

US06699947B1 Method for producing Phillips catalysts for polymerizing olefins with better productivity rates in the particle-form process 失效
标题翻译：用于在颗粒形成方法中以更好的生产率生产用于聚合烯烃的菲利普斯催化剂的方法
公开(公告)号：US06699947B1
公开(公告)日：2004-03-02
申请号：US10070805
申请日：2002-03-11
申请人： Kaspar Evertz , Guido Funk , Paulus de Lange , Peter Kölle , Andreas Deckers
发明人： Kaspar Evertz , Guido Funk , Paulus de Lange , Peter Kölle , Andreas Deckers
IPC分类号： C08F424
CPC分类号： C08F10/02 , B01J23/26 , C08F110/02 , C08F4/24 , C08F2/14 , C08F4/025 , C08F2500/12 , C08F2500/18
摘要： In a process for producing Phillips catalysts in which an oxidic support material is treated in suspension with a chromium salt solution and subsequently, after removing the solvent, calcined in an oxygen-containing atmosphere at above 300° C., the oxidic support material and/or the catalyst after calcination are/is, according to the present invention, comminuted until a mean particle size of
摘要翻译：在制备菲利普斯催化剂的方法中，其中氧化载体材料用铬盐溶液悬浮处理，随后在除去溶剂之后，在含氧气氛中在300℃以上煅烧，氧化载体材料和/ 或根据本发明的煅烧后的催化剂粉碎直至达到<100μm的平均粒度，并且尺寸<50μm的颗粒的比例为至少30％，优选在该范围内从40％到80％。还提供了在通过本发明的方法生产的催化剂存在下，在30至150℃的压力范围内，在环管反应器中制备乙烯的均聚物或共聚物的方法。

6. 发明授权

US06465608B1 Method for drying and degassing polyolefins 失效
标题翻译：干燥和脱气聚烯烃的方法
公开(公告)号：US06465608B1
公开(公告)日：2002-10-15
申请号：US09980566
申请日：2001-11-15
申请人： Michael Witt , Paulus De Lange , Thomas Perner , Andreas Deckers , Kaspar Evertz , Dieter Lilge
发明人： Michael Witt , Paulus De Lange , Thomas Perner , Andreas Deckers , Kaspar Evertz , Dieter Lilge
IPC分类号： C08F600
CPC分类号： C08F6/005 , C08F210/16 , C08F210/14 , C08F2500/12 , C08F2500/13
摘要： The invention relates to a method for drying and degassing polyolefins in which the polymerization product leaving a polymerization reactor is brought into contact with a degassing medium and simultaneously decompressed. The degassing medium employed according to the invention is the monomer to be polymerized, which, in particular, flows through a decompression tank in a circulation process and which is preferably also enriched with ethylene or other low-boiling olefins in an amount in the range from 0 to 100 mol %, based on the total amount of circulating gas. A polymerization in an amount of up to 10%, based on the total polymerization conversion, takes place in accordance with the invention inside the decompression tank.
摘要翻译：本发明涉及一种干燥脱气聚烯烃的方法，其中离开聚合反应器的聚合产物与脱气介质接触并同时减压。根据本发明使用的脱气介质是待聚合的单体，其特别是在循环过程中流过减压槽，并且其优选还富含乙烯或其它低沸点烯烃，其量为 0〜100摩尔％，基于循环气体的总量。根据本发明，在减压槽内进行基于总聚合转化率高达10％的聚合。

7. 发明授权

US09034293B2 Process for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide—direct heating 有权
标题翻译：通过气态甲酰胺直接加热催化脱水制备氢氰酸的方法
公开(公告)号：US09034293B2
公开(公告)日：2015-05-19
申请号：US12935840
申请日：2009-03-30
申请人： Ralf Boehling , Andreas Deckers , Achim Gritsch , Stefan Kotrel
发明人： Ralf Boehling , Andreas Deckers , Achim Gritsch , Stefan Kotrel
IPC分类号： C01C3/02 , B01J19/00 , B01J19/24
CPC分类号： C01C3/0204 , B01J19/0093 , B01J19/249 , B01J2219/00783 , B01J2219/00788 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/2453 , B01J2219/2459 , B01J2219/2465 , B01J2219/2474 , B01J2219/2479 , B01J2219/2481 , B01J2219/2486 , B01J2219/2487 , B01J2219/2497 , C01C3/02
摘要： Process for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide, wherein the dehydration of formamide is coupled with an exothermic reaction by the reactor used in the dehydration comprising two separate fluid paths which are separated by a common reactor wall, with one fluid path being provided for the dehydration of formamide and the second fluid path being provided for the exothermic reaction.
摘要翻译：通过气态甲酰胺的催化脱水制备氢氰酸的方法，其中甲酰胺的脱水通过用于脱水的反应器与放热反应相结合，所述反应器包括由共同反应器壁分离的两个分离的流体路径，其中提供一个流体路径用于甲酰胺的脱水和为放热反应提供的第二流体路径。

8. 发明申请

US20110207634A1 PREPARING ETHER CARBOXYLATES 有权
标题翻译：制备醚类羧酸酯
公开(公告)号：US20110207634A1
公开(公告)日：2011-08-25
申请号：US13030816
申请日：2011-02-18
申请人： Robert Baumann , Markus Christian Biel , Andreas Deckers , Alfred Oftring , Frank Rittig , Wolfgang Staffel
发明人： Robert Baumann , Markus Christian Biel , Andreas Deckers , Alfred Oftring , Frank Rittig , Wolfgang Staffel
IPC分类号： C09K8/60 , C11D1/74 , C07C67/00 , C07C227/02 , C07C69/708 , C07C229/26 , C07C229/24 , C07C231/12 , C07C235/74
CPC分类号： C11D3/3711 , A61K8/86 , A61K2800/10 , A61K2800/80 , A61K2800/805 , A61Q19/00 , C07C51/41 , C07C213/06 , C11D1/74 , C07C59/125
摘要： The present invention relates to a process for preparing ether carboxylates.
摘要翻译：本发明涉及一种制备醚羧酸盐的方法。

9. 再颁专利

USRE40140E1 Polymerization catalyst used for producing polyolefins that have excellent combined properties 有权
标题翻译：用于生产具有优异组合性能的聚烯烃的聚合催化剂
公开(公告)号：USRE40140E1
公开(公告)日：2008-03-04
申请号：US11541519
申请日：2001-05-14
申请人： Shahram Mihan , Martin Lux , Wolfgang Rohde , Andreas Deckers , Peter Kölle , Heinz Vogt
发明人： Shahram Mihan , Martin Lux , Wolfgang Rohde , Andreas Deckers , Peter Kölle , Heinz Vogt
IPC分类号： B01J27/06 , B01J21/08 , B01J35/08 , B01J13/00 , C01B33/12
CPC分类号： C08F10/02 , C08F4/24
摘要： The invention relates to a process for preparing a catalyst for the polymerization of olefins, which comprises: a) preparation of a finely divided silica xerogel, b) loading of the xerogel with chromium from a solution of chromium trioxide or a chromium compound which is converted into chromium trioxide under the conditions of step c), and c) activation of the resulting product at from 400 to 1100° C. in a water-free gas stream comprising oxygen in a concentration of above 10% by volume, wherein a fluoride doping with a fluorinating agent is carried out in step b) or in step c). Furthermore, the invention relates to a catalyst for the polymerization of olefins which is obtainable by the process of the invention and to a process for the polymerization of olefins in which an olefin or an olefin mixture is polymerized in the presence of a catalyst according to the invention.
摘要翻译：本发明涉及一种制备烯烃聚合催化剂的方法，该方法包括：a）制备细碎的二氧化硅干凝胶，b）用铬从三氧化铬溶液或铬化合物的溶液中加载干凝胶，在步骤c）的条件下转化为三氧化铬，和c）在含有浓度高于10体积％的氧的无水气流中，在400至1100℃下活化所得产物，其中氟化物掺杂在步骤b）或步骤c）中进行氟化剂。此外，本发明涉及可通过本发明的方法获得的烯烃聚合催化剂和烯烃聚合方法，其中烯烃或烯烃混合物在催化剂存在下聚合，根据发明。

10. 发明授权

US07094827B2 Thixotropic agents comprising ethylene terpolymer waxes 失效
标题翻译：包含乙烯三元共聚物蜡的触变剂
公开(公告)号：US07094827B2
公开(公告)日：2006-08-22
申请号：US10509652
申请日：2003-04-08
申请人： Andreas Fechtenkötter , Lars Wittkowski , Katrin Zeitz , Michael Ehle , Siegfried Gast , Wolfgang Kasel , Andreas Deckers
发明人： Andreas Fechtenkötter , Lars Wittkowski , Katrin Zeitz , Michael Ehle , Siegfried Gast , Wolfgang Kasel , Andreas Deckers
IPC分类号： B05D7/02
CPC分类号： C09D5/36 , C09D5/04 , C09D123/0869 , C08L2666/28
摘要： The invention relates to a method for producing thixotropic agents containing 0.1–30 wt.-% of at least one ethylene terpolymer wax, 5–7 wt.-% of at least one solvent, which is incompatible with the ethylene terpolymer wax, 5–85 wt.-% of of at least one solvent which is compatible with the ethylene terpolymer wax and with one or more of the first-named solvents.
摘要翻译：本发明涉及一种制备触变剂的方法，该触变剂含有0.1-30重量％的至少一种乙烯三元共聚物蜡，5-7重量％的至少一种与乙烯三元共聚物蜡不相容的溶剂， 85重量％的至少一种与乙烯三元共聚物蜡和一种或多种第一名称溶剂相容的溶剂。

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