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    • 3. 发明公开
    • APPARATUS FOR REMOVING RESIDUAL MONOMERS
    • US20230295352A1
    • 2023-09-21
    • US18006232
    • 2021-07-16
    • HANWHA SOLUTIONS CORPORATION
    • Dongwook LIMShinbeom LEEJunhye SONGWooyoul AHANHyojin JEONKeedo HAN
    • C08F6/00B01D3/26B01D3/32B01D3/34
    • C08F6/003B01D3/26B01D3/324B01D3/346
    • The present disclosure relates to an apparatus for removing residual monomers and, more specifically, to an apparatus for removing residual monomers, the apparatus being capable of preventing, during the removal of volatile materials by supplying a gas to a flowing distillation material, the formation of dead zones in which the distillation material does not flow or the flow rate thereof decreases. The apparatus for removing residual monomers, of the present disclosure, comprises: a main body capable of supplying a gas to a distillation material accommodated therein; distillation material supply part which is provided at the upper part of the main body and through which the distillation material is injected; a gas inflow part which is provided at the lower part of the main body and through which the gas is injected; a discharge part which is provided at the upper part of the main body, and which discharges volatile materials separated, by means of the gas, from the distillation material; a recovery part, which is provided at the lower part of the main body and recovers the distillation material from which the volatile materials have been removed; a plurality of trays which are provided inside the main body, and each of which has through-holes and a spiral channel; and a downcomer which is provided between the trays, and which is a moving passage through which the distillation material moves downward from the upper part of the main body.
    • 4. 发明公开
    • METHOD FOR CLEANING AQUEOUS WASTEWATER STREAMS LOADED WITH NITROBENZENE
    • US20230234859A1
    • 2023-07-27
    • US17996954
    • 2021-04-24
    • Covestro Deutschland AG
    • Thomas RosinPeter DrindaKlaus Pilarczyk
    • C02F1/00B01D3/34B01D3/38B01D3/42C02F1/10B01D3/26
    • C02F1/008B01D3/346B01D3/38B01D3/42C02F1/10B01D3/26C02F2101/38
    • The present invention relates to a process for purifying a wastewater stream WW1 contaminated with nitrobenzene, comprising (I) stripping of the wastewater stream WW1 with a stripping gas SG1 in a continuously operated stripping column to obtain a wastewater stream WW2 which contains nitrobenzene in a concentration reduced relative to WW1 (cNB,WW2), (II) further purification of the wastewater stream WW2 in a wastewater treatment plant, wherein a target value (cNB,WW2,TARGET) is specified for the concentration of nitrobenzene in the wastewater stream WW2, which is greater than zero but takes into account the requirements of the wastewater treatment plant for the maximum content of nitrobenzene in the wastewater streams supplied thereto, wherein, for at least one combination of specified boundary conditions of (a) nitrobenzene concentration in WW1, (b) the temperature of WW1, and (c) the temperature of SG1, a set of linear mathematical relationships of the type mSG1=x·mWW1 is stored in a database, which linear mathematical relationships define a range of concentrations of nitrobenzene in WW2, wherein the set comprises, in addition to a mathematical relationship (0) which corresponds to the target value cNB,WW2,TARGET, at least a first mathematical relationship (1) for a first value of cNB,WW2, which corresponds to 98% of the target value cNB,WW2,TARGET, and a second linear mathematical relationship (2) for a second value of cNB,WW2, which corresponds to 102% of the target value cNB,WW2,TARGET, and wherein the flow rate of the stripping gas is adapted to the flow rate of the wastewater WW1 such that the flow rate of WW1 is within a range of values (AB) that is generated by the first mathematical relationship (1) and the second mathematical relationship (2) at the respective flow rate of WW1, and controlling the concentration of nitrobenzene in WW2 (cNB,WW2) by adjusting the flow rate of stripping gas SG1 accordingly in the event of a measured actual value of this concentration which is outside a window of >98% to