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1. 发明授权

US5009869A Methods for purification of air 失效
标题翻译：净化空气的方法
公开(公告)号：US5009869A
公开(公告)日：1991-04-23
申请号：US138441
申请日：1987-12-28
申请人： Norman L. Weinberg , John D. Genders , Alfred O. Minklei
发明人： Norman L. Weinberg , John D. Genders , Alfred O. Minklei
IPC分类号： B01D53/32 , B01D53/34 , B01D53/60 , B01D53/72 , B01D53/74 , B01D53/77 , C02F1/467
CPC分类号： B01D53/34 , B01D53/326 , C02F1/4672
摘要： Air contaminated with chemical and biological pollutants is purified by treating chemically and electrochemically in a closed system minimizing the generation of by-products for disposal. Pollutants are treated in a scrubber zone with a scrubber liquid-electrolyte comprising pollutant degrading metal ions or complexed with inert metal ions and degraded either in an electrolyzer zone or in both the scrubber and electrolyzer zones where spent scrubber liquid-electrolyte is regenerated for further cleaning.

2. 发明授权

US5207877A Methods for purification of air 失效
标题翻译：净化空气的方法
公开(公告)号：US5207877A
公开(公告)日：1993-05-04
申请号：US670885
申请日：1991-03-18
申请人： Norman L. Weinberg , John D. Genders , Alfred O. Minklei
发明人： Norman L. Weinberg , John D. Genders , Alfred O. Minklei
IPC分类号： B01D53/32 , B01D53/34 , C02F1/467
CPC分类号： B01D53/34 , B01D53/326 , C02F1/4672
摘要： Air polluted with potentially harmful chemical and biological matter is purified and pollutants degraded to less hazardous substances by a combined chemical and electrochemical process. Scrubber liquid-electrolyte circulated between scrubber and electrolyzer zones containing an electrochemically renewable degradant complexes or oxidizes the pollutants with the aid of an electrochemical cell in the electrolyzer zone which also reactivates the degradant in the scrubber liquid for recycling. Adsorption of insoluble organics is enhanced by stable surfactant additives to the scrubber liquid-electrolyte. Surprisingly, the electrochemical cell performs efficiently without separators or membranes when the non-working cathodes comprise Magneli phase substoichiometric titanium oxides which preferentially generate hydrogen instead of reducing redox couples to their inactive lower valence state.
摘要翻译：被潜在有害的化学和生物物质污染的空气被净化，污染物通过组合的化学和电化学过程降解为较少的有害物质。在洗涤器和电解槽区域之间循环的洗涤液体 - 电解质，其含有电化学上可再生的降解物络合物，或者借助于电解槽区域中的电化学电池来氧化污染物，其还使洗涤器液体中的降解物再次反应以进行再循环。对洗涤液液 - 电解质的稳定的表面活性剂添加剂增强了不溶性有机物的吸附。令人惊奇的是，当非工作阴极包含优先产生氢而不是将氧化还原对降低至其无效低价态的Magneli相亚化学计量钛氧化物时，电化学电池高效地执行而没有隔膜或膜。

3. 发明授权

US4950368A Method for paired electrochemical synthesis with simultaneous production of ethylene glycol 失效
标题翻译：双电化学合成法同时生产乙二醇
公开(公告)号：US4950368A
公开(公告)日：1990-08-21
申请号：US335894
申请日：1989-04-10
申请人： Norman L. Weinberg , John D. Genders , Duane J. Mazur
发明人： Norman L. Weinberg , John D. Genders , Duane J. Mazur
IPC分类号： C07C29/14 , C07C31/20 , C25B3/00 , C25B3/02 , C25B3/04 , C25B3/10
CPC分类号： C25B3/00 , C25B3/105
摘要： Paired electrochemical synthesis reactions in which ethylene glycol is formed at the cathode of a membrane divided cell at high concentrations and current efficiencies, up to 99 percent. Simultaneously, a compatible process is also conducted at the anode of the same electrochemical cell by reacting indirectly generated anode products with organic substrates to form secondary products, such as polybasic acids. The process is especially advantageous in that such secondary products, where appropriate can be further reacted with the ethylene glycol prepared from the catholyte of the same cell to form useful tertiary products, especially polyesters like polyethylene terephthalate. Mole ratios of ethylene glycol and polybasic acid can be controlled through selective use of regeneratable redox reactant.

4. 发明授权

US5106463A High yield methods for electrochemical preparation of cysteine and analogues 失效
标题翻译：用于电化学制备半胱氨酸和类似物的高产率方法
公开(公告)号：US5106463A
公开(公告)日：1992-04-21
申请号：US232000
申请日：1988-08-15
申请人： John D. Genders , Norman L. Weinberg , Duane J. Mazur
发明人： John D. Genders , Norman L. Weinberg , Duane J. Mazur
IPC分类号： C25B3/04
CPC分类号： C25B3/04
摘要： Amino acid free bases are prepared electrochemically without production of intermediate acid salts. Amino acids having reducible disulfide linkages and at least one basic nitrogen group are reduced at a high surface area, noncontaminating cathode to provide a current density of at least 50 mA/cm.sup.2, product yield of at least 90% and an operating current efficiency of at least 90%.
摘要翻译：氨基酸游离碱电化学制备而不生产中间酸盐。具有可还原的二硫键和至少一个碱性氮基团的氨基酸在高表面积下被还原，不污染阴极，以提供至少50mA / cm 2的电流密度，至少90％的产物产率和在至少90％。

5. 发明授权

US4971666A Redox reactions in an electrochemical cell including an electrode comprising Magneli phase titanium oxide 失效
标题翻译：电化学电池中的氧化还原反应，包括包含Magneli相氧化钛的电极
公开(公告)号：US4971666A
公开(公告)日：1990-11-20
申请号：US506807
申请日：1990-04-10
申请人： Norman L. Weinberg , John D. Genders , Robert L. Clarke
发明人： Norman L. Weinberg , John D. Genders , Robert L. Clarke
IPC分类号： C25B1/00
CPC分类号： C25B1/00
摘要： An electrochemical cell including an electrode comprising Magneli phase titanium oxide is disclosed for use with reduction oxidation reactions. The use of the Magneli phase titanium oxide electrode advantageously inhibits certain redox back reactions.
摘要翻译：公开了包含Magneli相氧化钛的电极的电化学电池用于还原氧化反应。使用Magneli相二氧化钛电极有利地抑制某些氧化还原反应。

6. 发明授权

US4936970A Redox reactions in an electrochemical cell including an electrode comprising Magneli phase titanium oxide 失效
标题翻译：电化学电池中的氧化还原反应，包括包含Magneli相氧化钛的电极
公开(公告)号：US4936970A
公开(公告)日：1990-06-26
申请号：US270186
申请日：1988-11-14
申请人： Norman L. Weinberg , John D. Genders , Robert L. Clarke
发明人： Norman L. Weinberg , John D. Genders , Robert L. Clarke
IPC分类号： G01N27/30 , C25B1/00 , C25B11/10
CPC分类号： C25B1/00
摘要： An electrochemical cell including an electrode comprising Magneli phase titanium oxide is disclosed for use with reduction oxidation reactions. The use of the Magneli phase titanium oxide electrode advantageously inhibits certain redox back reactions.

7. 发明授权

US5520793A Methods of producing hydrogen iodide electrochemically 失效
标题翻译：电化学生产碘化碘的方法
公开(公告)号：US5520793A
公开(公告)日：1996-05-28
申请号：US415700
申请日：1995-04-03
申请人： J. David Genders , Norman L. Weinberg , Dan M. Hartsough
发明人： J. David Genders , Norman L. Weinberg , Dan M. Hartsough
IPC分类号： C25B1/24 , C25B1/00
CPC分类号： C25B1/24
摘要： Improved electrochemical processes for producing high purity grades of hydrogen iodide without developing cell fouling iodine solids through oxidation of iodide at the anode back migrating through ion exchange membrane into anolyte compartment. Two and three compartment electrochemical cells have anolyte solutions with chemical agents for oxidizing back migrating iodides to soluble iodine species to avoid build up of iodine solids on key cell components. Other embodiments include processes with undivided electrochemical cells fitted with hydrogen depolarized anodes, optionally operating electrogeneratively producing at least some of its own power requirements while simultaneously producing HI, or processes of making high purity HI with multi-phase aqueous/non-aqueous anolytes for solubilizing iodine solids as they develop in the anolyte compartment.
摘要翻译：改进用于生产高纯度等级的碘化氢的电化学方法，而不会通过在阳极处的碘化物氧化反过来通过离子交换膜迁移到阳极电解液室中来发展细胞污染碘固体。两个和三个隔室电化学电池具有阳极电解液，其具有用于氧化回迁移碘化物到可溶性碘物质的化学试剂，以避免在关键细胞组分上积聚碘固体。其他实施方案包括具有装配有氢去极化阳极的未分离的电化学电池的方法，任选地在电生产下产生其自身功率需求的至少一部分同时产生HI，或用多相水/非水性阳极电解液制备高纯度HI的方法用于溶解碘固体，因为它们在阳极电解液室中形成。

8. 发明授权

US5116592A Fluorinated carbons and uses thereof 失效
标题翻译：氟化碳及其用途
公开(公告)号：US5116592A
公开(公告)日：1992-05-26
申请号：US466073
申请日：1990-01-16
申请人： Norman L. Weinberg
发明人： Norman L. Weinberg
IPC分类号： C01B31/04 , C01B31/00 , C09C1/56 , H01M4/133 , H01M4/58 , H01M4/583 , H01M4/96 , H01M10/052 , H01M10/36
CPC分类号： H01M4/583 , C01B31/005 , H01M4/133 , H01M4/5835 , H01M4/96 , H01M10/052
摘要： Specifically fluorinated carbons have enhanced chemical and/or electrochemical stabilities to corrosion, improved hydrophobicity, lubricating properties, etc., making them especially useful as electrodes in both energy consuming and energy producing electrochemical cells, such as batteries, fuel cells and cells for the electrochemical synthesis of organic and inorganic chemical compounds. The specifically fluorinated carbons may also be employed as lubricants, in fabrication of reactors for generating energy, chemical reaction vessels and as catalyst supports.

9. 发明授权

US06638413B1 Methods and apparatus for electrolysis of water 失效
标题翻译：电解水的方法和装置
公开(公告)号：US06638413B1
公开(公告)日：2003-10-28
申请号：US08334952
申请日：1994-11-07
申请人： Norman L. Weinberg , Klaus Tomantschger , Robert S. Feldstein , J. David Genders , Joseph M. Rait
发明人： Norman L. Weinberg , Klaus Tomantschger , Robert S. Feldstein , J. David Genders , Joseph M. Rait
IPC分类号： C25B102
CPC分类号： C25B1/04 , C25B1/02 , Y02E60/366
摘要： A method and apparatus are provided for electrolyzing water for enhanced production of oxygen, hydrogen and heat by the steps of (i) providing an electrochemical cell comprising an isotopic hydrogen storage cathode, an electrically conductive anode and an ionically conducting electrolyte comprising water, and (ii) impressing a repeating sequence of voltages across the cathode and anode comprised of at least two cell voltage regimes, a first cell voltage regime consisting of a voltage sufficient to enhance cathodic absorption of hydrogen, and a second cell voltage regime consisting of at least one voltage pulse which is at least two times the voltage of the first cell voltage regime for a total duration no greater than 0.10 seconds.
摘要翻译：提供一种用于电解水以提高氧气，氢气和热量产生的方法和装置，其步骤如下：（i）提供包含同位素储氢阴极，导电阳极和包含水的离子导电电解质的电化学电池，和 ii）在包括至少两个电池电压方案的阴极和阳极之间施加电压的重复序列，由足以增强氢的阴极吸收的电压组成的第一电池电压状态，以及由至少一个电压脉冲，其持续时间不超过0.10秒是至少两倍于第一电池电压方式的电压。

10. 发明授权

US5841021A Solid state gas sensor and filter assembly 失效
标题翻译：固态气体传感器和过滤器组件
公开(公告)号：US5841021A
公开(公告)日：1998-11-24
申请号：US523687
申请日：1995-09-05
申请人： Emory S. De Castro , J. David Genders , Norman L. Weinberg
发明人： Emory S. De Castro , J. David Genders , Norman L. Weinberg
IPC分类号： G01N27/416 , G01N27/16 , B32B5/00 , H01L7/00
CPC分类号： G01N27/4162
摘要： An electrochemical gas sensor is provided, the use of which permits quantitative measurement of volatile gas contaminants in an atmosphere being monitored, generally at ambient temperatures below 100.degree. C. The sensor is constructed of a sensor electrode and a reference electrode on a separator in such a manner as to be exposed to the atmosphere which is sensed for gaseous contaminants. In an alternative embodiment, the sensors can be covered with a selective filter which will selectively allow only small molecule toxic gases to pass for sensing by the sensor electrode while excluding larger interfering gas molecules. In another alternative embodiment, a multiple layer electrochemical gas sensor detects the presence of volatile gas contaminants in a sample gas as well as humidity, temperature, and/or pressure of the gas sample.
摘要翻译：提供了一种电化学气体传感器，其使用允许定期测量正在监测的气氛中的挥发性气体污染物，通常在低于100℃的环境温度下。传感器由传感器电极和分离器上的参考电极构成一种暴露于被气体污染物检测到的气氛的方式。在替代实施例中，传感器可以被选择性过滤器覆盖，选择性过滤器将选择性地仅允许小分子有毒气体通过传感器电极进行感测，同时排除较大的干扰气体分子。在另一替代实施例中，多层电化学气体传感器检测样品气体中挥发性气体污染物的存在以及气体样品的湿度，温度和/或压力。

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