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1. 发明授权

US5482812A Wax Containing toner aggregation processes 失效
标题翻译：蜡含有调色剂聚集工艺
公开(公告)号：US5482812A
公开(公告)日：1996-01-09
申请号：US344060
申请日：1994-11-23
申请人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Stephan V. Drappel , Paul J. Gerroir
发明人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Stephan V. Drappel , Paul J. Gerroir
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/0815
摘要： A process for the preparation of toner compositions or toner particles comprising:(i) providing an aqueous pigment dispersion comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) providing a wax dispersion comprised of wax, a dispersant comprised of nonionic surfactant, ionic surfactant or mixtures thereof;(iii) shearing a mixture of the wax dispersion and the pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant;(iv) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(v) adding additional ionic surfactant to the aggregated suspension of (iv) to ensure that no, or minimal additional particle growth of the electrostatically bound toner size aggregates occurs on further increasing the temperature to coalesce the aggregates into toner particles (vi);(vi) heating the mixture of (v) with bound aggregates above about or at the Tg of the resin; and optionally(vii) separating the toner particles from the aqueous slurry by filtration and thereafter optionally washing.
摘要翻译：一种制备调色剂组合物或调色剂颗粒的方法，包括：（i）提供由颜料，离子表面活性剂和任选的电荷控制剂组成的水性颜料分散体; （ii）提供由蜡组成的蜡分散体，由非离子表面活性剂，离子表面活性剂或其混合物组成的分散剂; （iii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂组成的胶乳或乳液共混物来剪切蜡分散体和颜料分散体的混合物; （iv）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （v）向（iv）的聚集悬浮液中加入另外的离子表面活性剂，以确保在进一步升高温度以使聚集体聚结成调色剂颗粒（vi）时，静电结合的调色剂尺寸聚集体不会发生或最小的附加颗粒生长。（vi）将（v）混合物加热至高于树脂Tg或高于Tg的结合聚集体; 并且任选地（vii）通过过滤从调色剂颗粒与含水浆料分离，然后任选地洗涤。

2. 发明授权

US5501935A Toner aggregation processes 失效
标题翻译：调色剂聚合过程
公开(公告)号：US5501935A
公开(公告)日：1996-03-26
申请号：US373806
申请日：1995-01-17
申请人： Raj D. Patel , Michael A. Hopper , Paul J. Gerroir , Grazyna E. Kmiecik-Lawrynowicz
发明人： Raj D. Patel , Michael A. Hopper , Paul J. Gerroir , Grazyna E. Kmiecik-Lawrynowicz
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/08706 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/09733 , G03G9/0975
摘要： A process for the preparation of toner compositions consisting essentially of(i) preparing a pigment dispersion, which dispersion is comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant, and a nonionic surfactant;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(iv) subsequently adding further anionic or nonionic surfactant solution to minimize further growth in the coalescence (v); and(v) heating said bound aggregates above about the Tg of the resin and wherein said heating is from a temperature of about 103.degree. to about 120.degree. C., and wherein said toner compositions are spherical in shape.
摘要翻译：一种制备调色剂组合物的方法，其基本上由（i）制备颜料分散体组成，该分散体由颜料，离子表面活性剂和任选的电荷控制剂组成; （ii）用由树脂，具有与所述离子表面活性剂相反的电荷极性的反离子表面活性剂和非离子表面活性剂组成的胶乳或乳液共混物剪切所述颜料分散体; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （iv）随后加入其它阴离子或非离子表面活性剂溶液以最小化聚结中的进一步生长（v）; 和（v）在所述树脂的Tg附近加热所述结合的聚集体，并且其中所述加热温度为约103℃至约120℃，并且其中所述调色剂组合物的形状为球形。

3. 发明授权

US5763133A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5763133A
公开(公告)日：1998-06-09
申请号：US825451
申请日：1997-03-28
申请人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) an aqueous pigment dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said pigment dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的水性颜料分散体与（b）由线性聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和在所述颜料分散体中具有与所述第一离子型表面活性剂相反的电荷极性的第二离子表面活性剂; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg，以实现所述聚集体的熔融或聚结。

4. 发明授权

US5747215A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5747215A
公开(公告)日：1998-05-05
申请号：US841300
申请日：1997-04-29
申请人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) a colorant dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said colorant dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates, and wherein said linear polymer is of an M.sub.w of from about 20,000 to about 40,000.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的着色剂分散体与（b）由直链聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和第二离子表面活性剂，其电荷极性与所述着色剂分散体中所述第一离子表面活性剂的极性相反; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg以实现所述聚集体的熔融或聚结，并且其中所述线性聚合物的Mw为约20,000至约40,000。

5. 发明授权

US5936008A Ink jet inks containing toner particles as colorants 失效
标题翻译：含有调色剂颗粒作为着色剂的喷墨油墨
公开(公告)号：US5936008A
公开(公告)日：1999-08-10
申请号：US560783
申请日：1995-11-21
申请人： Robert N. Jones , Edward J. Radigan, Jr. , Susan Robinette , Raj D. Patel , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Garland J. Nichols , Beng S. Ong
发明人： Robert N. Jones , Edward J. Radigan, Jr. , Susan Robinette , Raj D. Patel , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Garland J. Nichols , Beng S. Ong
IPC分类号： B41J2/01 , B41M5/00 , C09D11/00 , C09D11/10
CPC分类号： C09D11/32 , Y10S260/38
摘要： An ink for ink jet printing includes a liquid vehicle comprising water and toner particles with a colorant dispersed in or associated with the toner particles. The ink composition combines the print quality advantages of xerographic printing with the economic advantages of ink jet printing, thereby providing waterfast, archival quality prints.
摘要翻译：用于喷墨印刷的油墨包括液体载体，其包含水和具有分散在调色剂颗粒中或与调色剂颗粒相关联的着色剂的调色剂颗粒。油墨组合物将静电印刷的印刷质量优点与喷墨印刷的经济优点相结合，从而提供耐水性，档案质量的印刷品。

6. 发明授权

US5604076A Toner compositions and processes thereof 失效
标题翻译：调色剂组合物及其工艺
公开(公告)号：US5604076A
公开(公告)日：1997-02-18
申请号：US595143
申请日：1996-02-01
申请人： Raj D. Patel , Guerino G. Sacripante , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Francisco E. Torres
发明人： Raj D. Patel , Guerino G. Sacripante , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Francisco E. Torres
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/0806
摘要： A process for the preparation of toner compositions comprising:(i) preparing a latex or emulsion resin comprised of a polyester core encapsulated within a styrene based resin shell by heating said polyester emulsion containing an anionic surfactant with a mixture of monomers of styrene and acrylic acid, and with potassium persulfate, ammonium persulfate, sodium bisulfite, or mixtures thereof;(ii) adding a pigment dispersion, which dispersion is comprised of a pigment, a cationic surfactant, and optionally a charge control agent, followed by the sharing of the resulting blend;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution; and(iv) heating said electrostatically bound aggregates above about the Tg of the resin.
摘要翻译：一种制备调色剂组合物的方法，包括：（i）通过将含有阴离子表面活性剂的聚酯乳液与苯乙烯和丙烯酸的单体混合物加热，制备由包封在苯乙烯基树脂壳内的聚酯芯构成的胶乳或乳液树脂和过硫酸钾，过硫酸铵，亚硫酸氢钠或其混合物; （ii）添加颜料分散体，该分散体由颜料，阳离子表面活性剂和任选的电荷控制剂组成，然后共享所得共混物; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; 和（iv）将所述静电结合的聚集体加热到高于树脂的Tg的高度。

7. 发明授权

US5514763A Styrene/butadiene toner resins with excellent gloss and fix properties 失效
标题翻译：苯乙烯/丁二烯调色剂树脂具有优异的光泽和固定性能
公开(公告)号：US5514763A
公开(公告)日：1996-05-07
申请号：US312196
申请日：1994-09-26
申请人： Grazyna E. Kmiecik-Lawrynowicz , T. Brian McAneney , Raj D. Patel , Michael A. Hopper , David J. Sanders
发明人： Grazyna E. Kmiecik-Lawrynowicz , T. Brian McAneney , Raj D. Patel , Michael A. Hopper , David J. Sanders
IPC分类号： C08F212/08 , G03G9/087 , C08F236/06 , G03G9/08 , G03G9/09
CPC分类号： C08F212/08 , G03G9/08706 , G03G9/08797
摘要： A toner composition includes a styrene/butadiene resin having a weight average molecular weight of less than about 70,000 and a number average molecular weight of from about 8,000 to about 12,000, has a glass transition temperature of from about 50.degree. C. to about 60.degree. C. and provides excellent gloss and high fix properties at a low fusing temperature. The styrene/butadiene resin is produced by an emulsion polymerization process that includes forming an emulsion of a surfactant, styrene monomer, butadiene monomer and a water-soluble monomer in water, and then polymerizing the monomers in the presence of a water-soluble initiator.
摘要翻译：调色剂组合物包括重均分子量小于约70,000并且数均分子量为约8,000至约12,000的苯乙烯/丁二烯树脂的玻璃化转变温度为约50℃至约60℃ 并且在低定影温度下提供优异的光泽度和高固定性。苯乙烯/丁二烯树脂通过乳液聚合方法制备，其包括在水中形成表面活性剂，苯乙烯单体，丁二烯单体和水溶性单体的乳液，然后在水溶性引发剂的存在下使单体聚合。

8. 发明授权

US5977210A Modified emulsion aggregation processes 失效
标题翻译：改性乳液聚集方法
公开(公告)号：US5977210A
公开(公告)日：1999-11-02
申请号：US380550
申请日：1995-01-30
申请人： Raj D. Patel , Marcel P. Breton , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Beng S. Ong
发明人： Raj D. Patel , Marcel P. Breton , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Beng S. Ong
IPC分类号： C08F2/26 , C09D11/00
CPC分类号： C09D11/30 , C08F2/26 , Y10S977/902
摘要： A process for the preparation of ink compositions comprising the emulsion polymerization of monomer, water, surfactant, and initiator with stirring and heating to provide a latex; mixing therewith a pigment dispersion of pigment particles, water, and cationic surfactant; blending the mixture; thereafter stirring the mixture; and subsequently adding additional anionic surfactant to stabilize the aggregate particles.
摘要翻译：一种制备油墨组合物的方法，包括在搅拌和加热下单体，水，表面活性剂和引发剂的乳液聚合以提供胶乳; 与颜料颗粒，水和阳离子表面活性剂的颜料分散体混合; 混合混合物然后搅拌混合物; 并随后加入另外的阴离子表面活性剂以稳定聚集体颗粒。

9. 发明授权

US5525452A Toner aggregation processes 失效
标题翻译：调色剂聚合过程
公开(公告)号：US5525452A
公开(公告)日：1996-06-11
申请号：US497988
申请日：1995-07-03
申请人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
发明人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0815 , G03G9/0804
摘要： A process for the preparation of toner compositions comprising (i) preparing a pigment dispersion in water, which dispersion is comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) shearing said pigment dispersion with an aqueous latex or emulsion blend comprised of a nonionic surfactant, resin, and a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(iv) heating the electrostatically bound aggregates above about the Tg of the resin, which heating is accomplished at a pH of from about 4.0 to about 6.0 while continuously stirring the electrostatically bound aggregates to form toner particles;(v) washing the toner particles with a basic aqueous solution, which solution is of a pH of from between about 10.0 and about 12.0; and thereafter optionally(iv) separating the toner particles from the emulsion blend containing water by filtration and then drying the toner particles.
摘要翻译：一种制备调色剂组合物的方法，包括（i）在水中制备颜料分散体，该分散体由颜料，离子表面活性剂和任选的电荷控制剂组成; （ii）用包含非离子表面活性剂，树脂和抗衡离子表面活性剂的水性胶乳或乳液共混物剪切所述颜料分散体，其电荷极性与所述离子表面活性剂相反; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （iv）将高于约树脂Tg的静电结合聚集体加热，在约4.0至约6.0的pH下进行加热，同时连续搅拌静电结合的聚集体以形成调色剂颗粒; （v）用碱性水溶液洗涤调色剂颗粒，该溶液的pH为约10.0至约12.0; 然后任选地（iv）通过过滤从含有水的乳液共混物中分离调色剂颗粒，然后干燥调色剂颗粒。

10. 发明授权

US5370964A Toner aggregation process 失效
标题翻译：调色剂聚合过程
公开(公告)号：US5370964A
公开(公告)日：1994-12-06
申请号：US158343
申请日：1993-11-29
申请人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Melvin D. Croucher , T. Hwee Ng , William J. Dale
发明人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Melvin D. Croucher , T. Hwee Ng , William J. Dale
IPC分类号： G03G9/08
CPC分类号： G03G9/0815 , G03G9/0804
摘要： A process for the preparation of toner comprising:(i) preparing a pigment dispersion in water, which dispersion is comprised of pigment, an ionic surfactant, and an optional charge control agent;(ii) shearing the pigment dispersion with a polymeric latex comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant, and which latex contains a nonionic surfactant thereby forming a homogeneous or a uniform blend;(iii) heating the above sheared homogeneous blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates;(iv) reshearing the above electrostatically bound toner aggregates (iii) to fragment or break down said toner aggregates of (iii) into smaller average diameter particle size;(v) heating the resulting formed sheared homogeneous blend (iv) comprised of resin, pigment particles, and the ionic, counterionic and nonionic surfactants in water below about the glass transition temperature (Tg) of the resin while continuously stirring at about 450 to about 800 revolutions per minute to form electrostatically bound toner size aggregates with a narrow particle size distribution;(vi) adding further ionic or nonionic surfactant in an amount of from about 0.1 to about 10 percent by weight of water to minimize further growth or enlargement of the particles in the coalescence step (vii); and(vii) heating the formed statically bound aggregated particles of (vi) about above the Tg of the resin to provide coalesced particles of toner(viii) separating said toner; and(ix) drying said toner.
摘要翻译：一种制备调色剂的方法，包括：（i）在水中制备颜料分散体，该分散体由颜料，离子表面活性剂和任选的电荷控制剂组成; （ii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂的聚合胶乳剪切颜料分散体，并且该胶乳含有非离子表面活性剂，从而形成均匀或均匀的共混物; （iii）在树脂的玻璃化转变温度（Tg）附近加热上述剪切均匀混合物以形成静电结合的调色剂尺寸聚集体; （iv）重新研磨上述静电结合的调色剂聚集体（iii）以将（iii）的所述调色剂聚集体碎裂或分解成更小的平均直径粒径; （v）在低于约玻璃化转变温度（Tg）的树脂下，将所形成的由树脂，颜料颗粒和离子型，抗衡离子和非离子表面活性剂组成的剪切的均匀混合物（iv）加热至约450至约 800转/分钟，形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （vi）以约0.1至约10重量％的水加入另外的离子或非离子表面活性剂以最小化在聚结步骤（vii）中颗粒的进一步生长或增大; （vii）将所形成的静态结合的（vi）聚集的颗粒加热到树脂的Tg附近，以提供聚结的调色剂颗粒（viii）分离所述调色剂; 和（ix）干燥所述调色剂。

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