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1. 发明授权

US07858667B2 Alcohol synthesis from CO or CO2 有权
标题翻译：来自CO或CO 2的酒精合成
公开(公告)号：US07858667B2
公开(公告)日：2010-12-28
申请号：US11611160
申请日：2006-12-15
申请人： Jianli Hu , Robert A. Dagle , Jamelyn D. Holladay , Chunshe Cao , Yong Wang , James F. White , Douglas C. Elliott , Don J. Stevens
发明人： Jianli Hu , Robert A. Dagle , Jamelyn D. Holladay , Chunshe Cao , Yong Wang , James F. White , Douglas C. Elliott , Don J. Stevens
IPC分类号： C07C27/00
CPC分类号： C07C29/152 , B01J19/0093 , B01J2219/00835 , B01J2219/00873 , B01J2219/00961 , B01J2219/00984 , C07C29/157 , Y02P20/52 , C07C31/04 , C07C31/08 , C07C31/02
摘要： Methods for producing alcohols from CO or CO2 and H2 utilizing a palladium-zinc on alumina catalyst are described. Methods of synthesizing alcohols over various catalysts in microchannels are also described. Ethanol, higher alcohols, and other C2+ oxygenates can produced utilizing Rh—Mn or a Fisher-Tropsch catalyst.
摘要翻译：描述了使用氧化铝催化剂上的钯 - 锌从CO或CO 2和H 2生产醇的方法。还描述了在微通道中在各种催化剂上合成醇的方法。可以使用Rh-Mn或Fisher-Tropsch催化剂生产乙醇，高级醇和其他C2 +含氧化合物。

2. 发明授权

US08203023B2 Tailored fischer-tropsch synthesis product distribution 有权
标题翻译：定制费托合成产品分销
公开(公告)号：US08203023B2
公开(公告)日：2012-06-19
申请号：US12023939
申请日：2008-01-31
申请人： Yong Wang , Chunshe Cao , Xiaohong Shari Li , Douglas C. Elliott
发明人： Yong Wang , Chunshe Cao , Xiaohong Shari Li , Douglas C. Elliott
IPC分类号： C07C9/22 , C07C1/02
CPC分类号： B01J19/0093 , B01J2219/00835 , B01J2219/0086 , C10G2/332 , C10G2/333 , Y02P20/142
摘要： Novel methods of Fischer-Tropsch synthesis are described. It has been discovered that conducting the Fischer-Tropsch synthesis over a catalyst with a catalytically active surface layer of 35 microns or less results in a liquid hydrocarbon product with a high ratio of C5-C20:C20+. Descriptions of novel Fischer-Tropsch catalysts and reactors are also provided. Novel hydrocarbon compositions with a high ratio of C5-C20:C20+ are also described.
摘要翻译：描述了费 - 托合成的新方法。已经发现，通过具有35微米或更小的催化活性表面层的催化剂进行费 - 托合成导致具有高比率的C 5 -C 20：C 20 +的液态烃产物。还提供了新型费 - 托催化剂和反应器的描述。还描述了具有高比例的C5-C20：C20 +的新型烃组合物。

3. 发明申请

US20080207969A1 Tailored Fischer-Tropsch Synthesis Product Distribution 有权
标题翻译：定制费托合成产品分销
公开(公告)号：US20080207969A1
公开(公告)日：2008-08-28
申请号：US12023939
申请日：2008-01-31
申请人： Yong Wang , Chunshe Cao , Xiaohong Shari Li , Douglas C. Elliott
发明人： Yong Wang , Chunshe Cao , Xiaohong Shari Li , Douglas C. Elliott
IPC分类号： C07C1/04 , C10G2/00
CPC分类号： B01J19/0093 , B01J2219/00835 , B01J2219/0086 , C10G2/332 , C10G2/333 , Y02P20/142
摘要： Novel methods of Fischer-Tropsch synthesis are described. It has been discovered that conducting the Fischer-Tropsch synthesis over a catalyst with a catalytically active surface layer of 35 microns or less results in a liquid hydrocarbon product with a high ratio of C5-C20:C20+. Descriptions of novel Fischer-Tropsch catalysts and reactors are also provided. Novel hydrocarbon compositions with a high ratio of C5-C20:C20+ are also described.
摘要翻译：描述了费 - 托合成的新方法。已经发现，在具有35微米或更小的催化活性表面层的催化剂上进行费 - 托合成导致具有高比率C 5 -C 3 - 20 ：C 20 + +。还提供了新型费 - 托催化剂和反应器的描述。还描述了具有高比例的C 5 -C 20 -C 20 O +的新型烃组合物。

4. 发明授权

US07425657B1 Palladium catalyzed hydrogenation of bio-oils and organic compounds 有权
标题翻译：钯催化氢化生物油和有机化合物
公开(公告)号：US07425657B1
公开(公告)日：2008-09-16
申请号：US11759075
申请日：2007-06-06
申请人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
发明人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
IPC分类号： C07C41/48 , C07C41/50 , C07C33/03 , C07C31/18
CPC分类号： C07C29/172 , B01J21/18 , B01J23/44 , B01J23/462 , B01J37/0201 , C07C29/149 , C07C2601/08 , C07C2601/14 , C07D307/06 , C10G1/00 , C10G1/06 , C10G1/086 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1014 , C10G2300/4018 , Y02E50/14 , Y02E50/32 , Y02P20/52 , Y02P30/20 , C07C35/14 , C07C35/08 , C07C31/04 , C07C31/08 , C07C31/20 , C07C31/125 , C07C35/06
摘要： The invention provides palladium-catalyzed hydrogenations of bio-oils and certain organic compounds. Experimental results have shown unexpected and superior results for palladium-catalyzed hydrogenations of organic compounds typically found in bio-oils.
摘要翻译：本发明提供钯催化的生物油和某些有机化合物的氢化。实验结果已经显示出对于通常在生物油中发现的有机化合物的钯催化氢化的意想不到的和优异的结果。

5. 发明申请

US20090113787A1 Palladium Catalyzed Hydrogenation of Bio-Oils and Organic Compounds 有权
标题翻译：钯催化生物油和有机化合物的氢化
公开(公告)号：US20090113787A1
公开(公告)日：2009-05-07
申请号：US12140929
申请日：2008-06-17
申请人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
发明人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
IPC分类号： C10L1/18
CPC分类号： C07C29/172 , B01J21/18 , B01J23/44 , B01J23/462 , B01J37/0201 , C07C29/149 , C07C2601/08 , C07C2601/14 , C07D307/06 , C10G1/00 , C10G1/06 , C10G1/086 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1014 , C10G2300/4018 , Y02E50/14 , Y02E50/32 , Y02P20/52 , Y02P30/20 , C07C35/14 , C07C35/08 , C07C31/04 , C07C31/08 , C07C31/20 , C07C31/125 , C07C35/06
摘要： The invention provides palladium-catalyzed hydrogenations of bio-oils and certain organic compounds. Experimental results have shown unexpected and superior results for palladium-catalyzed hydrogenations of organic compounds typically found in bio-oils.
摘要翻译：本发明提供钯催化的生物油和某些有机化合物的氢化。实验结果已经显示出对于通常在生物油中发现的有机化合物的钯催化氢化的意想不到的和优异的结果。

6. 发明授权

US07956224B2 Palladium catalyzed hydrogenation of bio-oils and organic compounds 有权
标题翻译：钯催化氢化生物油和有机化合物
公开(公告)号：US07956224B2
公开(公告)日：2011-06-07
申请号：US12140929
申请日：2008-06-17
申请人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
发明人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
IPC分类号： C07C37/00 , C07C35/06
CPC分类号： C07C29/172 , B01J21/18 , B01J23/44 , B01J23/462 , B01J37/0201 , C07C29/149 , C07C2601/08 , C07C2601/14 , C07D307/06 , C10G1/00 , C10G1/06 , C10G1/086 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1014 , C10G2300/4018 , Y02E50/14 , Y02E50/32 , Y02P20/52 , Y02P30/20 , C07C35/14 , C07C35/08 , C07C31/04 , C07C31/08 , C07C31/20 , C07C31/125 , C07C35/06
摘要： The invention provides palladium-catalyzed hydrogenations of bio-oils and certain organic compounds. Experimental results have shown unexpected and superior results for palladium-catalyzed hydrogenations of organic compounds typically found in bio-oils.
摘要翻译：本发明提供钯催化的生物油和某些有机化合物的氢化。实验结果已经显示出对于通常在生物油中发现的有机化合物的钯催化氢化的意想不到的和优异的结果。

7. 发明授权

US06570043B2 Converting sugars to sugar alcohols by aqueous phase catalytic hydrogenation 有权
公开(公告)号：US06570043B2
公开(公告)日：2003-05-27
申请号：US09845646
申请日：2001-04-27
申请人： Douglas C. Elliott , Todd A. Werpy , Yong Wang , John G. Frye, Jr.
发明人： Douglas C. Elliott , Todd A. Werpy , Yong Wang , John G. Frye, Jr.
IPC分类号： C07C2700
CPC分类号： C07C29/141 , B01J21/063 , B01J23/462 , C07C31/26
摘要： The present invention provides a method of converting sugars to their corresponding sugar alcohols by catalytic hydrogenation in the aqueous phase. It has been found that surprisingly superior results can be obtained by utilizing a relatively low temperature (less than 120° C.), selected hydrogenation conditions, and a hydrothermally stable catalyst. These results include excellent sugar conversion to the desired sugar alcohol, in combination with long life under hydrothermal conditions.

8. 发明授权

US08608981B2 Methods for sulfate removal in liquid-phase catalytic hydrothermal gasification of biomass 有权
标题翻译：生物质液相催化水热气化硫酸盐去除方法
公开(公告)号：US08608981B2
公开(公告)日：2013-12-17
申请号：US13541003
申请日：2012-07-03
申请人： Douglas C. Elliott , James Oyler
发明人： Douglas C. Elliott , James Oyler
IPC分类号： C01B3/38 , C01B3/24
CPC分类号： B01J19/14 , B01J21/18 , B01J23/462 , B01J23/75 , B01J23/78 , B01J39/02 , B09B3/00 , B09B3/0083 , C10B53/02 , C10J3/78 , C10J2300/0916 , C10J2300/0923 , C10J2300/0979 , C10L3/08 , C10L5/44 , C10L9/086 , Y02E50/10 , Y02E50/14 , Y02E50/30 , Y02P20/145 , Y02P20/52
摘要： Processing of wet biomass feedstock by liquid-phase catalytic hydrothermal gasification must address catalyst fouling and poisoning. One solution can involve heating the wet biomass with a heating unit to a pre-treatment temperature sufficient for organic constituents in the feedstock to decompose, for precipitates of inorganic wastes to form, for preheating the wet feedstock in preparation for subsequent removal of soluble sulfate contaminants, or combinations thereof. Processing further includes reacting the soluble sulfate contaminants with cations present in the feedstock material to yield a sulfate-containing precipitate and separating the inorganic precipitates and/or the sulfate-containing precipitates out of the wet feedstock. Having removed much of the inorganic wastes and the sulfate contaminants that can cause poisoning and fouling, the wet biomass feedstock can be exposed to the heterogeneous catalyst for gasification.
摘要翻译：通过液相催化水热气化处理湿生物质原料必须解决催化剂污染和中毒问题。一种解决方案可以包括用加热单元将湿生物质加热到足以使原料中的有机成分分解的预处理温度，用于沉淀无机废物以形成，用于预热湿原料以备后续除去可溶性硫酸盐污染物，或其组合。处理进一步包括使可溶性硫酸盐污染物与原料中存在的阳离子反应以产生含硫酸盐的沉淀物，并将无机沉淀物和/或硫酸盐沉淀物从湿原料中分离出来。除去大量无机废物和可能引起中毒和结垢的硫酸盐污染物，湿生物质原料可暴露于非均相催化剂进行气化。

9. 发明授权

US5977013A Catalyst and method for aqueous phase reactions 失效
标题翻译：催化剂和水相反应方法
公开(公告)号：US5977013A
公开(公告)日：1999-11-02
申请号：US780094
申请日：1996-12-19
申请人： Douglas C. Elliott , Todd R. Hart
发明人： Douglas C. Elliott , Todd R. Hart
IPC分类号： B01J23/72 , B01J23/755 , B01J23/835 , B01J23/889 , B01J23/89 , C01B3/32
CPC分类号： C01B3/326 , B01J23/72 , B01J23/755 , B01J23/835 , B01J23/889 , B01J23/8896 , B01J23/892 , C01B2203/1041 , C01B2203/1052 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , Y02P20/52
摘要： The present invention is a catalyst in the form of a plurality of porous particles wherein each particle is a support having nickel metal catalytic phase or reduced nickel deposited thereon in a first dispersed phase and an additional metal deposited onto the support in a second dispersed phase. The additional metal is effective in retarding or reducing agglomeration or sintering of the nickel metal catalytic phase without substantially affecting the catalytic activity, thereby increasing the life time of the catalyst.
摘要翻译：本发明是多个多孔颗粒形式的催化剂，其中每个颗粒是在第一分散相中沉积有镍金属催化相或还原镍的载体，以及在第二分散相中沉积到载体上的附加金属。另外的金属有效地延缓或减少镍金属催化相的附聚或烧结，而基本上不影响催化活性，从而增加催化剂的使用寿命。

10. 发明授权

US5883266A Hydrogenated 5-carbon compound and method of making 失效
标题翻译：氢化5碳化合物及其制备方法
公开(公告)号：US5883266A
公开(公告)日：1999-03-16
申请号：US8356
申请日：1998-01-16
申请人： Douglas C. Elliott , John G. Frye
发明人： Douglas C. Elliott , John G. Frye
IPC分类号： C07D307/06 , C07D307/33 , C07D309/00 , C07C27/00 , C07D307/02
CPC分类号： C07D307/33 , C07D307/06
摘要： The present invention is based upon the surprising discovery that a 5-carbon compound selected from the group of 4-oxopentanoic acid, at least one lactone of 4-oxopentanoic acid, and combinations thereof, may be hydrogenated with a bimetallic catalyst of a noble metal in combination with a second metal and preserve the pendant methyl group. It was further unexpectedly discovered that the same conditions of bimetallic catalyst in the presence of hydrogen are useful for catalyzing the different intermediate reactions for example angelicalactone to gamma-valerolactone and gamma-valerolactone to 1,4-pentanediol. Finally, it was surprising that levulinic acid could be converted to 2-methyltetrahydrofuran with heating in the presence of the bimetallic catalyst and hydrogen in a single process vessel. The method of the present invention unexpectedly produced a fuel or fuel component having 2-methyltetrahydrofuran either in a yield greater than 4.5 mol % or in combination with alcohols.
摘要翻译：本发明基于惊人的发现，即选自4-氧代戊酸，至少一种4-氧代戊酸的内酯的5-碳化合物及其组合可以用贵金属的双金属催化剂氢化与第二金属组合并保护侧甲基。进一步出人意料地发现，在氢存在下，相同条件的双金属催化剂可用于催化不同的中间反应，例如天然内酯至γ-戊内酯和γ-戊内酯至1,4-戊二醇。最后，令人惊讶的是，在双金属催化剂和氢气存在下，乙酰丙酸可以在单一工艺容器中加热转化为2-甲基四氢呋喃。本发明的方法意外地产生具有2-甲基四氢呋喃的燃料或燃料组分，其产率大于4.5mol％或与醇组合。

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