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1. 发明授权

US5824748A Composite pressure sensitive adhesive microspheres 失效
标题翻译：复合压敏胶微球
公开(公告)号：US5824748A
公开(公告)日：1998-10-20
申请号：US657266
申请日：1996-06-03
申请人： Michael R. Kesti , James E. Garbe , Joaquin Delgado , Spencer F. Silver , Richard J. Goetz
发明人： Michael R. Kesti , James E. Garbe , Joaquin Delgado , Spencer F. Silver , Richard J. Goetz
IPC分类号： C08F2/18 , C08F265/06 , C09J151/00 , C09J201/00 , C08F265/04
CPC分类号： C09J151/003 , C08F265/06 , Y10S525/903 , Y10T428/2982
摘要： Composite pressure sensitive adhesive microspheres are provided comprising two or more water insoluble polymers that are mixed wholly within the boundaries of polymeric microspheres. The range of monomers and polymers are chosen to tailor the properties of the composite pressure sensitive adhesive microspheres for specific performance and/or application requirements. Any polymer that can be dissolved into a solvent monomer or mixture of solvent monomers can be used to prepare the composite pressure sensitive adhesive microspheres. Pressure sensitive adhesive microspheres according to this invention can be prepared using free radical suspension polymerization.
摘要翻译：提供复合压敏粘合剂微球体，其包含完全混合在聚合物微球界限内的两种或多种水不溶性聚合物。选择单体和聚合物的范围以根据具体的性能和/或应用要求来定制复合压敏粘合剂微球的性质。可以将可溶解于溶剂单体或溶剂单体混合物中的任何聚合物用于制备复合压敏粘合剂微球。根据本发明的压敏粘合剂微球可以使用自由基悬浮聚合制备。

2. 发明授权

US5714237A Partially crosslinked microspheres 失效
标题翻译：部分交联微球
公开(公告)号：US5714237A
公开(公告)日：1998-02-03
申请号：US585795
申请日：1996-01-16
申请人： Terrence E. Cooprider , Michael D. Crandall , James E. Garbe , Richard J. Goetz , Michael R. Kesti
发明人： Terrence E. Cooprider , Michael D. Crandall , James E. Garbe , Richard J. Goetz , Michael R. Kesti
IPC分类号： C08F2/44 , C08F8/00 , C08F20/10 , C08F20/18 , C09J121/00 , C09J133/06 , C09J201/00 , B32B3/00
CPC分类号： C09J133/06 , C08F20/18 , C08L2205/18 , Y10T428/24893
摘要： An adhesive composition is provided comprising: (a) a plurality of polymeric, elastomeric microspheres wherein the microspheres are the reaction product of reactants comprising polymerizable starting materials comprising at least one C.sub.4 -C.sub.14 alkyl (meth)acrylate monomer and optionally at least one comonomer and have a solvent soluble portion that is 30-98% of the microsphere.
摘要翻译：提供了一种粘合剂组合物，其包括：（a）多个聚合弹性体微球，其中所述微球是包含可聚合起始材料的反应物的反应产物，其包含至少一种（甲基）丙烯酸烷基酯单体和任选的至少一种共聚单体，具有溶剂可溶部分，为微球的30-98％。

3. 再颁专利

USRE37563E1 Partially crosslinked microspheres 有权
标题翻译：部分交联微球
公开(公告)号：USRE37563E1
公开(公告)日：2002-02-26
申请号：US09443254
申请日：1999-11-18
申请人： Terrence E. Cooprider , Michael D. Crandall , James E. Garbe , Richard J. Goetz , Michael R. Kesti
发明人： Terrence E. Cooprider , Michael D. Crandall , James E. Garbe , Richard J. Goetz , Michael R. Kesti
IPC分类号： B32B300
CPC分类号： C09J133/06 , C08F20/18 , C08L2205/18 , Y10T428/24893
摘要： An adhesive composition is provided comprising: (a) a plurality of polymeric, elastomeric microspheres wherein the microspheres are the reaction product of reactants comprising polymerizable starting materials comprising at least one C4-C14 alkyl (meth)acrylate monomer and optionally at least one comonomer and have a solvent soluble portion that is 30-98% of the microsphere.
摘要翻译：提供了一种粘合剂组合物，其包括：（a）多个聚合弹性体微球，其中所述微球是包含可聚合起始材料的反应物的反应产物，其包含至少一种（甲基）丙烯酸烷基酯单体和任选的至少一种共聚单体，具有溶剂可溶部分，为微球的30-98％。

4. 发明授权

US06872268B2 Method of conforming an adherent film to a substrate by application of vacuum 失效
标题翻译：通过施加真空使粘附膜与基底相适应的方法
公开(公告)号：US06872268B2
公开(公告)日：2005-03-29
申请号：US10167347
申请日：2002-06-11
申请人： John R. David , Jeffrey O. Emslander , Danny L. Fleming , Michael R. Kesti , Larry A. Meixner , Frank T. Sher , Ronald S. Steelman , David J. Yarusso
发明人： John R. David , Jeffrey O. Emslander , Danny L. Fleming , Michael R. Kesti , Larry A. Meixner , Frank T. Sher , Ronald S. Steelman , David J. Yarusso
IPC分类号： B32B33/00 , B29C65/48 , B29L9/00 , B44C1/10 , C04B41/45 , C04B41/61 , C09J7/02 , C09J201/00 , C23C26/00 , G09F7/18 , G09F15/00 , G09F19/22 , B32B31/04
CPC分类号： B44C1/10 , B32B37/003 , C04B41/009 , C04B41/4503 , C04B41/61 , C09J7/38 , C09J2201/28 , C23C26/00 , Y10T156/1028 , C04B41/4515 , C04B2103/54 , C04B28/02
摘要： Films are closely conformed to substrates by reducing the air pressure to a subatmospheric level in at least one airflow pathway that is present in the film or the substrate. The reduced air pressure enables the film to tightly contact the substrate in locations where protrusions or depressions on the substrate are present. The method is particularly useful for conforming film containing graphics to a variety of substrates such as the sides of semi-trailers or concrete block walls, even in instances where the semi-trailer sides include rivets and/or grooves and where the concrete block wall is relatively rough.
摘要翻译：通过在存在于膜或基底中的至少一个气流路径中将空气压力降低到低于大气压的水平，薄膜紧密地与基底相一致。降低的空气压力使膜能够在存在基板上的突起或凹陷的位置处紧密接触基板。该方法对于使膜包含图形与各种衬底例如半挂车或混凝土块壁的侧面一致是特别有用的，即使在半挂车侧面包括铆钉和/或凹槽的情况下，以及混凝土阻挡壁比较粗糙

5. 发明授权

US07141133B2 Method of conforming a film to a surface 有权
公开(公告)号：US07141133B2
公开(公告)日：2006-11-28
申请号：US10325509
申请日：2002-12-19
申请人： Michael R. Kesti , Frank T. Sher , Stephen J. Aden , Ronald S. Steelman , John R. David
发明人： Michael R. Kesti , Frank T. Sher , Stephen J. Aden , Ronald S. Steelman , John R. David
IPC分类号： B32B37/10
CPC分类号： B29C63/0078 , B29C63/0047 , B29C63/02 , B29C2791/006 , Y10T156/1028 , Y10T156/1056 , Y10T156/1057
摘要： Methods of applying film to substrates are provided wherein the film matingly conforms to the configuration of the substrate, including areas adjacent protrusions or depressions in the substrate. In certain embodiments, the film is punctured by a probe and a vacuum is applied to the probe in order to aspirate air and urge the film toward a position of compliance with the substrate. Optionally, the film is softened by heat in order to facilitate conformance with the shape of the substrate.

6. 发明授权

US4890163A Interrupting a transition sequence between video sources 失效
标题翻译：中断视频源之间的转换序列
公开(公告)号：US4890163A
公开(公告)日：1989-12-26
申请号：US178106
申请日：1988-04-06
申请人： Brion Johnson , Michael R. Kesti , Keith Y. Reynolds
发明人： Brion Johnson , Michael R. Kesti , Keith Y. Reynolds
IPC分类号： H04N5/268
CPC分类号： H04N5/268
摘要： A transition interrupt for a video switcher which occurs at any point during or just prior to a transition between a program bus source and a preset bus source replaces the source on the preset bus with a new source. The program bus executes a cut or fade to black of the current source, and then the new source from the preset bus is switched to the program bus so that the new source is now on the program bus at black. The program bus is held at black, if necessary, until any necessary initial activation sequence is completed, such as preroll for a tape or cassette recorder, and then brought up from black to complete the new transition due to the transition interrupt.

7. 发明授权

US07687126B2 Adhesive articles and release liners 有权
标题翻译：粘合制品和脱模衬垫
公开(公告)号：US07687126B2
公开(公告)日：2010-03-30
申请号：US11209146
申请日：2005-08-22
申请人： Danny L. Fleming , Michael R. Kesti , John A. Nielsen , Richard L. Peloquin , Frank T. Sher , David J. Yarusso
发明人： Danny L. Fleming , Michael R. Kesti , John A. Nielsen , Richard L. Peloquin , Frank T. Sher , David J. Yarusso
IPC分类号： B32B33/00
CPC分类号： C09J7/403 , C09J7/10 , Y10S428/914 , Y10T156/1023 , Y10T428/14 , Y10T428/1471 , Y10T428/1476 , Y10T428/1486 , Y10T428/24479 , Y10T428/24612 , Y10T428/2486 , Y10T428/28 , Y10T428/2839
摘要： The present application is directed to adhesive articles and release liners. Namely, the present application is directed to an article comprising an adhesive layer with a structured surface. The structured surface comprises a first groove and a second groove recessed into the adhesive layer from a reference plane defined by the adhesive surface on either rim of the groove. In some embodiments, the second groove is contained within the first groove, and in other embodiments the grooves are separate. The first groove and the second groove have walls. The wall angle of the first groove with respect to the reference plane is non-zero and is smaller than the wall angle of the second groove with respect to the reference plane. The application is also directed to release liners for the adhesive article, wherein the surface of the release liner is the inverse of the adhesive surface.
摘要翻译：本申请涉及粘合剂制品和脱模衬垫。即，本申请涉及包含具有结构化表面的粘合剂层的制品。结构化表面包括第一凹槽和从由凹槽的任一边缘上的粘合剂表面限定的参考平面凹入粘合剂层的第二凹槽。在一些实施例中，第二凹槽包含在第一凹槽内，而在其它实施例中凹槽是分开的。第一槽和第二槽具有壁。第一凹槽相对于参考平面的壁角不是零并且小于第二凹槽相对于参考平面的壁角。该应用还涉及用于粘合剂制品的剥离衬垫，其中剥离衬垫的表面与粘合剂表面相反。

8. 发明授权

US5756625A Stabilized adhesive microspheres 失效
标题翻译：稳定粘合剂微球
公开(公告)号：US5756625A
公开(公告)日：1998-05-26
申请号：US731351
申请日：1996-10-11
申请人： Michael D. Crandall , Michael R. Kesti
发明人： Michael D. Crandall , Michael R. Kesti
IPC分类号： C08F2/00 , C08F2/44 , C08F220/00 , C08F291/00 , C08J9/16 , C09J4/02 , C09J4/06 , C09J133/06 , C08F18/02 , C08F12/30 , C08F20/10 , C08F218/02
CPC分类号： C09J4/06
摘要： Stabilized microsphere adhesive composition comprising: a plurality of polymeric, elastomeric microspheres wherein the microspheres are the reaction product of reactants comprising polymerizable starting materials comprising at least one C.sub.4 -C.sub.14 alkyl (meth)acrylate monomer and optionally at least one comonomer, at least one vinyl-unsaturated additive having both an ionic moiety and a hydrophobic moiety and containing at least 5 but not more than 40 carbon atoms in an amount about 0.1 to 3 parts by weight of the microspheres; optionally, a polymeric stabilizer in an amount of between about 0.1 and about 3 parts by weight per 100 parts by weight of the microspheres; a surfactant in an amount of no greater than about 5 parts by weight per 100 parts by weight of the microspheres; optionally a modifier, wherein the modifier is at least one of a chain transfer agent, a tackifier, a solvent or the like in an amount that is sufficient to provide microspheres with a n-heptane soluble portion in the range of 30-98%; and (f) an initiator in an amount effective to catalyze the polymerization reaction present in amounts ranging from about 0.1 to approximately 2 parts by weight per 100 parts by weight of the polymerizable monomer starting material.
摘要翻译：稳定的微球粘合剂组合物包括：多个聚合弹性体微球，其中微球是包含可聚合原料的反应物的反应产物，其包含至少一种（甲基）丙烯酸C 4 -C 14烷基酯单体和任选的至少一种共聚单体，至少一种乙烯基 - 不饱和添加剂，其具有离子部分和疏水部分，并且含有约0.1至3重量份的微球的至少5个但不多于40个碳原子; 任选地，相对于每100重量份的微球，约0.1至约3重量份的量的聚合物稳定剂; 相对于100重量份微球，表面活性剂的量不大于约5重量份; 任选的改性剂，其中改性剂是链转移剂，增粘剂，溶剂等中的至少一种，其量足以提供具有30-98％范围内的正庚烷可溶部分的微球; 和（f）有效催化聚合反应的量的引发剂的存在量为每100重量份可聚合单体原料约0.1-约2重量份。

9. 发明申请

US20100143654A1 ADHESIVE ARTICLES AND RELEASE LINERS 有权
标题翻译：粘贴文章和发布内容
公开(公告)号：US20100143654A1
公开(公告)日：2010-06-10
申请号：US12706262
申请日：2010-02-16
申请人： Danny L. Fleming , Michael R. Kesti , John A. Nielsen , Richard L. Peloquin , Frank T. Sher , David J. Yarusso
发明人： Danny L. Fleming , Michael R. Kesti , John A. Nielsen , Richard L. Peloquin , Frank T. Sher , David J. Yarusso
IPC分类号： B32B3/30
CPC分类号： C09J7/403 , C09J7/10 , Y10S428/914 , Y10T156/1023 , Y10T428/14 , Y10T428/1471 , Y10T428/1476 , Y10T428/1486 , Y10T428/24479 , Y10T428/24612 , Y10T428/2486 , Y10T428/28 , Y10T428/2839
摘要： The present application is directed to adhesive articles and release liners. Namely, the present application is directed to an article comprising an adhesive layer with a structured surface. The structured surface comprises a first groove and a second groove recessed into the adhesive layer from a reference plane defined by the adhesive surface on either rim of the groove. In some embodiments, the second groove is contained within the first groove, and in other embodiments the grooves are separate. The first groove and the second groove have walls. The wall angle of the first groove with respect to the reference plane is non-zero and is smaller than the wall angle of the second groove with respect to the reference plane. The application is also directed to release liners for the adhesive article, wherein the surface of the release liner is the inverse of the adhesive surface.
摘要翻译：本申请涉及粘合剂制品和脱模衬垫。即，本申请涉及包含具有结构化表面的粘合剂层的制品。结构化表面包括第一凹槽和从由凹槽的任一边缘上的粘合剂表面限定的参考平面凹入粘合剂层的第二凹槽。在一些实施例中，第二凹槽包含在第一凹槽内，而在其它实施例中凹槽是分开的。第一槽和第二槽具有壁。第一凹槽相对于参考平面的壁角不是零并且小于第二凹槽相对于参考平面的壁角。该应用还涉及用于粘合剂制品的剥离衬垫，其中剥离衬垫的表面与粘合剂表面相反。

10. 发明授权

US06368708B1 Polyolefin microspheres 失效
标题翻译：聚烯烃微球
公开(公告)号：US06368708B1
公开(公告)日：2002-04-09
申请号：US08667153
申请日：1996-06-20
申请人： Katherine A. Brown , Michael R. Kesti
发明人： Katherine A. Brown , Michael R. Kesti
IPC分类号： C08F11006
CPC分类号： C09D123/20 , C08F10/00 , C08F110/14 , C08L2205/18 , C08L2666/02 , C09J123/20 , Y10S526/909 , Y10S526/931 , Y10T428/2861 , Y10T428/2878 , Y10T428/2982 , Y10T428/31855 , C08F2/14 , C08F2500/24 , C08F4/7006
摘要： Microspheres comprise a polymer or copolymer including one or more of 1) a plurality of C3 or larger alpha-olefin units wherein the polymer has an average number of branch points less than one per monomer unit, and 2) a plurality of C2 alpha-olefin units wherein the polymer has an average number of branch points greater than 0.01 per monomer unit, the microspheres having an average diameter in the range of 1 to 300 micrometers. Optionally, the polymer of the microspheres can be crosslinked. The microspheres can be prepared by suspension or dispersion polymerization processes using aqueous or organic reaction media.
摘要翻译：微球包括聚合物或共聚物，其包括1）多个C3或更多的α-烯烃单元中的一种或多种，其中聚合物具有每个单体单元小于1的平均分支点数，以及2）多个C 2α-烯烃单元，其中聚合物具有大于每单体单元0.01的分支点的平均数，该微球的平均直径在1至300微米的范围内。任选地，微球的聚合物可以交联。微球可以通过使用水或有机反应介质的悬浮或分散聚合方法制备。

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