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    • 4. 发明授权
    • Atmospheric gas separation method
    • 大气分离法
    • US5396772A
    • 1995-03-14
    • US209851
    • 1994-03-11
    • Kevin McKeigueRamachandran Krishnamurthy
    • Kevin McKeigueRamachandran Krishnamurthy
    • F25J3/02B01D3/16B01J19/32F25J3/04
    • F25J3/044B01J19/32F25J3/04284F25J3/04909B01J2219/326F25J2200/74F25J2290/10F25J2290/12
    • A method of cryogenically separating a mixture of atmospheric gases within a distillation column system having at least one distillation column. In accordance with the method, liquid and gaseous phases of the mixture of atmospheric gases to be separated are countercurrently passed through structured packing. The column is operated with a pressure greater than 2 bars and with a vapor rate of the vapor phase that is less than a critical vapor rate at which the column floods and which varies with the liquid rate of the liquid phase. Minimum and critical vapor rates at which the column floods are set in accordance with experimentally derived data for maximum column utilization in terms of packing volume or column throughput. Additionally, separation performance in terms of HETP increases with the increase in pressure so that a lower than prior art height of structured packing can be used to obtain a particular separation.
    • 在具有至少一个蒸馏塔的蒸馏塔系统内低温分离大气气体混合物的方法。 根据该方法,待分离的大气气体的混合物的液相和气相逆流通过规整填料。 柱子的压力大于2巴,气相的蒸汽速率小于塔溢流时的临界蒸气速率,并随着液相的液体速率而变化。 根据实验导出的数据,根据包装体积或色谱柱通过量来最大色谱柱利用率设置色谱柱泛洪的最小和临界蒸气速率。 此外,HETP方面的分离性能随着压力的增加而增加,因此可以使用低于现有技术的规整填料的高度来获得特定的分离。
    • 10. 发明授权
    • Liquid-vapor contact column
    • 液 - 气接触柱
    • US5486318A
    • 1996-01-23
    • US366350
    • 1994-12-29
    • Kevin McKeigueRamachandran Krishnamurthy
    • Kevin McKeigueRamachandran Krishnamurthy
    • B01D53/18B01D3/16B01D3/26B01J19/32B01F3/04
    • B01D3/141B01J19/32B01J2219/3221B01J2219/32213B01J2219/32227B01J2219/32268Y10S261/72
    • A liquid-vapor contact column comprising a column shell and one or more beds of structured packing located within the column shell. Each bed of structured packing includes a plurality of vertical stacks which are formed of at least two upper and lower levels of structured packing. The structured packing is partitioned to form the vertical stacks. When the structured packing is formed from corrugated sheet material, the vertical stacks can also be spaced from one another with the corrugated sheets making up the structured packing rotated 90.degree. with respect to boarding vertical stacks of structured packing. The partitions or the rotated arrangement of the packing inhibit liquid migration in a transverse, horizontal direction of the column. This promotes constant liquid and vapor flow characteristics through each of the vertical stacks of structured packing to resist widespread liquid channeling throughout the column.
    • 一种液 - 气接触柱,其包括柱壳和位于柱壳内的一个或多个规则填料床。 每个规整填料床均包括由至少两个上层和下层的规整填料形成的多个垂直叠层。 结构化填料被分隔形成垂直堆叠。 当规格填料由波纹板材形成时,垂直堆叠也可以彼此间隔开,使构成规整填料的波纹板相对于结构化填料的堆叠垂直堆叠旋转90°。 填料的隔板或旋转布置禁止液体沿塔的横向水平方向移动。 这通过规则填料的每个垂直堆叠促进恒定的液体和蒸汽流动特性,以抵抗整个塔的广泛的液体通道。