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1. 发明授权

US07700788B2 Hydroxymethyl furfural oxidation methods 有权
标题翻译：羟甲基糠醛氧化法
公开(公告)号：US07700788B2
公开(公告)日：2010-04-20
申请号：US11932436
申请日：2007-10-31
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/44
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中将包含HMF的原料提供到反应器中。将空气和O2中的至少一个提供到反应器中。起始材料与包含Pt的催化剂在载体材料上接触，其中接触在约50℃至约200℃的反应器温度下进行。制备其中提供ZrO 2并被煅烧的氧化催化剂的方法。将ZrO 2与乙酰丙酮化铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2的流量下钝化。

2. 发明申请

US20100152470A1 Hydroxymethyl Furfural Oxidation Methods 有权
公开(公告)号：US20100152470A1
公开(公告)日：2010-06-17
申请号：US12712100
申请日：2010-02-24
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/46
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.

3. 发明授权

US08193382B2 Hydroxymethyl furfural oxidation methods 有权
公开(公告)号：US08193382B2
公开(公告)日：2012-06-05
申请号：US12712100
申请日：2010-02-24
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/48
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.

4. 发明授权

US08193381B2 Hydroxymethyl furfural oxidation methods 有权
标题翻译：羟甲基糠醛氧化法
公开(公告)号：US08193381B2
公开(公告)日：2012-06-05
申请号：US12712095
申请日：2010-02-24
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/02 , C07D307/48
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中提供包含HMF的原料进入反应器。将空气和O2中的至少一个提供到反应器中。起始材料与包含Pt的催化剂在载体材料上接触，其中接触在约50℃至约200℃的反应器温度下进行。制备其中提供ZrO 2并被煅烧的氧化催化剂的方法。将ZrO 2与乙酰丙酮化铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2的流量下钝化。

5. 发明申请

US20100152469A1 Hydroxymethyl Furfural Oxidation Methods 有权
标题翻译：羟甲基糠醛氧化法
公开(公告)号：US20100152469A1
公开(公告)日：2010-06-17
申请号：US12712095
申请日：2010-02-24
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/68
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中将包含HMF的原料提供到反应器中。将空气和O2中的至少一个提供到反应器中。起始材料与包含Pt的催化剂在载体材料上接触，其中接触在约50℃至约200℃的反应器温度下进行。制备其中提供ZrO 2并被煅烧的氧化催化剂的方法。将ZrO 2与乙酰丙酮化铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2的流量下钝化。

6. 发明授权

US07858667B2 Alcohol synthesis from CO or CO2 有权
标题翻译：来自CO或CO 2的酒精合成
公开(公告)号：US07858667B2
公开(公告)日：2010-12-28
申请号：US11611160
申请日：2006-12-15
申请人： Jianli Hu , Robert A. Dagle , Jamelyn D. Holladay , Chunshe Cao , Yong Wang , James F. White , Douglas C. Elliott , Don J. Stevens
发明人： Jianli Hu , Robert A. Dagle , Jamelyn D. Holladay , Chunshe Cao , Yong Wang , James F. White , Douglas C. Elliott , Don J. Stevens
IPC分类号： C07C27/00
CPC分类号： C07C29/152 , B01J19/0093 , B01J2219/00835 , B01J2219/00873 , B01J2219/00961 , B01J2219/00984 , C07C29/157 , Y02P20/52 , C07C31/04 , C07C31/08 , C07C31/02
摘要： Methods for producing alcohols from CO or CO2 and H2 utilizing a palladium-zinc on alumina catalyst are described. Methods of synthesizing alcohols over various catalysts in microchannels are also described. Ethanol, higher alcohols, and other C2+ oxygenates can produced utilizing Rh—Mn or a Fisher-Tropsch catalyst.
摘要翻译：描述了使用氧化铝催化剂上的钯 - 锌从CO或CO 2和H 2生产醇的方法。还描述了在微通道中在各种催化剂上合成醇的方法。可以使用Rh-Mn或Fisher-Tropsch催化剂生产乙醇，高级醇和其他C2 +含氧化合物。

7. 发明授权

US07585472B2 Microcombustors, microreformers, and methods involving combusting or reforming fluids 有权
标题翻译：微型燃烧器，微型重整器和涉及燃烧或重整流体的方法
公开(公告)号：US07585472B2
公开(公告)日：2009-09-08
申请号：US10434443
申请日：2003-05-07
申请人： Jamelyn D. Holladay , Yong Wang , Jianli Hu , Ya-Huei Chin , Robert A. Dagle , Guanguang Xia , Eddie G. Baker , Daniel R. Palo , Max Phelps , Heon Jung
发明人： Jamelyn D. Holladay , Yong Wang , Jianli Hu , Ya-Huei Chin , Robert A. Dagle , Guanguang Xia , Eddie G. Baker , Daniel R. Palo , Max Phelps , Heon Jung
IPC分类号： B01J8/04
CPC分类号： F23C13/00 , B01J19/0093 , B01J21/04 , B01J21/066 , B01J23/60 , B01J23/63 , B01J37/03 , B01J2219/00783 , B01J2219/00833 , B01J2219/00835 , B01J2219/00873 , B01J2219/00891 , C01B3/323 , C01B3/384 , C01B2203/00 , C01B2203/0233 , C01B2203/04 , C01B2203/0445 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0816 , C01B2203/0822 , C01B2203/0827 , C01B2203/1011 , C01B2203/1052 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , C01B2203/1217 , C01B2203/1223 , C01B2203/1288 , C01B2203/1619 , F23C2900/03001 , Y02P20/128 , Y02P20/52
摘要： The invention describes combustors and steam reformers and methods of combustion and steam reforming. For example, integrated combustion reactors are described in which heat from combustion is transferred to an endothermic reaction. Thermally efficient reactors and methods of alcohol steam reforming are also described. Also described is an integrated combustor/reformer containing a methanation catalyst.
摘要翻译：本发明描述了燃烧器和蒸汽重整器以及燃烧和蒸汽重整的方法。例如，描述了将来自燃烧的热转移到吸热反应的综合燃烧反应器。还描述了热效率的反应器和醇蒸汽重整的方法。还描述了含有甲烷化催化剂的一体化燃烧器/重整器。

8. 发明授权

US07566441B2 Methods of conducting catalytic combustion in a multizone reactor, and a method of making a thermally stable catalyst support 有权
标题翻译：在多区域反应器中进行催化燃烧的方法以及制备热稳定催化剂载体的方法
公开(公告)号：US07566441B2
公开(公告)日：2009-07-28
申请号：US10966158
申请日：2004-10-15
申请人： Francis P. Daly , Junko M. Watson , Yong Wang , Jianli Hu , Chunshe Cao , Richard Long , Rachid Taha
发明人： Francis P. Daly , Junko M. Watson , Yong Wang , Jianli Hu , Chunshe Cao , Richard Long , Rachid Taha
IPC分类号： C07C1/02 , C01B3/26 , F23C13/00
CPC分类号： B01J23/42 , B01J19/0093 , B01J23/688 , B01J35/04 , B01J35/10 , B01J35/1014 , B01J37/0215 , B01J2219/00783 , B01J2219/00788 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/00873 , B01J2219/00957 , B01J2219/00984 , C01B3/382 , C01B3/386 , C01B3/40 , C01B32/40 , C01B2203/0244 , C01B2203/0261 , C01B2203/107 , C01B2203/1082 , C01B2203/1217 , C01B2203/1235 , C01B2203/143 , C01B2203/1614 , C01B2203/82 , F23C13/00 , F23C2900/03001 , Y02P20/52
摘要： The invention provides methods of combusting a fuel in a reactor that includes at least 3 zones each of which contains a solid catalyst. A method of making a thermally-stable alumina support from fumed alumina is also described.
摘要翻译：本发明提供在反应器中燃烧燃料的方法，其包括至少3个区，每个区含有固体催化剂。还描述了由热解氧化铝制备热稳定氧化铝载体的方法。

9. 发明申请

US20090113787A1 Palladium Catalyzed Hydrogenation of Bio-Oils and Organic Compounds 有权
标题翻译：钯催化生物油和有机化合物的氢化
公开(公告)号：US20090113787A1
公开(公告)日：2009-05-07
申请号：US12140929
申请日：2008-06-17
申请人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
发明人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
IPC分类号： C10L1/18
CPC分类号： C07C29/172 , B01J21/18 , B01J23/44 , B01J23/462 , B01J37/0201 , C07C29/149 , C07C2601/08 , C07C2601/14 , C07D307/06 , C10G1/00 , C10G1/06 , C10G1/086 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1014 , C10G2300/4018 , Y02E50/14 , Y02E50/32 , Y02P20/52 , Y02P30/20 , C07C35/14 , C07C35/08 , C07C31/04 , C07C31/08 , C07C31/20 , C07C31/125 , C07C35/06
摘要： The invention provides palladium-catalyzed hydrogenations of bio-oils and certain organic compounds. Experimental results have shown unexpected and superior results for palladium-catalyzed hydrogenations of organic compounds typically found in bio-oils.
摘要翻译：本发明提供钯催化的生物油和某些有机化合物的氢化。实验结果已经显示出对于通常在生物油中发现的有机化合物的钯催化氢化的意想不到的和优异的结果。

10. 发明申请

US20070173653A1 Method of performing sugar dehydration and catalyst treatment 失效
标题翻译：糖脱水和催化剂处理方法
公开(公告)号：US20070173653A1
公开(公告)日：2007-07-26
申请号：US11342146
申请日：2006-01-26
申请人： Jianli Hu , Johnathan Holladay , Xinjie Zhang , Yong Wang
发明人： Jianli Hu , Johnathan Holladay , Xinjie Zhang , Yong Wang
IPC分类号： C07D311/22
CPC分类号： C07H1/00
摘要： The invention includes a method of treating a solid acid catalyst. After exposing the catalyst to a mixture containing a sugar alcohol, the catalyst is washed with an organic solvent and is then exposed to a second reaction mixture. The invention includes a process for production of anhydrosugar alcohol. A solid acid catalyst is provided to convert sugar alcohol in a first sample to an anhydrosugar alcohol. The catalyst is then washed with an organic solvent and is subsequently utilized to expose a second sample. The invention includes a method for selective production of an anhydrosugar. A solid acid catalyst is provided within a reactor and anhydrosugar alcohol is formed by flowing a starting sugar alcohol into the reactor. The acid catalyst is then exposed to an organic solvent which allows a greater amount of additional anhydrosugar to be produced than would occur without exposing the acid catalyst to the organic solvent.
摘要翻译：本发明包括一种处理固体酸催化剂的方法。在将催化剂暴露于含有糖醇的混合物之后，用有机溶剂洗涤催化剂，然后暴露于第二反应混合物。本发明包括生产脱水葡萄糖醇的方法。提供固体酸催化剂以将第一样品中的糖醇转化为脱水葡萄糖醇。然后将催化剂用有机溶剂洗涤，随后用于暴露第二个样品。本发明包括选择性生产脱水糖的方法。在反应器内提供固体酸催化剂，通过将起始糖醇流入反应器而形成脱水葡萄糖醇。然后将酸催化剂暴露于有机溶剂，其允许比不会将酸催化剂暴露于有机溶剂而产生更多量的额外的脱水糖。

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