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1. 发明授权

US5482812A Wax Containing toner aggregation processes 失效
标题翻译：蜡含有调色剂聚集工艺
公开(公告)号：US5482812A
公开(公告)日：1996-01-09
申请号：US344060
申请日：1994-11-23
申请人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Stephan V. Drappel , Paul J. Gerroir
发明人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Stephan V. Drappel , Paul J. Gerroir
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/0815
摘要： A process for the preparation of toner compositions or toner particles comprising:(i) providing an aqueous pigment dispersion comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) providing a wax dispersion comprised of wax, a dispersant comprised of nonionic surfactant, ionic surfactant or mixtures thereof;(iii) shearing a mixture of the wax dispersion and the pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant;(iv) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(v) adding additional ionic surfactant to the aggregated suspension of (iv) to ensure that no, or minimal additional particle growth of the electrostatically bound toner size aggregates occurs on further increasing the temperature to coalesce the aggregates into toner particles (vi);(vi) heating the mixture of (v) with bound aggregates above about or at the Tg of the resin; and optionally(vii) separating the toner particles from the aqueous slurry by filtration and thereafter optionally washing.
摘要翻译：一种制备调色剂组合物或调色剂颗粒的方法，包括：（i）提供由颜料，离子表面活性剂和任选的电荷控制剂组成的水性颜料分散体; （ii）提供由蜡组成的蜡分散体，由非离子表面活性剂，离子表面活性剂或其混合物组成的分散剂; （iii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂组成的胶乳或乳液共混物来剪切蜡分散体和颜料分散体的混合物; （iv）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （v）向（iv）的聚集悬浮液中加入另外的离子表面活性剂，以确保在进一步升高温度以使聚集体聚结成调色剂颗粒（vi）时，静电结合的调色剂尺寸聚集体不会发生或最小的附加颗粒生长。（vi）将（v）混合物加热至高于树脂Tg或高于Tg的结合聚集体; 并且任选地（vii）通过过滤从调色剂颗粒与含水浆料分离，然后任选地洗涤。

2. 发明授权

US5763133A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5763133A
公开(公告)日：1998-06-09
申请号：US825451
申请日：1997-03-28
申请人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) an aqueous pigment dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said pigment dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的水性颜料分散体与（b）由线性聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和在所述颜料分散体中具有与所述第一离子型表面活性剂相反的电荷极性的第二离子表面活性剂; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg，以实现所述聚集体的熔融或聚结。

3. 发明授权

US5747215A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5747215A
公开(公告)日：1998-05-05
申请号：US841300
申请日：1997-04-29
申请人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) a colorant dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said colorant dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates, and wherein said linear polymer is of an M.sub.w of from about 20,000 to about 40,000.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的着色剂分散体与（b）由直链聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和第二离子表面活性剂，其电荷极性与所述着色剂分散体中所述第一离子表面活性剂的极性相反; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg以实现所述聚集体的熔融或聚结，并且其中所述线性聚合物的Mw为约20,000至约40,000。

4. 发明授权

US06562541B2 Toner processes 失效
公开(公告)号：US06562541B2
公开(公告)日：2003-05-13
申请号：US09960425
申请日：2001-09-24
申请人： Daryl Vanbesien , Raj D. Patel , Michael A. Hopper , Stephan V. Drappel
发明人： Daryl Vanbesien , Raj D. Patel , Michael A. Hopper , Stephan V. Drappel
IPC分类号： C08J3215
CPC分类号： G03G9/0804 , G03G9/0806
摘要： A process for the preparation of toner by, for example, mixing a latex with a colorant mixture comprised of colorant, an ionic surfactant, and a polytetrafluoroethylene; adding a coagulant; heating the resulting mixture below about the glass transition temperature (Tg) of the latex resin; adding a stabilizer; heating above about the Tg of the latex resin; and isolating the toner.

5. 发明授权

US06899987B2 Toner processes 失效
标题翻译：墨粉处理
公开(公告)号：US06899987B2
公开(公告)日：2005-05-31
申请号：US10393635
申请日：2003-03-20
申请人： Daryl Vanbesien , Raj D. Patel , Michael A. Hopper , Stephan V. Drappel
发明人： Daryl Vanbesien , Raj D. Patel , Michael A. Hopper , Stephan V. Drappel
IPC分类号： G03G9/08 , C03J3/215
CPC分类号： G03G9/0804 , G03G9/0806
摘要： A process for the preparation of toner by, for example, mixing a latex with a colorant mixture comprised of colorant, an ionic surfactant, and a polytetrafluoroethylene; adding a coagulant; heating the resulting mixture below about the glass transition temperature (Tg) of the latex resin; adding a stabilizer; heating above about the Tg of the latex resin; and isolating the toner.
摘要翻译：通过例如将胶乳与由着色剂，离子表面活性剂和聚四氟乙烯组成的着色剂混合物混合来制备调色剂的方法; 加入凝结剂; 将所得混合物加热至胶乳树脂的玻璃化转变温度（Tg）以下; 添加稳定剂; 加热高于胶乳树脂的Tg; 并分离调色剂。

6. 发明授权

US07494757B2 Ultra low melt toners comprised of crystalline resins 有权
标题翻译：由结晶树脂组成的超低熔体调色剂
公开(公告)号：US07494757B2
公开(公告)日：2009-02-24
申请号：US11089149
申请日：2005-03-25
申请人： Guerino G. Sacripante , Ke Zhou , Michael S. Hawkins , Kimberly D. Nosella , Edward G. Zwartz , Nicoleta D. Mihai , Valerie M. Farrugia , Stephan V. Drappel , Paul J. Gerroir
发明人： Guerino G. Sacripante , Ke Zhou , Michael S. Hawkins , Kimberly D. Nosella , Edward G. Zwartz , Nicoleta D. Mihai , Valerie M. Farrugia , Stephan V. Drappel , Paul J. Gerroir
IPC分类号： G03G9/087
CPC分类号： G03G9/08755 , G03G9/081 , G03G9/08791 , G03G9/08795 , G03G9/08797
摘要： A toner having an amorphous resin, a crystalline resin, and a colorant, wherein the crystalline resin has a melting temperature of at least 70° C. and a recrystallization point of at least 47° C. exhibits improved document offset properties and improved heat cohesion. Annealing the toner further improves the heat cohesion and morphology of the toner.
摘要翻译：具有无定形树脂，结晶性树脂和着色剂的调色剂，其中结晶性树脂的熔融温度为70℃以上，再结晶点为47℃以上，表现出改善的文件偏移性和改善的热粘合性。使调色剂退火进一步提高了调色剂的热粘合性和形态。

7. 发明授权

US07723004B2 Ultra low melt toners comprised of crystalline resins 失效
标题翻译：由结晶树脂组成的超低熔体调色剂
公开(公告)号：US07723004B2
公开(公告)日：2010-05-25
申请号：US12353863
申请日：2009-01-14
申请人： Guerino G. Sacripante , Ke Zhou , Michael S. Hawkins , Kimberly D. Nosella , Edward G. Zwartz , Nicoleta D. Mihai , Valerie M. Farrugia , Stephan V. Drappel , Paul J. Gerroir
发明人： Guerino G. Sacripante , Ke Zhou , Michael S. Hawkins , Kimberly D. Nosella , Edward G. Zwartz , Nicoleta D. Mihai , Valerie M. Farrugia , Stephan V. Drappel , Paul J. Gerroir
IPC分类号： G03G9/087
CPC分类号： G03G9/08755 , G03G9/081 , G03G9/08791 , G03G9/08795 , G03G9/08797
摘要： A toner having an amorphous resin, a crystalline resin, and a colorant, wherein the crystalline resin has a melting temperature of at least 70° C. and a recrystallization point of at least 47° C. exhibits improved document offset properties and improved heat cohesion. Annealing the toner further improves the heat cohesion and morphology of the toner.
摘要翻译：具有无定形树脂，结晶性树脂和着色剂的调色剂，其中结晶性树脂的熔融温度为70℃以上，再结晶点为47℃以上，表现出改善的文件偏移性和改善的热粘合性。使调色剂退火进一步提高了调色剂的热粘合性和形态。

8. 发明授权

US07686939B2 Crystalline wax 有权
标题翻译：结晶蜡
公开(公告)号：US07686939B2
公开(公告)日：2010-03-30
申请号：US11273798
申请日：2005-11-14
申请人： Raj D. Patel , David J. Sanders , T Hwee Ng , Stephan V. Drappel , Sandra J. Gardner , Sonja Hadzidedic , Louis V. Isganitis , Timothy L. Lincoln , Kevin F. Marcell
发明人： Raj D. Patel , David J. Sanders , T Hwee Ng , Stephan V. Drappel , Sandra J. Gardner , Sonja Hadzidedic , Louis V. Isganitis , Timothy L. Lincoln , Kevin F. Marcell
IPC分类号： C10G73/36
CPC分类号： C08F10/02 , C08F6/04 , C08F10/06 , C08F110/02 , C08F110/06 , G03G9/08782 , G03G9/08795 , G03G9/08797 , C08L23/12 , C08L23/06 , C08F2500/03 , C08F2500/20 , C08F2500/23
摘要： Embodiments include a fractionated and/or distilled wax having from about 30 to about 64 carbon units, a degree of crystallinity as calculated by heat of melting and as measured by DSC of from about 55 to about 100, a Mw is from about 500 to about 800, and a polydispersity of from about 1 to about 1.05.
摘要翻译：实施方案包括具有约30至约64个碳单元的分馏和/或蒸馏的蜡，通过熔化热计算的结晶度，并且通过DSC测量为约55至约100，Mw为约500至约 800，多分散性为约1至约1.05。

9. 发明授权

US07662272B2 Crystalline wax 有权
标题翻译：结晶蜡
公开(公告)号：US07662272B2
公开(公告)日：2010-02-16
申请号：US11273895
申请日：2005-11-14
申请人： Raj D. Patel , David J. Sanders , T Hwee Ng , Stephan V. Drappel , Sandra J. Gardner , Sonja Hadzidedic , Timothy L. Lincoln , Kevin F. Marcell , Louis V. Isganitis
发明人： Raj D. Patel , David J. Sanders , T Hwee Ng , Stephan V. Drappel , Sandra J. Gardner , Sonja Hadzidedic , Timothy L. Lincoln , Kevin F. Marcell , Louis V. Isganitis
IPC分类号： C10G73/36
CPC分类号： G03G9/08782 , C08F6/04 , C08L23/04 , C08L25/14 , C08L91/06 , C08L2666/02
摘要： Embodiments include a distilled wax having a crystallinity of from about 55 to about 100 percent, wherein the degree of crystallinity is calculated using the following formulas: [Heat of enthalpy (Hm) J/g/294 J/g]×100=degree of crystallinity (Xc); [Heat of recrystallization (Hrc) J/g/294 J/g]×100=degree of crystallinity (Xc); and Sc/(Sc+Sa)]×100%, wherein Sc is a diffraction peak area of a crystalline component of the wax and the Sa is a diffraction peak area of an amorphous component of the wax; and wherein the Mp, Mn and Mw of the wax are all within the range of from about 500 to about 800, and wherein the wax has a polydispersity of from about 1 to about 1.05.
摘要翻译：实施方案包括结晶度为约55至约100％的蒸馏蜡，其中结晶度用下列公式计算：[热焓（Hm）J / g / 294J / g]×100 =结晶度（Xc）; [重结晶热（Hrc）J / g / 294J / g] x100 =结晶度（Xc）; 和Sc /（Sc + Sa）]×100％，其中Sc是蜡的结晶成分的衍射峰面积，Sa是蜡的无定形成分的衍射峰面积; 并且其中所述蜡的Mp，Mn和Mw均在约500至约800的范围内，并且其中所述蜡具有约1至约1.05的多分散性。

10. 发明申请

US20090123864A1 Ultra Low Melt Toners Comprised of Crystalline Resins 失效
标题翻译：超低熔体碳粉由晶体树脂组成
公开(公告)号：US20090123864A1
公开(公告)日：2009-05-14
申请号：US12353863
申请日：2009-01-14
申请人： Guerino G. SACRIPANTE , Ke Zhou , Michael S. Hawkins , Kimberly D. Nosella , Edward G. Zwartz , Nicoleta D. Mihai , Valerie M. Farrugia , Stephan V. Drappel , Paul J. Gerroir
发明人： Guerino G. SACRIPANTE , Ke Zhou , Michael S. Hawkins , Kimberly D. Nosella , Edward G. Zwartz , Nicoleta D. Mihai , Valerie M. Farrugia , Stephan V. Drappel , Paul J. Gerroir
IPC分类号： G03G9/087
CPC分类号： G03G9/08755 , G03G9/081 , G03G9/08791 , G03G9/08795 , G03G9/08797
摘要： A toner having an amorphous resin, a crystalline resin, and a colorant, wherein the crystalline resin has a melting temperature of at least 70° C. and a recrystallization point of at least 47° C. exhibits improved document offset properties and improved heat cohesion. Annealing the toner further improves the heat cohesion and morphology of the toner.
摘要翻译：具有无定形树脂，结晶性树脂和着色剂的调色剂，其中结晶性树脂的熔融温度为70℃以上，再结晶点为47℃以上，表现出改善的文件偏移性和改善的热粘合性。使调色剂退火进一步提高了调色剂的热粘合性和形态。

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