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1. 发明授权

US06230614B1 Device for reducing the oxidation of food products 失效
标题翻译：减少食品氧化的装置
公开(公告)号：US06230614B1
公开(公告)日：2001-05-15
申请号：US09692220
申请日：2000-10-20
申请人： Pascal Del Gallo , Gilles Lagrange , Lucie Prost
发明人： Pascal Del Gallo , Gilles Lagrange , Lucie Prost
IPC分类号： A23L334
CPC分类号： B01D53/326 , A23L3/3418 , A23L3/3436 , B01D71/024
摘要： Provided is a device for treating a food product in order to reduce or eliminate the detrimental effects of the presence of oxygen which is in contact with the external surface of the product. The device includes a vat provided with a hood, containing a food product whose free surface is in contact with the atmospheric air, a solid electrolyte membrane, each face of the membrane being connected to an electrode, each electrode being connected to a current generator, a heater for making the electrolyte operate at the desired working temperature, a pump for discharging oxygen extracted, by the solid electrolyte, from the atmospheric air present above the food product, in a pipe, a pump for circulating the atmosphere to be treated, an oxygen analyzer for measuring the oxygen level in the gas atmosphere above the food product, a control unit for modifying the operation of the solid electrolyte as a function of the oxygen level and the gas atmosphere to be treated and the recirculation rate of the atmosphere and, optionally, a cooling unit.
摘要翻译：提供了一种用于处理食品的装置，以便减少或消除与产品的外表面接触的氧的存在的有害影响。该装置包括具有罩的容器，其容纳食品，其自由表面与大气接触;固体电解质膜，膜的每个面与电极连接，每个电极连接到电流发生器，用于使电解液在期望的工作温度下工作的加热器，用于排出由固体电解质从存在于食品上方的大气中排出的氧的泵，管道，用于循环待处理气氛的泵，用于测量食品上方的气体气氛中的氧气含量的氧分析器，用于改变固体电解质作为氧水平和待处理气体气氛以及大气再循环的函数的操作的控制单元，可选地，冷却单元。

2. 发明授权

US06207038B1 Process for preparing a composite electrolyte based on BIMEVOX and the use of said compound in separating oxygen from a gas mixture 失效
标题翻译：基于BIMEVOX制备复合电解质的方法以及所述化合物在从气体混合物中分离氧气中的用途
公开(公告)号：US06207038B1
公开(公告)日：2001-03-27
申请号：US09346308
申请日：1999-07-02
申请人： César Marlu Steil , Jacques Fouletier , Michel Kleitz , Gilles Lagrange , Pascal Del Gallo , Gaëtan Mairesse , Jean-Claude Boivin
发明人： César Marlu Steil , Jacques Fouletier , Michel Kleitz , Gilles Lagrange , Pascal Del Gallo , Gaëtan Mairesse , Jean-Claude Boivin
IPC分类号： C25C110
CPC分类号： C01G31/006 , B01D53/326 , B01D2257/104 , C01B13/0233 , C01B2210/0046 , C01P2002/54 , C01P2004/03 , C01P2006/40 , G01N27/4073
摘要： A process for preparing a solid composite electrolyte comprising at least one compound of the BIMEVOX family is provided. The process comprises at least one step of preparing a mixture of one or more compounds of the BIMEVOX family with one or more chemically inert compounds, at least one step of compacting the mixture obtained, and at least one sintering step during which the temperature reached, over a nonzero time interval, has a value greater than the optimum sintering temperature for the compound of the BIMEVOX family.
摘要翻译：提供了一种制备包含至少一种BIMEVOX族化合物的固体复合电解质的方法。该方法包括至少一个步骤：制备一种或多种BIMEVOX族化合物与一种或多种化学惰性化合物的混合物，至少一个压实所获得混合物的步骤和至少一个烧结步骤，在非零时间间隔内，具有大于BIMEVOX系列化合物的最佳烧结温度的值。

3. 发明授权

US6143162A Process for separating oxygen from a gaseous mixture containing it and device for practicing this process 失效
标题翻译：用于从含有它的气体混合物中分离氧的方法和用于实施该方法的装置
公开(公告)号：US6143162A
公开(公告)日：2000-11-07
申请号：US181090
申请日：1998-10-28
申请人： Jean-Claude Boivin , Pascal Del Gallo , Jacques Fouletier , Michel Kleitz , Philippe Labrune , Gilles Lagrange , Gaetan Mairesse , Guy Nowogrocki , Marlu Cesar Steil
发明人： Jean-Claude Boivin , Pascal Del Gallo , Jacques Fouletier , Michel Kleitz , Philippe Labrune , Gilles Lagrange , Gaetan Mairesse , Guy Nowogrocki , Marlu Cesar Steil
IPC分类号： A23L3/3418 , B01D53/32 , C01B13/02 , C25B9/06 , C25B9/08 , C25C1/10
CPC分类号： B01D53/326 , A23L3/3418 , C01B13/0233 , B01D2257/104 , C01B2210/0046 , C01B2210/0062 , C01B2210/0071 , C01B2210/0075 , C01B2210/0082
摘要： Process for separating oxygen from a gas mixture containing it employs a solid-electrolyte electrochemical cell, where the cell includes a homogeneous structure of one or more BIMEVOX derivatives, with dynamic electrodes created "in situ" that are reversible and self-adaptive, and at least two current collectors.
摘要翻译：用于从含有它的气体混合物中分离氧的方法采用固体电解质电化学电池，其中电池包括一种或多种BIMEVOX衍生物的均匀结构，动态电极“原位”形成为可逆的和自适应的，并且在至少两个集电器。

4. 发明授权

US06524372B1 Silica gel incorporating polyazacycloalkane structural units 有权
标题翻译：掺有多氮杂环烷结构单元的硅胶
公开(公告)号：US06524372B1
公开(公告)日：2003-02-25
申请号：US09600954
申请日：2000-07-25
申请人： Robert Corriu , Catherine Reye , Ahmad Mehdi , Gérard Dubois , Claude Chuit , Franck Denat , Bruno Roux-Fouillet , Roger Guilard , Gilles Lagrange , Stéphane Brandes
发明人： Robert Corriu , Catherine Reye , Ahmad Mehdi , Gérard Dubois , Claude Chuit , Franck Denat , Bruno Roux-Fouillet , Roger Guilard , Gilles Lagrange , Stéphane Brandes
IPC分类号： B01D5302
CPC分类号： C07F7/0896 , B01D53/02 , B01D2253/20 , B01D2253/202 , B01D2256/12 , B01D2257/104 , C01B13/0262 , C01B15/013 , C01B21/0455 , C01B2210/0045 , C01B2210/0046 , C07F7/1804
摘要： A novel compound which can be used in the field of separation and purification of gases is disclosed. The compound can be incorporated into a silica gel incorporating polyazacycloalkane structural units for separating a predetermined gas from a mixture of gases. The mixture of gases is brought into contact with a metallated hybrid gel under conditions which make possible the absorption of the gas to be separated, followed by a phase of desorption of the attached gas, and the recovery of the gas.
摘要翻译：公开了一种可用于气体分离和纯化领域的新型化合物。该化合物可以并入含有用于从气体混合物中分离预定气体的多氮杂环烷结构单元的硅胶中。使气体混合物与金属化混合凝胶接触，使得可能吸收待分离的气体，随后附着气体的解吸相和气体的回收。

5. 发明授权

US5573655A Electrochemical cell and its use in the separation or electrochemical extraction of oxygen 失效
标题翻译：电化学电池及其在氧气分离或电化学提取中的应用
公开(公告)号：US5573655A
公开(公告)日：1996-11-12
申请号：US244030
申请日：1994-07-28
申请人： Gaetan Mairesse , Jean-Claude Boivin , Gilles Lagrange , Panayotis Cocolios
发明人： Gaetan Mairesse , Jean-Claude Boivin , Gilles Lagrange , Panayotis Cocolios
IPC分类号： B01D53/32 , C01B13/02 , C01G31/00 , C25B9/00 , C25B9/08 , C25B11/06 , G01N27/407 , H01M8/12 , C25B1/02
CPC分类号： C01B13/0233 , B01D53/326 , G01N27/4073 , H01M8/1266 , C01B2210/0046 , C01B2210/0051 , C01B2210/0062 , C01B2210/0071 , C01B2210/0075 , C01B2210/0082 , Y02E60/525 , Y02P70/56
摘要： The present invention relates to an electrochemical cell comprising a solid electrolyte which conducts O.sup.2- anions in contact with an anode and a cathode of identical or different composition, the solid electrolyte being comprised of a composition derived from Bi.sub.4 V.sub.2 O.sub.11 of which at least one of the constituent cationic elements is substituted by at least one substituting element such that the gamma phase structural type of Bi.sub.4 V.sub.2 O.sub.11 is maintained as well as the equilibrium of charges, at least one of the anode or of the cathode is a material containing at least one element of substitution of said composition derived from Bi.sub.4 V.sub.2 O.sub.11, that element being in a metallic or cationic state. The invention equally relates to the use of the electrochemical cell with a view towards the separation or extraction of oxygen.
摘要翻译： PCT No.PCT / FR93 / 00871 Sec。 371日期：1994年7月28日 102（e）日期1994年7月28日PCT提交1993年9月13日PCT公布。公开号WO94 / 06544 日期：1994年3月31日本发明涉及一种电化学电池，其包含固体电解质，其导电与阳极和阴极具有相同或不同组成的接触，所述固体电解质由衍生自Bi4V2O11的组合物组成，至少一种构成的阳离子元素被至少一个取代元素取代，使得维持Bi 4 V 2 O 11的γ相结构类型以及电荷的平衡，阳极或阴极中的至少一个是至少含有衍生自Bi4V2O11的所述组合物的一种取代元素是该元素处于金属或阳离子状态。本发明同样涉及电化学电池用于分离或提取氧气的用途。

6. 发明授权

US6144898A Control process and device for treating the surface of a solid substrate 失效
标题翻译：用于处理固体基材表面的控制方法和装置
公开(公告)号：US6144898A
公开(公告)日：2000-11-07
申请号：US882328
申请日：1997-06-25
申请人： Gilles Lagrange , Isabelle Hibon
发明人： Gilles Lagrange , Isabelle Hibon
IPC分类号： B05D3/00 , B29C59/12 , C23C16/50 , G05D13/00
CPC分类号： B29C59/12 , B29C2037/90 , Y10S205/918
摘要： A control device for operation of a system for treating a surface of a solid running substrate by dielectric-barrier electrical discharge in a controlled gaseous atmosphere, comprising (A) a system which includes (i) a treatment device through which a substrate to be treated runs at a speed, (ii) the system is connected to the treatment device for supplying the treatment device with a flow of gas, (iii) the system is connected to the treatment device for supplying the treatment device with electrical power in order to produce the electrical discharge and (iv) the system sucking out the gas, (B) a data processing unit capable of receiving, as input, a datum regarding the speed at which the substrate is running through the treatment device, the data processing unit further comprising an output side connected to the system for controlling the electrical power supply system, in order to regulate the flow of gas delivered by the or each of the gas supply system and/or the electrical power delivered by the electrical power supply system to the device as a function of the speed at which the substrate is running through the treatment device, so as to obtain a surface treatment of the substrate with an equivalent quality whatever the speed at which the substrate is running through the treatment.
摘要翻译：一种控制装置，用于操作在受控气体气氛中通过电介质阻挡放电来处理固体运行衬底的表面的系统，包括（A）系统，其包括（i）待处理衬底的处理装置以一定的速度运行，（ii）系统连接到治疗装置以向处理装置提供气体流，（iii）系统连接到治疗装置，以便为治疗装置供电以产生放电和（iv）系统吸出气体，（B）数据处理单元，其能够接收关于基板运行通过处理装置的速度的数据作为输入，数据处理单元还包括连接到用于控制电力供应系统的系统的输出侧，以便调节由气体供应系统或每个气体供应系统输送的气体的流量和/或电力d 作为基板通过处理装置运行的速度的函数，由电力供应系统供给到装置，以便以基本运行的速度以相同的质量获得基板的表面处理通过治疗。

7. 发明授权

US5582710A Electrochemical cell and its use for the separation and the electrochemical extraction of oxygen 失效
标题翻译：电化学电池及其用于分离和电化学提取的氧气
公开(公告)号：US5582710A
公开(公告)日：1996-12-10
申请号：US244034
申请日：1994-05-16
申请人： Gaetan Mairesse , Jean-Claude Boivin , Gilles Lagrange , Panayotis Cocolios
发明人： Gaetan Mairesse , Jean-Claude Boivin , Gilles Lagrange , Panayotis Cocolios
IPC分类号： B01D53/32 , C01B13/02 , C01G31/00 , C25B9/00 , C25B9/08 , C25B11/06 , G01N27/407 , C25B1/02
CPC分类号： G01N27/4073 , B01D53/326 , C01B13/0233 , C01B2210/0046 , C01B2210/0051 , C01B2210/0062 , C01B2210/0071 , C01B2210/0075 , C01B2210/0082
摘要： The present invention relates to an electrochemical cell comprising a solid electrolyte conductive for O.sup.2- anions in contact with an anode and a cathode of identical or different composition, the electrolyte solid being comprised of a composition derived from Bi.sub.4 V.sub.2 O.sub.11 of which at least one of the cationic constituent elements is substituted by at least one substituting element chosen such that the gamma phase structural type of Bi.sub.4 V.sub.2 O.sub.11 is maintained, as well as the equilibrium of charges, at least one of the anode or the cathode including two parts, a first part being of a mixed electronic and ionic conductive material in contact with the solid electrolyte, the second part being an electronic conductive material superposed on the first part. The invention equally relates to the use of the electrochemical cell with a view towards the separation or the extraction of oxygen.
摘要翻译： PCT No.PCT / FR93 / 00872 Sec。 371日期1994年5月16日 102（e）日期1994年5月16日PCT提交1992年9月13日PCT公布。出版物WO94 / 06545 日期：1994年3月31日本发明涉及一种电化学电池，其包含用于与阳极和阴极相接触或相同或不同组成的阴离子导电的固体电解质，电解质固体由衍生自Bi4V2O11的组合物组成，阳离子组成元素中的至少一个被至少一个选择为使得维持Bi4V2O11的γ相结构类型以及电荷的平衡的取代元素所取代，阳极或阴极中的至少一个包括两个部分，一个第一部分是与固体电解质接触的混合电子和离子导电材料，第二部分是重叠在第一部分上的电子导电材料。本发明同样涉及电化学电池用于分离或提取氧气的用途。

8. 发明授权

US06372903B1 Method for preparing polyazacycloalkanes grafted on silica gel and use of grafted compounds 失效
标题翻译：制备接枝在硅胶上的多氮杂环烷烃和使用接枝化合物的方法
公开(公告)号：US06372903B1
公开(公告)日：2002-04-16
申请号：US09600996
申请日：2000-07-26
申请人： Ahmad Mehdi , Franck Denat , Frédéric Barbette , Roger Guilard , Gilles Lagrange
发明人： Ahmad Mehdi , Franck Denat , Frédéric Barbette , Roger Guilard , Gilles Lagrange
IPC分类号： C07D25502
CPC分类号： B01J20/3263 , B01J20/3204 , B01J20/3219 , B01J20/3259 , B01J45/00 , C07F7/1804
摘要： The invention concerns a method for preparing polyazacycloalkanes immobilised on a silica gel from a polyazacycloalkane of formula (A) in which: R1 and R2 represent a hydrogen atom, an alkyl radical, or a [hetero(aryl)]alkyl radical; W1, W2 and W3 represent a radical of formula (B): —[(CT1T2)n—[N(R3)]p—(CT3T4)m]l— such as defined in the description; R3 represents a hydrogen atom, an alkyl radical or a [hetero(aryl)]alkyl radical, provided that the polyazacycloalkane ring of the compound of formula (A) comprises not more than 30 cyclic carbon atoms, and not more than 6 cyclic nitrogen atoms. The invention is characterised in that: (a) the compound of formula (A) is reacted with a compound of formula (C): Z—R4—Si(X1)(X2)(X3), such as defined in the description to form a compound of formula (D); (b) said compound of formula (D) is condensed on the silanol sites of a silica gel to form the immobilised polyazacycloalkane of formula (E); and (c) some ethanol sites having not reacted are, if required, protected by Z′, a group protecting the hydroxyl function. The invention is useful for separating oxygen from air.
摘要翻译：本发明涉及一种由式（A）的多氮杂环烷固定在硅胶上的多氮杂环烷烃的方法，其中：R1和R2表示氢原子，烷基或[杂（芳基）]烷基; W1，W2和W3表示式（B）的基团： - [（CT1T2）n- [N（R3）] p-（CT3T4）m] -1-如描述中所定义; R 3表示氢原子，烷基或[杂（芳基）]烷基，条件是式（A）化合物的多氮杂环烷烃环包含不多于30个环状碳原子，并且不超过6个环状氮原子。本发明的特征在于：（a）式（A）化合物与式（C）化合物：Z-R 4 -Si（X 1）（X 2）（X 3）形成式（D）的化合物; （b）所述式（D）化合物在硅胶的硅烷醇位上缩合形成式（E）的固定化的多氮杂环烷烃; 和（c）如果需要，一些没有反应的乙醇部位被保护羟基官能团的Z'保护。本发明可用于从空气中分离氧气。

9. 发明授权

US6094606A Control process and device for treating the surface of a solid substrate 失效
标题翻译：用于处理固体基材表面的控制方法和装置
公开(公告)号：US6094606A
公开(公告)日：2000-07-25
申请号：US882334
申请日：1997-06-25
申请人： Gilles Lagrange , Isabelle Hibon
发明人： Gilles Lagrange , Isabelle Hibon
IPC分类号： B05D3/00 , B29C59/12 , G05D13/00
CPC分类号： B29C59/12 , B29C2037/90 , Y10S205/918
摘要： A control device for operation of a system for treating a surface of a solid running substrate by dielectric-barrier electrical discharge in a controlled gaseous atmosphere, comprising (A) a system which includes (i) a treatment device through which a substrate to be treated runs at a speed, (ii) the system is connected to the treatment device for supplying the treatment device with gas, (iii) the system is connected to the device for supplying the treatment device with electrical power in order to produce the electrical discharge and (iv) the system for sucking out the gas (B) a data processing unit designed to receive, as input, a datum regarding the speed at which the substrate is running through the treatment device, the data processing unit being connected, on the output side, to the gas supply system, to the electrical power supply system and to the gas suction system, in order: (a) upon starting the treatment device and when the running speed of the substrate is greater than a predetermined speed, to carry out the following actions: initiate operation of the suction system, initiate operation of the gas supply system, initiate operation of the electrical power supply system, and (b) upon stopping the device and/or when the running speed of the substrate drops to a level below a predetermined speed to carry out the following actions: interrupt operation of the electrical power supply system, interrupt operation of the gas supply system, and interrupt operation of the suction system.
摘要翻译：一种控制装置，用于操作在受控气体气氛中通过电介质阻挡放电来处理固体运行衬底的表面的系统，包括（A）系统，其包括（i）待处理衬底的处理装置以一定的速度运行，（ii）系统连接到用于向处理装置供应气体的处理装置，（iii）系统连接到用于向治疗装置供电以供产生放电的装置，（iv）用于吸出气体的系统（B）数据处理单元，该数据处理单元被设计为接收作为输入的数据处理单元，所述数据处理单元接收与所述基板正在运行的速度相关联的数据处理单元，一侧，供气系统，供电系统和吸气系统，以：（a）启动处理装置时，当基板的运行速度大于ap 确定速度，执行以下动作：启动吸入系统的运行，启动供气系统的运行，启动供电系统的运行，以及（b）停止设备和/或当运行速度基板下降到低于预定速度的水平，以执行以下动作：电力供应系统的中断操作，气体供应系统的中断操作和抽吸系统的中断操作。

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