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1. 发明授权

US07253300B2 Production process for high purity tricyclo-[5.2.1.02,6]decane-2-carboxylic acid ester 有权
标题翻译：高纯度三环[5.2.1.02,6]癸烷-2-羧酸酯的制备方法
公开(公告)号：US07253300B2
公开(公告)日：2007-08-07
申请号：US10942880
申请日：2004-09-17
申请人： Mitsuharu Kitamura , Takashi Kojima , Yoshiharu Ataka , Tomoaki Kubota , Kinji Kato , Kazuyuki Fukuda
发明人： Mitsuharu Kitamura , Takashi Kojima , Yoshiharu Ataka , Tomoaki Kubota , Kinji Kato , Kazuyuki Fukuda
IPC分类号： C07C67/36 , C07C69/74
CPC分类号： C07C67/60 , C07B2200/09 , C07C51/58 , C07C67/14 , C07C2603/68 , C07C61/135 , C07C69/753
摘要： In a process for producing tricyclo[5.2.1.02,6]decane-2-carboxylic acid ester by reacting tricyclo[5.2.1.02,6]deca-3-ene with carbon monoxide and alcohol in the presence of HF, carried out separately are (a) a step in which tricyclo[5.2.1.02,6]deca-3-ene is reacted with carbon monoxide to produce acyl fluoride and (b) a step in which acyl fluoride obtained in the step described above is reacted with alcohol to produce an ester. Also, the reaction conditions at the step (a) described above are selected or a step for carrying out isomerization reaction of tricyclo[5.2.1.02,6]decane-2-carboxylic fluoride obtained at the step (a) is interposed between the step (a) and the step (b). Further, the crude product of tricyclo[5.2.1.02,6]decane-2-carboxylic acid ester thus obtained is subjected to contact treatment with specific glycol in the presence of an acid catalyst and then distilled.
摘要翻译：在三环[5.2.1.0 2,6]癸烷-3-羧酸酯的三辛酸[5.2.1.0 2,6]癸烷-2-羧酸酯的制备方法中，在一种HF存在下与一氧化碳和乙醇一起使用，分别进行（a）将三环[5.2.1.0 2,6]癸-3-烯与一氧化碳反应的步骤产生酰氟和（b）使上述步骤中得到的酰基氟与醇反应生成酯的步骤。此外，选择上述步骤（a）中的反应条件或在步骤（a）中获得的三环[5.2.1.0 2,6]癸烷-2-羧酸氟化物进行异构化反应的步骤（a）介于步骤（a）和步骤（b）之间。此外，将由此获得的三环[5.2.1.0 2,6]癸烷-2-羧酸酯的粗产物在酸催化剂存在下用特定的二醇进行接触处理，然后蒸馏。

2. 发明授权

US09056820B2 Alicyclic alcohol 有权
标题翻译：脂环醇
公开(公告)号：US09056820B2
公开(公告)日：2015-06-16
申请号：US13977274
申请日：2011-12-27
申请人： Mitsuharu Kitamura , Yoshiharu Ataka , Kazuyuki Fukuda
发明人： Mitsuharu Kitamura , Yoshiharu Ataka , Kazuyuki Fukuda
IPC分类号： C07C31/135 , C11B9/00 , C07C29/147 , C07C53/44 , C07C35/08 , C07C29/149 , C07C51/58 , C07C67/14
CPC分类号： C07C35/08 , C07C29/149 , C07C31/1355 , C07C51/58 , C07C67/14 , C07C2601/14 , C11B9/0034 , C07C61/08 , C07C69/75
摘要： Provided is an alicyclic alcohol compound which can be used as a raw material for a compound perfume, and which has excellent floral-green-like aromas which are crisp and fresh; also provided are a manufacturing method for the same, and a perfume composition which contains the alicyclic alcohol compound. An alicyclic alcohol compound having a specified structure represented by chemical formula (1) has excellent floral-green-like aromas which are crisp and fresh; and a method for manufacturing the alicyclic alcohol compound represented by chemical formula (1) by reacting, in the presence of hydrogen fluoride, 1-isopropyl-4-methylcyclohexene and carbon monoxide, reacting the resulting 4-isopropyl-1-methylcyclohexane carboxylic acid fluoride with alcohol, and, after having acquired a cyclohexane carbonyl compound, reducing the cyclohexane carbonyl compound.
摘要翻译：提供可用作复合香料的原料的脂环族醇化合物，其具有优良的鲜绿色的花绿色香气，还提供了其制备方法和含有脂环族醇化合物的香料组合物。由化学式（1）表示的具有特定结构的脂环族醇化合物具有优异的花绿色香气，其清爽新鲜; 以及在氟化氢，1-异丙基-4-甲基环己烯和一氧化碳的存在下使化学式（1）表示的脂环族醇化合物的制造方法，使得到的4-异丙基-1-甲基环己烷羧酸氟化物与醇反应后，在获得环己烷羰基化合物后，还原环己烷羰基化合物。

3. 发明申请

US20130345477A1 NOVEL ALICYCLIC ALCOHOL 有权
标题翻译：新的ALICYCLIC酒精
公开(公告)号：US20130345477A1
公开(公告)日：2013-12-26
申请号：US13977221
申请日：2011-12-27
申请人： Mitsuharu Kitamura , Yoshiharu Ataka , Kazuyuki Fukuda
发明人： Mitsuharu Kitamura , Yoshiharu Ataka , Kazuyuki Fukuda
IPC分类号： C07C31/135 , C07C29/147
CPC分类号： C07C31/1355 , C07C29/147 , C07C29/149 , C07C31/135 , C07C53/44 , C07C2601/14 , C11B9/0034
摘要： Provided is an alicyclic alcohol compound which can be used as a raw material for a compound perfume, and which has excellent floral-green-like aromas which are crisp and fresh; also provided are a manufacturing method for the same, and a perfume composition which contains the alicyclic alcohol compound. An alicyclic alcohol compound having a specified structure represented by chemical formula (1) has excellent floral-green-like aromas which are crisp and fresh; and a method for manufacturing the alicyclic alcohol compound represented by chemical formula (1) by reacting, in the presence of hydrogen fluoride, 4-isopropyl-1-methylcyclohexene and carbon monoxide, isomerising the resulting 4-isopropyl-1-methylcyclohexane carboxylic acid fluoride, thus making 2-methyl-2-(4-methylcyclohexyl)-propionyl fluoride, reacting with alcohol and acquiring a cyclohexane carbonyl compound, and then reducing the cyclohexane carbonyl compound.
摘要翻译：提供可用作复合香料的原料的脂环族醇化合物，其具有优良的鲜绿色的花绿色香气，还提供了其制备方法和含有脂环族醇化合物的香料组合物。由化学式（1）表示的具有特定结构的脂环族醇化合物具有优异的花绿色香气，其清爽新鲜; 以及通过在氟化氢，4-异丙基-1-甲基环己烯和一氧化碳的存在下，使得到的4-异丙基-1-甲基环己烷羧酸氟化物异构化来制造由化学式（1）表示的脂环族醇化合物的方法，由此制备2-甲基-2-（4-甲基环己基） - 丙酰氟，与醇反应并获得环己烷羰基化合物，然后还原环己烷羰基化合物。

4. 发明申请

US20050101799A1 Production process for high purity tricyclo-[5.2.1. 02,6]decane-2-carboxylic acid ester 有权
公开(公告)号：US20050101799A1
公开(公告)日：2005-05-12
申请号：US10942880
申请日：2004-09-17
申请人： Mitsuharu Kitamura , Takashi Kojima , Yoshiharu Ataka , Tomoaki Kubota , Kinji Kato , Kazuyuki Fukuda
发明人： Mitsuharu Kitamura , Takashi Kojima , Yoshiharu Ataka , Tomoaki Kubota , Kinji Kato , Kazuyuki Fukuda
IPC分类号： C07C51/58 , C07C61/135 , C07C67/14 , C07C67/60 , C07C69/74
CPC分类号： C07C67/60 , C07B2200/09 , C07C51/58 , C07C67/14 , C07C2603/68 , C07C61/135 , C07C69/753
摘要： An object of the present invention is to provide a process for producing high purity tricyclo[5.2.1.02,6]decane-2-carboxylic acid ester which has a small content of an unsaturated compound and which has an excellent fragrance and is useful as a perfume or a perfume component. In a process for producing tricyclo[5.2.1.02,6]decane-2-carboxylic acid ester by reacting tricyclo[5.2.1.02,6]deca-3-ene with carbon monoxide and alcohol in the presence of HF, carried out separately are (a) a step in which tricyclo[5.2.1.02,6]deca-3-ene is reacted with carbon monoxide to produce acyl fluoride and (b) a step in which acyl fluoride obtained in the step described above is reacted with alcohol to produce an ester, whereby tricyclo[5.2.1.02,6]decane-2-carboxylic acid ester having a small content of an unsaturated compound can be obtained at a high yield. Also, the reaction conditions at the step (a) described above are selected or a step for carrying out isomerization reaction of tricyclo[5.2.1.02,6] decane-2-carboxylic fluoride obtained at the step (a) is interposed between the step (a) and the step (b), whereby capable of being efficiently produced is tricyclo[5.2.1.02,6]decane-2-carboxylic acid ester having a structural ratio of 1.0 or more in exo-tricyclo[5.2.1.02,6]decane-endo-2-carboxylic acid ester/endo-tricyclo[5.2.1.02,6]decane-exo-2-carboxylic acid ester. Further, the crude product of tricyclo[5.2.1.02,6]decane-2-carboxylic acid ester thus obtained is subjected to contact treatment with specific glycol in the presence of an acid catalyst and then distilled, whereby high purity tricyclo[5.2.1.02,6]decane-2-carboxylic acid ester which is reduced in impurity aldehyde and which is excellent in a fragrance can industrially advantageously be produced.

5. 发明授权

US09029613B2 Alicyclic alcohol 有权
标题翻译：脂环醇
公开(公告)号：US09029613B2
公开(公告)日：2015-05-12
申请号：US13977221
申请日：2011-12-27
申请人： Mitsuharu Kitamura , Yoshiharu Ataka , Kazuyuki Fukuda
发明人： Mitsuharu Kitamura , Yoshiharu Ataka , Kazuyuki Fukuda
IPC分类号： C07C31/135 , C11B9/00 , C07C29/147 , C07C29/149 , C07C53/44
CPC分类号： C07C31/1355 , C07C29/147 , C07C29/149 , C07C31/135 , C07C53/44 , C07C2601/14 , C11B9/0034
摘要： Provided is an alicyclic alcohol compound which can be used as a raw material for a compound perfume, and which has excellent floral-green-like aromas which are crisp and fresh; also provided are a manufacturing method for the same, and a perfume composition which contains the alicyclic alcohol compound. An alicyclic alcohol compound having a specified structure represented by chemical formula (1) has excellent floral-green-like aromas which are crisp and fresh; and a method for manufacturing the alicyclic alcohol compound represented by chemical formula (1) by reacting, in the presence of hydrogen fluoride, 4-isopropyl-1-methylcyclohexene and carbon monoxide, isomerizing the resulting 4-isopropyl-1-methylcyclohexane carboxylic acid fluoride, thus making 2-methyl-2-(4-methylcyclohexyl)-propionyl fluoride, reacting with alcohol and acquiring a cyclohexane carbonyl compound, and then reducing the cyclohexane carbonyl compound.
摘要翻译：提供可用作复合香料的原料的脂环族醇化合物，其具有优良的鲜绿色的花绿色香气，还提供了其制备方法和含有脂环族醇化合物的香料组合物。由化学式（1）表示的具有特定结构的脂环族醇化合物具有优异的花绿色香气，其清爽新鲜; 和通过在氟化氢，4-异丙基-1-甲基环己烯和一氧化碳的存在下，使得到的4-异丙基-1-甲基环己烷羧酸氟化物异构化，由化学式（1）表示的脂环族醇化合物的制造方法，由此制备2-甲基-2-（4-甲基环己基） - 丙酰氟，与醇反应并获得环己烷羰基化合物，然后还原环己烷羰基化合物。

6. 发明申请

US20130338403A1 NOVEL ALICYCLIC ALCOHOL 有权
标题翻译：新的ALICYCLIC酒精
公开(公告)号：US20130338403A1
公开(公告)日：2013-12-19
申请号：US13977274
申请日：2011-12-27
申请人： Mitsuharu Kitamura , Yoshiharu Ataka , Kazuyuki Fukuda
发明人： Mitsuharu Kitamura , Yoshiharu Ataka , Kazuyuki Fukuda
IPC分类号： C07C35/08 , C07C29/149
CPC分类号： C07C35/08 , C07C29/149 , C07C31/1355 , C07C51/58 , C07C67/14 , C07C2601/14 , C11B9/0034 , C07C61/08 , C07C69/75
摘要： Provided is an alicyclic alcohol compound which can be used as a raw material for a compound perfume, and which has excellent floral-green-like aromas which are crisp and fresh; also provided are a manufacturing method for the same, and a perfume composition which contains the alicyclic alcohol compound. An alicyclic alcohol compound having a specified structure represented by chemical formula (1) has excellent floral-green-like aromas which are crisp and fresh; and a method for manufacturing the alicyclic alcohol compound represented by chemical formula (1) by reacting, in the presence of hydrogen fluoride, 1-isopropyl-4-methylcyclohexene and carbon monoxide, reacting the resulting 4-isopropyl-1-methylcyclohexane carboxylic acid fluoride with alcohol, and, after having acquired a cyclohexane carbonyl compound, reducing the cyclohexane carbonyl compound.
摘要翻译：提供可用作复合香料的原料的脂环族醇化合物，其具有优良的鲜绿色的花绿色香气，还提供了其制备方法和含有脂环族醇化合物的香料组合物。由化学式（1）表示的具有特定结构的脂环族醇化合物具有优异的花绿色香气，其清爽新鲜; 以及在氟化氢，1-异丙基-4-甲基环己烯和一氧化碳的存在下使化学式（1）表示的脂环族醇化合物的制造方法，使得到的4-异丙基-1-甲基环己烷羧酸氟化物与醇反应后，在获得环己烷羰基化合物后，还原环己烷羰基化合物。

7. 发明授权

US08247026B2 Optical film and method for producing same 失效
标题翻译：光学膜及其制造方法
公开(公告)号：US08247026B2
公开(公告)日：2012-08-21
申请号：US12293990
申请日：2007-03-19
申请人： Fumiaki Nishino , Katsunori Nishiura , Kazuyuki Fukuda , Toshihiko Takaki , Takehiro Miyashita
发明人： Fumiaki Nishino , Katsunori Nishiura , Kazuyuki Fukuda , Toshihiko Takaki , Takehiro Miyashita
IPC分类号： B05D5/06
CPC分类号： G02B5/0278 , C03C17/008 , C03C2218/113 , G02B5/0242 , Y10T428/24355
摘要： Disclosed is a method for producing an optical film composed of a transparent resin and a metal oxide, which film has high light transmittance and light diffusion property even it is formed thin. Also disclosed is such an optical film. Specifically disclosed is a method for producing an optical film having a total light transmittance of not less than 70% and a haze value of not less than 20%, which comprises a step (A) wherein a metal compound to form a metal oxide through a sol-gel reaction is subjected to a sol-gel reaction in a solvent; a step (B) for providing a solution containing a transparent resin as a solute; a step (C) for mixing the mixture obtained in the step (A) with the solution obtained in the step (B); and a step (D) wherein the mixture obtained in the step (C) is applied or spread over a substrate or container and then heated for evaporating the solvent, thereby forming a film thereon.
摘要翻译：公开了一种由透明树脂和金属氧化物构成的光学膜的制造方法，该膜即使形成得较薄，也具有高透光性和光扩散性。还公开了这种光学膜。具体公开了一种制造光透过率为70％以上且雾度值为20％以上的光学膜的制造方法，其特征在于，包括通过以下方式形成金属氧化物的金属化合物的工序（A）溶胶 - 凝胶反应在溶剂中进行溶胶 - 凝胶反应; 提供含有透明树脂作为溶质的溶液的工序（B）将步骤（A）中获得的混合物与步骤（B）中获得的溶液混合的步骤（C）; 和步骤（D），其中将步骤（C）中获得的混合物施加或铺展在基材或容器上，然后加热以蒸发溶剂，从而在其上形成膜。

8. 发明申请

US20090075859A1 FRAGRANCE COMPOSITION 有权
标题翻译： FRAGRANCE组成
公开(公告)号：US20090075859A1
公开(公告)日：2009-03-19
申请号：US11911751
申请日：2006-06-29
申请人： Naotoshi Toki , Kosaku Ishida , Kazuyuki Fukuda
发明人： Naotoshi Toki , Kosaku Ishida , Kazuyuki Fukuda
IPC分类号： A61K8/34 , A61K8/49 , C07C35/23 , A61Q11/00
CPC分类号： C11D3/50 , A61K8/34 , A61Q13/00 , C07B2200/07 , C07C29/00 , C07C2602/28 , C11B9/0053 , C11B9/0076 , C07C35/36
摘要： A fragrance composition containing 0.0005 to 10% by mass of a decalin alcohol as component (a) represented by formula (1a) and 90 to 99.9995% by mass of one or more polycyclic woody-amber fragrances as component (b) selected from the group consisting of 7-acetyl-1,2,3,4,5,6,7,8-octahydro-1,1,6,7-tetramethylnaphthalene, 1,2,3,4,4a,5,6,7-octahydro-2,5,5-trimethyl-2-naphthalenol, 1,2,3,4,4a,7,8,8a-octahydro-2,4a,5,8a-tetramethyl-1-naphthyl formate, 3a-ethyldodecahydro-6,6,9a-trimethylnaphtho[2,1-b]furan, and racemic or optically active dodecahydro-3a,6,6,9a-tetramethylnaphtho[2,1-b]furan; and a cosmetic product, a household product and an environmental/sanitary product containing the fragrance composition. The fragrance composition of the present invention is a highly versatile fragrance composition that brings about an odor of natural ambergris and can attain effects to enhance warmth and an odor quality even in a small amount.
摘要翻译：作为组分（b）的含有0.0005至10质量％的作为组分（a）的十氢化萘作为组分（1a）和90至99.9995质量％的一种或多种多环琥珀香料的香料组合物，选自组由7-乙酰基-1,2,3,4,5,6,7,8-八氢-1,1,6,7-四甲基萘，1,2,3,4,4a，5,6,7- 八氢-2,5,5-三甲基-2-萘酚，1,2,3,4,4a，7,8,8a-八氢-2,4a，5,8a-四甲基-1-萘基甲酸酯，3a-乙基十二氢 -6,6,9a-三甲基萘并[2,1-b]呋喃，和外消旋或光学活性十二氢-3a,6,6,9a-四甲基萘并[2,1-b]呋喃; 和化妆品，家用产品和含有香料组合物的环保/卫生产品。本发明的香料组合物是高度通用的香料组合物，其具有天然琥珀酸的气味，并且即使少量也可获得增强温度和气味质量的效果。

9. 发明授权

US07491833B2 Valerolactone compounds and perfume composition 有权
标题翻译：缬草内酯化合物和香料组合物
公开(公告)号：US07491833B2
公开(公告)日：2009-02-17
申请号：US10529290
申请日：2003-09-26
申请人： Sakuya Tanaka , Kazuyuki Fukuda , Takahiro Asada
发明人： Sakuya Tanaka , Kazuyuki Fukuda , Takahiro Asada
IPC分类号： C07D309/00 , A61Q13/00
CPC分类号： C07D315/00 , A23L27/2052 , C07D263/58 , C07D309/30 , C11B9/008
摘要： A valerolactone compound represented by the formula (I): wherein each of R1 and R2 is independently a hydrogen atom, a methyl group or an ethyl group wherein when R1 is a hydrogen atom, R2 is not a hydrogen atom; and wherein when R2 is a hydrogen atom, R1 is not a hydrogen atom, R3 is a hydrogen atom or a methyl group, and R4 is a propyl group, a 1-propenyl group or a phenyl group; a valerolactone compound represented by the formula (II): a process for preparing the same; and a perfume composition comprising the above-mentioned valerolactone compound.
摘要翻译：由式（I）表示的戊内酯化合物：其中R 1和R 2各自独立地为氢原子，甲基或乙基，其中当R 1为氢原子时，R 2不为氢原子; 并且其中当R 2是氢原子时，R 1不是氢原子，R 3是氢原子或甲基，R 4是丙基，1-丙烯基或苯基; 由式（II）表示的戊内酯化合物：其制备方法; 和包含上述戊内酯化合物的香料组合物。

10. 发明授权

US07400568B2 Optical device, optical pickup and optical disk apparatus 失效
标题翻译：光学装置，光学拾取器和光盘装置
公开(公告)号：US07400568B2
公开(公告)日：2008-07-15
申请号：US10722482
申请日：2003-11-28
申请人： Seiichi Katou , Katsuhiko Kimura , Teruhisa Akashi , Kazuyuki Fukuda , Ryoji Okada , Hiromitsu Imamiya , Toshio Sugiyama , Hideo Suenaga
发明人： Seiichi Katou , Katsuhiko Kimura , Teruhisa Akashi , Kazuyuki Fukuda , Ryoji Okada , Hiromitsu Imamiya , Toshio Sugiyama , Hideo Suenaga
IPC分类号： G11B7/00
CPC分类号： G11B7/22 , G11B7/123 , G11B7/1275 , G11B7/1356 , G11B7/1359 , G11B2007/0006 , H01L2224/45144 , H01L2224/48091 , H01L2224/48464 , H01L2924/19107 , H01L2924/00014
摘要： An optical device wherein an optical component and a plurality of light emitting elements are mounted on an identical substrate, a level of a surface on which the optical component is mounted is different from that of a surface on which the light emitting elements are mounted by a step provided on the substrate, at least one plane vertical to the surface on which the optical component is mounted and located on a periphery of the substrate is opened, a reflecting surface, a transmitting surface or a diffraction grating surface of the optical component is provided along sides generated by the step provided in the substrate, optical axes of the plurality of light emitting elements of which polarization axes are in parallel with each other intersect with each other on the surface, and an exit light beam of the light emitting elements is emitted from the opened plane.
摘要翻译：一种光学器件，其中光学部件和多个发光元件安装在相同的基板上，安装有光学部件的表面的水平与安装有发光元件的表面的水平不同提供在基板上的至少一个垂直于其上安装有光学部件并且位于基板的周边上的表面的平面，提供光学部件的反射表面，透射表面或衍射光栅表面沿着由衬底中提供的台阶产生的边，偏振轴彼此平行的多个发光元件的光轴在表面上彼此相交，并且发射元件的出射光束从开放的飞机。

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