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1. 发明授权

US5936008A Ink jet inks containing toner particles as colorants 失效
标题翻译：含有调色剂颗粒作为着色剂的喷墨油墨
公开(公告)号：US5936008A
公开(公告)日：1999-08-10
申请号：US560783
申请日：1995-11-21
申请人： Robert N. Jones , Edward J. Radigan, Jr. , Susan Robinette , Raj D. Patel , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Garland J. Nichols , Beng S. Ong
发明人： Robert N. Jones , Edward J. Radigan, Jr. , Susan Robinette , Raj D. Patel , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Garland J. Nichols , Beng S. Ong
IPC分类号： B41J2/01 , B41M5/00 , C09D11/00 , C09D11/10
CPC分类号： C09D11/32 , Y10S260/38
摘要： An ink for ink jet printing includes a liquid vehicle comprising water and toner particles with a colorant dispersed in or associated with the toner particles. The ink composition combines the print quality advantages of xerographic printing with the economic advantages of ink jet printing, thereby providing waterfast, archival quality prints.
摘要翻译：用于喷墨印刷的油墨包括液体载体，其包含水和具有分散在调色剂颗粒中或与调色剂颗粒相关联的着色剂的调色剂颗粒。油墨组合物将静电印刷的印刷质量优点与喷墨印刷的经济优点相结合，从而提供耐水性，档案质量的印刷品。

2. 发明授权

US06096927A Process for removal and recovery of an arylamine compound 有权
标题翻译：芳胺化合物的除去和回收方法
公开(公告)号：US06096927A
公开(公告)日：2000-08-01
申请号：US365486
申请日：1999-08-02
申请人： Satish R. Parikh , Edward J. Radigan, Jr. , Anthony M. Horgan , John A. Bergfjord, Sr.
发明人： Satish R. Parikh , Edward J. Radigan, Jr. , Anthony M. Horgan , John A. Bergfjord, Sr.
IPC分类号： C07C209/86 , C07C211/50 , C07C211/00
CPC分类号： C07C209/86
摘要： A process for recovery of N,N'-bis(alkylphenyl)-[1,1'-biphenyl]-4,4'-diamine from an electrophotographic imaging member, the process includingproviding an electrophotographic imaging member including at least one imaging layer, the imaging layer including a film forming binder and N,N'-bis(alkylphenyl)[1,1'-biphenyl]-4,4'-diamine,contacting the at least one imaging layer with warm toluene to dissolve toluene soluble materials including the film forming binder and N,N'-bis(alkylphenyl)-[1,1'-biphenyl]-4,4'-diamine to form a mixture containing undissolved material and a solution of toluene and the toluene soluble materials,isolating the solution from the undissolved material,concentrating the solution in a partial vacuum and with applied heat,cooling the concentrate,mixing the concentrate with acetone to precipitate the N,N'-bis(alkylphenyl)-[1,1'-biphenyl]-4,4'-diamine,separating the N,N'-bis(alkylphenyl)-[1,1'-biphenyl]-4,4'-diamine precipitate from the concentrate,washing the N,N'-bis(alkylphenyl)-[1,1'-biphenyl]-4,4'-diamine precipitate with acetone,drying the N,N'-bis(alkylphenyl)-[1,1'-biphenyl]-4,4'-diamine precipitate,and purifying the N,N'-bis(alkylphenyl)-[1,1'-biphenyl]-4,4'-diamine precipitate.
摘要翻译：一种从电子照相成像部件回收N，N'-双（烷基苯基） - [1,1'-联苯] -4,4'-二胺的方法，该方法包括提供电子照相成像部件，其包括至少一个成像层，成像层包括成膜粘合剂和N，N'-双（烷基苯基）[1,1'-联苯] -4,4'-二胺，使至少一个成像层与热甲苯接触以溶解甲苯可溶物包括成膜粘合剂和N，N'-双（烷基苯基） - [1,1'-联苯] -4,4'-二胺以形成含有未溶解材料的混合物和甲苯和甲苯可溶物质的溶液，来自未溶解材料的溶液，将溶液浓缩在部分真空中并加热，冷却浓缩物，将浓缩物与丙酮混合以沉淀N，N'-双（烷基苯基） - [1,1'-联苯] - 4,4'-二胺，从浓缩物中分离出N，N'-双（烷基苯基） - [1,1'-联苯] -4,4'-二胺沉淀物，洗涤 N，N'-双（烷基苯基） - [1,1'-联苯] -4,4'-二胺与丙酮沉淀，干燥N，N'-双（烷基苯基） - [1,1'-联苯基] - 4,4'-二胺沉淀，纯化N，N'-双（烷基苯基） - [1,1'-联苯] -4,4'-二胺沉淀。

3. 发明授权

US5772744A Ink compositions for thermal ink printing 失效
标题翻译：用于热油墨印刷的油墨组合物
公开(公告)号：US5772744A
公开(公告)日：1998-06-30
申请号：US961335
申请日：1997-10-30
申请人： Kurt B. Gundlach , Richard L. Colt , Edward J. Radigan, Jr.
发明人： Kurt B. Gundlach , Richard L. Colt , Edward J. Radigan, Jr.
IPC分类号： B41J2/01 , B41M5/00 , C09D11/00 , C09D11/02
CPC分类号： C09D11/38
摘要： Disclosed is an ink composition which comprises water, a colorant, betaine, a tertiary amine, and a material of the formula �(F.sub.2n+1 C.sub.n CH.sub.2 S).sub.2 (CH.sub.3)C--CH.sub.2 CH.sub.2 COO.sup.- !�B.sup.+ !, wherein n is an integer of from about 8 to about 20 and B is a cation. In one specific embodiment, n is 10 and B is (HO--CH.sub.2 CH.sub.2).sub.2 NH.sub.3.sup.+. In another specific embodiment, the tertiary amine is 1-methylimidazole. In yet another specific embodiment of the present invention, the colorant is an anionic dye with carboxylate groups, sulfonate groups, or both carboxylate and sulfonate groups. Also disclosed is a process for preparing the aforementioned ink composition wherein a liquid containing the material of the formula �(F.sub.2n+1 CnCH.sub.2 S).sub.2 (CH.sub.3)C--CH.sub.2 CH.sub.2 COO.sup.- !�B.sup.+ ! is subjected to centrifugation. Also disclosed are ink jet printing processes employing the aforementioned ink.
摘要翻译：公开了一种油墨组合物，其包含水，着色剂，甜菜碱，叔胺和式[（F2n + 1CnCH2S）2（CH3）C-CH2CH2COO - ] [B +]的材料，其中n为约8至约20，B为阳离子。在一个具体实施方案中，n为10，B为（HO-CH 2 CH 2）2 NH 3 +。在另一个具体实施方案中，叔胺是1-甲基咪唑。在本发明的另一个具体实施方案中，着色剂是具有羧酸酯基，磺酸酯基团或羧酸酯基和磺酸酯基团的阴离子染料。还公开了制备上述油墨组合物的方法，其中将含有式[（F2n + 1CnCH2S）2（CH3）C-CH2CH2COO - ] [B +]的物质的液体进行离心。还公开了采用上述油墨的喷墨印刷方法。

4. 发明授权

US07592110B2 Polyhydroxy siloxane photoconductors 失效
标题翻译：多羟基硅氧烷感光体
公开(公告)号：US07592110B2
公开(公告)日：2009-09-22
申请号：US11705932
申请日：2007-02-13
申请人： Kenny-Tuan Dinh , John F. Yanus , Raymond K. Crandall , Edward J. Radigan, Jr.
发明人： Kenny-Tuan Dinh , John F. Yanus , Raymond K. Crandall , Edward J. Radigan, Jr.
IPC分类号： G03G7/00
CPC分类号： G03G5/0542 , G03G5/0546 , G03G5/0578 , G03G5/0614 , G03G5/0618 , G03G5/14708 , G03G5/14773
摘要： An imaging member including an optional supporting substrate, a photogenerating layer, and at least one charge transport layer comprised of at least one charge transport component, and an overcoating layer in contact with and contiguous to the charge transport, and which overcoating is comprised of an acrylated polyol, a polyalkylene glycol, a crosslinking agent, a hydroxy functionalized siloxane and a charge transport component.
摘要翻译：一种成像构件，其包括任选的支撑衬底，光生成层以及至少一个电荷传输层，所述至少一个电荷传输层包括至少一个电荷传输组件，以及与所述电荷传输接触并邻近所述电荷传输的外涂层，以及所述外涂层由丙烯酸酯化多元醇，聚亚烷基二醇，交联剂，羟基官能化硅氧烷和电荷输送组分。

5. 发明授权

US6001899A Ink compositions with improved waterfastness and smear resistance 失效
标题翻译：具有改善耐水性和耐沾污性的油墨组合物
公开(公告)号：US6001899A
公开(公告)日：1999-12-14
申请号：US047097
申请日：1998-03-24
申请人： Kurt B. Gundlach , Richard L. Colt , Luis A. Sanchez , Maura A. Sweeney , Edward J. Radigan, Jr.
发明人： Kurt B. Gundlach , Richard L. Colt , Luis A. Sanchez , Maura A. Sweeney , Edward J. Radigan, Jr.
IPC分类号： C09D11/00 , C09D179/04 , C09D11/02 , C09D11/10
CPC分类号： C09D11/30 , C09D179/04
摘要： Disclosed is an ink composition which comprises water, an anionic dye, and a polyquaternary amine compound selected from the group consisting of polydiallyl ammonium compounds, polyquaternized polyvinylamines, polyquaternized polyallylamines, and mixtures thereof. Also disclosed are methods for using the aforementioned ink composition in ink jet printing processes.
摘要翻译：公开了一种油墨组合物，其包含水，阴离子染料和选自聚二烯丙基铵化合物，聚季铵化聚乙烯胺，聚季铵化聚烯丙基胺及其混合物的聚季胺化合物。还公开了在喷墨印刷方法中使用上述油墨组合物的方法。

6. 发明授权

US5389133A Ink compositions for ink jet printing 失效
标题翻译：用于喷墨印刷的油墨组合物
公开(公告)号：US5389133A
公开(公告)日：1995-02-14
申请号：US227828
申请日：1994-04-14
申请人： Kurt B. Gundlach , Richard L. Colt , Edward J. Radigan, Jr. , William M. Schwarz , Julia A. Kohlmeier
发明人： Kurt B. Gundlach , Richard L. Colt , Edward J. Radigan, Jr. , William M. Schwarz , Julia A. Kohlmeier
IPC分类号： C09D11/00 , C09D11/02
CPC分类号： C09D11/38
摘要： Disclosed is a process for preparing an aqueous ink composition which comprises adjusting the pH of the ink with phosphorous acid or phosphite salts. Also disclosed are ink compositions prepared by this process. In certain preferred embodiments, the ink compositions can also contain betaine, sulfolane, dimethyl sulfoxide, or N,N'-bis(3-aminopropyl)-1,2-ethylenediamine, as well as mixtures thereof. In other preferred embodiments, the ink composition comprises an organic component selected from the group consisting of sulfolane, dimethyl sulfoxide, and mixtures thereof, and anions selected from the group consisting of phosphite, hypophosphite, phosphate, polyphosphate, sulfate, hexafluorophosphate, glycolate, acetate, ethylenediaminetetraacetate, formate, borate, sulfite, sulfamate, and mixtures thereof.
摘要翻译：公开了一种制备水性油墨组合物的方法，其包括用亚磷酸或亚磷酸盐调节油墨的pH。还公开了通过该方法制备的油墨组合物。在某些优选实施方案中，油墨组合物还可以含有甜菜碱，环丁砜，二甲基亚砜或N，N'-双（3-氨基丙基）-1,2-乙二胺，以及它们的混合物。在其它优选实施方案中，油墨组合物包含选自环丁砜，二甲基亚砜及其混合物的有机组分和选自亚磷酸盐，次磷酸盐，磷酸盐，多磷酸盐，硫酸盐，六氟磷酸盐，乙醇酸盐，乙酸盐乙二胺四乙酸盐，甲酸盐，硼酸盐，亚硫酸盐，氨基磺酸盐及其混合物。

7. 发明授权

US5772743A Ink compositions for thermal ink jet printing 失效
标题翻译：用于热喷墨印刷的油墨组合物
公开(公告)号：US5772743A
公开(公告)日：1998-06-30
申请号：US961435
申请日：1997-10-30
申请人： Kurt B. Gundlach , Luis A. Sanchez , Cheryl A. Hanzlik , Kathy-Jo Brodsky , Richard L. Colt , Aileen M. Montes , Edward J. Radigan, Jr.
发明人： Kurt B. Gundlach , Luis A. Sanchez , Cheryl A. Hanzlik , Kathy-Jo Brodsky , Richard L. Colt , Aileen M. Montes , Edward J. Radigan, Jr.
IPC分类号： B41J2/215 , B41M5/00 , C09D11/00 , C09D11/02
CPC分类号： C09D11/38
摘要： Disclosed is an ink composition which comprises (a) water, (b) a colorant, (c) a fluorinated material selected from: (1) those of the formula �(F.sub.2n+1 C.sub.n CH.sub.2 S).sub.2 (CH.sub.3)C--CH.sub.2 CH.sub.2 COO.sup.- !�B.sup.+ !, wherein n is an integer of from about 8 to about 20 and B is a cation, (2) those of the formula �(F.sub.3 C(F.sub.2 C).sub.n CH.dbd.CHCH.sub.2 OCH(OH)CH.sub.2).sub.2 NCH.sub.2 COO.sup.- !�X.sup.+ !, wherein X is a cation and n is an integer of from about 3 to about 20, and (3) mixtures thereof, and (d) a monomeric compound having at least two carboxylic acid functional groups. Also disclosed is a process for preparing said ink composition which comprises (i) admixing the ink ingredients, and (ii) subjecting the mixture thus formed to ultrasonification, thereby reducing the average particle diameter of liposomes of the fluorinated material in the ink. Further disclosed is a process which entails (i) incorporating into an ink jet printing apparatus the aforementioned ink composition, and (ii) causing droplets of the ink composition to be ejected in an imagewise pattern onto a substrate. In a preferred embodiment, the printing apparatus employs a thermal ink jet process wherein the ink in the nozzles is selectively heated in an imagewise pattern, thereby causing droplets of the ink to be ejected in imagewise pattern.
摘要翻译：公开了一种油墨组合物，其包含（a）水，（b）着色剂，（c）选自以下的氟化材料：（1）式[（F2n + 1CnCH2S）2（CH3）C-CH2CH2COO - ] [ B +]，其中n为约8至约20的整数，B为阳离子，（2）式[（F3C（F2C）nCH = CHCH2OCH（OH）CH2）2NCH2COO - ] [X +]的那些，其中 X是阳离子，n是约3至约20的整数，和（3）它们的混合物，和（d）具有至少两个羧酸官能团的单体化合物。还公开了一种制备所述油墨组合物的方法，其包括（i）混合油墨成分，和（ii）使由此形成的混合物经过超声处理，从而降低油墨中氟化材料的脂质体的平均粒径。进一步公开的方法是（i）将上述油墨组合物结合到喷墨打印设备中，和（ii）使油墨组合物的液滴以成像图案喷射到基材上。在优选实施例中，印刷设备采用热喷墨工艺，其中喷嘴中的油墨以成像图案选择性加热，从而使油墨的液滴以成像图案喷射。

8. 发明授权

US5554213A Ink compositions for ink jet printing 失效
标题翻译：用于喷墨印刷的油墨组合物
公开(公告)号：US5554213A
公开(公告)日：1996-09-10
申请号：US347937
申请日：1994-12-01
申请人： Edward J. Radigan, Jr. , Richard L. Colt , Kurt B. Gundlach , Miguel A. Fontanez
发明人： Edward J. Radigan, Jr. , Richard L. Colt , Kurt B. Gundlach , Miguel A. Fontanez
IPC分类号： C09D11/00 , C09D11/02
CPC分类号： C09D11/38
摘要： Disclosed are ink compositions comprising water, a colorant, and a phosphite salt of the general formula ##STR1## wherein R, R', R" and R'" can each, independently of each other, be hydrogen, an alkyl group, a substituted alkyl group, an aryl group, or a substituted aryl group. Also disclosed is a process for preparing an ink composition which comprises admixing water, a colorant, a base, and an acid selected from the group consisting of hypophosphoric acid, hypophosphorous acid, alkyl phosphonic acids, aryl phosphonic acids, alkyl phosphinic acids, aryl phosphinic acids, and mixtures thereof, wherein the pH of the ink is adjusted by a process selected from the group consisting of (a) adding the acid to an aqueous solution containing the base, and (b) adding the base to an aqueous solution containing the acid. Further disclosed are ink compositions comprising water, a colorant, and a salt selected from the group consisting of hypophosphate salts, hypophosphite salts, alkyl phosphite salts, aryl phosphite salts, alkyl phosphonite salts, aryl phosphonite salts, and mixtures thereof.
摘要翻译：公开了包含水，着色剂和通式“IMAGE”或“IMAGE”的亚磷酸盐的油墨组合物，其中R，R'，R“和R”'各自独立地为氢，烷基，取代的烷基，芳基或取代的芳基。还公开了一种制备油墨组合物的方法，该方法包括混合水，着色剂，碱和选自由次磷酸，次磷酸，烷基膦酸，芳基膦酸，烷基次膦酸，芳基次膦酸酸及其混合物，其中通过选自（a）将酸添加到含有碱的水溶液中的方法调节油墨的pH，和（b）将碱添加到含有酸。还公开了包含水，着色剂和选自次磷酸盐，次磷酸盐，亚磷酸烷基酯，亚磷酸芳基酯，烷基亚膦酸盐，芳基亚膦酸盐及其混合物的盐的油墨组合物。

9. 发明授权

US5360472A Waterfast dye compositions 失效
标题翻译：耐水染料组合物
公开(公告)号：US5360472A
公开(公告)日：1994-11-01
申请号：US96912
申请日：1993-07-26
申请人： Edward J. Radigan, Jr. , Louis V. Isganitis , Warren E. Solodar , Kurt B. Gundlach
发明人： Edward J. Radigan, Jr. , Louis V. Isganitis , Warren E. Solodar , Kurt B. Gundlach
IPC分类号： C09D11/00 , C09D11/02
CPC分类号： C09D11/30
摘要： Disclosed are dye compositions of the formula ##STR1## wherein Cp and Cp' are each coupler compounds of the formula ##STR2## wherein the --COOH group and the --OH group can be in any position on either ring, provided that in the naphthalene ring system there is present least one hydrogen activated through resonance by the --OH group for an electrophilic aromatic substitution coupling reaction, n represents the number of substituents on the rings and is a number of from 0 to 8, and R represents the substituent groups on the ring, wherein each R is independently selected from the group consisting of hydroxyl groups, alkyl groups, substituted alkyl groups, aryl groups, substituted aryl groups, aryl-alkyl groups, substituted aryl-alkyl groups, halogen atoms, and nitro groups. Also disclosed are aqueous ink compositions containing the dyes, processes for making the dyes, processes for making the inks containing the dyes, and printing processes employing the inks.
摘要翻译：公开了下式的染料组合物，其中Cp和Cp'分别是式IMA的成色剂化合物，其中-COOH基团和-OH基团可以在任一个环上的任何位置，条件是在萘环中系统存在通过-OH基团通过亲电子芳族取代偶联反应共振而发生的至少一个氢，n表示环上的取代基的数目，为0至8的数，R表示取代基环，其中每个R独立地选自羟基，烷基，取代的烷基，芳基，取代的芳基，芳基 - 烷基，取代的芳基 - 烷基，卤素原子和硝基。还公开了含有染料的水性油墨组合物，用于制备染料的方法，制备含有染料的油墨的方法，以及采用该油墨的印刷方法。

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