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1. 发明授权

US07504533B2 Process for the production of isocyanates 有权
标题翻译：生产异氰酸酯的方法
公开(公告)号：US07504533B2
公开(公告)日：2009-03-17
申请号：US11409940
申请日：2006-04-24
申请人： Matthias Böhm , Wolfgang Lorenz , Bill L. Brady, Jr. , Donald L. Pferdehirt
发明人： Matthias Böhm , Wolfgang Lorenz , Bill L. Brady, Jr. , Donald L. Pferdehirt
IPC分类号： C07C263/00 , C07C249/00
CPC分类号： C07C263/10 , C01B7/0706 , C01B7/0731 , C07C263/20 , C07C265/14
摘要： Isocyanates are produced by a) reacting at least one amine with phosgene, optionally in the presence of a solvent to produce the corresponding isocyanate and a stream containing hydrogen chloride, phosgene and optionally solvent, low-boiling compounds and inert substances is obtained, b) separating the stream containing hydrogen chloride, phosgene and optionally solvent, low-boiling compounds and inert substances in an at least two-stage sequence of absorption steps that includes (1) at least one isothermal absorption step and (2) at least one adiabatic absorption step, to obtain (i) a hydrogen chloride stream containing phosgene in concentrations of at most 0.5 wt. % (based on the weight of the hydrogen chloride stream) and (ii) a liquid phosgene stream, and c) recycling the liquid phosgene stream (ii) to the reaction of amine with phosgene.
摘要翻译：异氰酸酯通过以下方法制备：a）任选地在溶剂存在下使至少一种胺与光气反应以产生相应的异氰酸酯，并且获得含有氯化氢，光气和任选溶剂的低沸点化合物和惰性物质的流，b）在至少两级的吸收步骤序列中分离含有氯化氢，光气和任选溶剂的低沸点化合物和惰性物质，其包括（1）至少一个等温吸收步骤和（2）至少一个绝热吸收步骤，以获得（i）含有至多0.5重量％浓度的光气的氯化氢流。％（基于氯化氢流的重量）和（ii）液体光气流，和c）将液体光气流（ii）再循环到胺与光气的反应中。

2. 发明授权

US09150493B2 Method for producing aromatic amines in the liquid phase 有权
标题翻译：在液相中生产芳香胺的方法
公开(公告)号：US09150493B2
公开(公告)日：2015-10-06
申请号：US13521523
申请日：2011-01-10
申请人： Wolfgang Lorenz , Bernd Pennemann
发明人： Wolfgang Lorenz , Bernd Pennemann
IPC分类号： C07C211/00 , C07C209/36
CPC分类号： C07C209/36 , C07C211/51
摘要： The invention relates to a process for the preparation of aromatic amines in the liquid phase by catalytic hydrogenation of the corresponding nitroaromatic compounds in at least two reaction spaces connected in series, wherein at least one reaction space is operated isothermally and at least the reaction space connected downstream thereof is operated adiabatically, and in preferred embodiments the sudden adiabatic temperature change is used for monitoring the reaction.
摘要翻译：本发明涉及通过在至少两个串联连接的反应空间中对相应的硝基芳族化合物进行催化氢化在液相中制备芳族胺的方法，其中至少一个反应空间是等温运行的，并且至少连接的反应空间其下游绝热操作，在优选的实施方案中，突然的绝热温度变化用于监测反应。

3. 发明授权

US09102594B2 Method for producing isocyanates in the gas phase 有权
标题翻译：在气相中生产异氰酸酯的方法
公开(公告)号：US09102594B2
公开(公告)日：2015-08-11
申请号：US13696195
申请日：2011-04-29
申请人： Rainer Bruns , Wolfgang Lorenz , Andreas Karl Rausch , Stefan Wershofen , Tim Loddenkemper
发明人： Rainer Bruns , Wolfgang Lorenz , Andreas Karl Rausch , Stefan Wershofen , Tim Loddenkemper
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for the preparation of isocyanates by reaction of the corresponding amines with phosgene in the gas phase, wherein a diluent containing between 90.0000% by weight and 99.9999% by weight of substances which are inert in the phosgenation process and between 0.0001% by weight and 10.0000% by weight of oxygen is present during the conversion of the amine into the gas phase and the molar ratio of amine to oxygen (O2) is ≧1,000:1.
摘要翻译：本发明涉及一种通过相应的胺与气相中的光气反应来制备异氰酸酯的方法，其中包含在光气化过程中为惰性的物质的90.0000重量％至99.9999重量％的稀释剂和0.0001 在胺转化为气相期间存在重量％和10.0000％重量的氧，胺与氧（O 2）的摩尔比为≧1,000:1。

4. 发明申请

US20130131377A1 METHOD FOR PRODUCING ISOCYANATES IN THE GAS PHASE 有权
标题翻译：在气相中生产异氰酸酯的方法
公开(公告)号：US20130131377A1
公开(公告)日：2013-05-23
申请号：US13696195
申请日：2011-04-29
申请人： Rainer Bruns , Wolfgang Lorenz , Andreas Karl Rausch , Stefan Wershofen , Tim Loddenkemper
发明人： Rainer Bruns , Wolfgang Lorenz , Andreas Karl Rausch , Stefan Wershofen , Tim Loddenkemper
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for the preparation of isocyanates by reaction of the corresponding amines with phosgene in the gas phase, wherein a diluent containing between 90.0000% by weight and 99.9999% by weight of substances which are inert in the phosgenation process and between 0.0001% by weight and 10.0000% by weight of oxygen is present during the conversion of the amine into the gas phase and the molar ratio of amine to oxygen (O2) is ≧1,000:1.
摘要翻译：本发明涉及一种通过相应的胺与气相中的光气反应来制备异氰酸酯的方法，其中包含在光气化过程中为惰性的物质的90.0000重量％至99.9999重量％的稀释剂和0.0001 在胺转化为气相期间存在重量％和10.0000％（重量）的氧，胺与氧（O 2）的摩尔比≥1000:1。

5. 发明申请

US20090209784A1 Process for the preparation of isocyanates 有权
标题翻译：异氰酸酯的制备方法
公开(公告)号：US20090209784A1
公开(公告)日：2009-08-20
申请号：US12378508
申请日：2009-02-17
申请人： Wolfgang Lorenz , Matthias Boehm , Richard Adamson , Friedhelm Steffens , Anke Hielscher
发明人： Wolfgang Lorenz , Matthias Boehm , Richard Adamson , Friedhelm Steffens , Anke Hielscher
IPC分类号： C07C263/10
CPC分类号： C01B7/035 , C07C263/10 , C07C263/20 , C07C265/14 , C07C265/12
摘要： The present invention relates to a process for the preparation of isocyanates by reacting the appropriate amines with phosgene, condensing the gas mixture thereby obtained, stripping the liquid phase thereby obtained and returning the solvent so retained in liquid form to the reaction stage. The gaseous constituents are then purified further in an absorption process.
摘要翻译：本发明涉及通过使适当的胺与光气反应制备异氰酸酯的方法，将由此得到的气体混合物冷凝，将由此获得的液相汽提，并使溶剂保持液态返回到反应阶段。然后在吸收过程中进一步纯化气态成分。

6. 发明申请

US20070249859A1 Process for the production of isocyanates 有权
标题翻译：生产异氰酸酯的方法
公开(公告)号：US20070249859A1
公开(公告)日：2007-10-25
申请号：US11409940
申请日：2006-04-24
申请人： Matthias Bohm , Wolfgang Lorenz , Bill Brady , Donald Pferdehirt
发明人： Matthias Bohm , Wolfgang Lorenz , Bill Brady , Donald Pferdehirt
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C01B7/0706 , C01B7/0731 , C07C263/20 , C07C265/14
摘要： Isocyanates are produced by a) reacting at least one amine with phosgene, optionally in the presence of a solvent to produce the corresponding isocyanate and a stream containing hydrogen chloride, phosgene and optionally solvent, low-boiling compounds and inert substances is obtained, b) separating the stream containing hydrogen chloride, phosgene and optionally solvent, low-boiling compounds and inert substances in an at least two-stage sequence of absorption steps that includes (1) at least one isothermal absorption step and (2) at least one adiabatic absorption step, to obtain (i) a hydrogen chloride stream containing phosgene in concentrations of at most 0.5 wt. % (based on the weight of the hydrogen chloride stream) and (ii) a liquid phosgene stream, and c) recycling the liquid phosgene stream (ii) to the reaction of amine with phosgene.
摘要翻译：异氰酸酯通过以下方法制备：a）任选地在溶剂存在下使至少一种胺与光气反应以产生相应的异氰酸酯，并且获得含有氯化氢，光气和任选溶剂的低沸点化合物和惰性物质的流，b）在至少两级的吸收步骤序列中分离含有氯化氢，光气和任选溶剂的低沸点化合物和惰性物质，其包括（1）至少一个等温吸收步骤和（2）至少一个绝热吸收步骤，以获得（i）含有至多0.5重量％浓度的光气的氯化氢料流。％（基于氯化氢流的重量）和（ii）液体光气流，和c）将液体光气流（ii）再循环到胺与光气的反应中。

7. 发明申请

US20070128365A1 RADIATION-CURABLE, ELECTRICALLY CONDUCTIVE COATIING MIXTURE 有权
标题翻译：辐射可固化，导电性混合混合物
公开(公告)号：US20070128365A1
公开(公告)日：2007-06-07
申请号：US11611812
申请日：2006-12-15
申请人： Matthias Koch , Kerstin Unger , Wolfgang Lorenz , Andreas Kunz , Eva Wilke
发明人： Matthias Koch , Kerstin Unger , Wolfgang Lorenz , Andreas Kunz , Eva Wilke
IPC分类号： B05D3/00 , C08F2/46 , B32B15/08
CPC分类号： C09D5/24 , C09D5/084 , Y10T428/12569
摘要： The present invention relates to electrically conductive and electrically weldable anti-corrosion compositions for coating metal surfaces, a process for coating metal surfaces with electrically conductive organic coatings, as well as the correspondingly coated and optionally painted metal strips, sheets or parts, the coatings comprising: an organic binder, an anti-corrosion pigment, at least one conductive pigment with a density of at least 3 g/cm3 and optionally at least one conductive pigment with a density of less than 3 g/cm3.
摘要翻译：本发明涉及用于涂覆金属表面的导电和可电焊接的防腐蚀组合物，用导电有机涂层涂覆金属表面的方法，以及相应地涂覆和任选涂漆的金属条，片或部分，所述涂层包括：有机粘合剂，防腐蚀颜料，至少一种密度为至少3g / cm 3的导电颜料和任选的至少一种导电颜料，密度小于3g / cm 3。

8. 发明授权

US06835459B2 Conductive organic coatings 失效
标题翻译：导电有机涂料
公开(公告)号：US06835459B2
公开(公告)日：2004-12-28
申请号：US10275538
申请日：2002-11-06
申请人： Wolfgang Lorenz , Andreas Kunz , Eva Wilke
发明人： Wolfgang Lorenz , Andreas Kunz , Eva Wilke
IPC分类号： B32B1504
CPC分类号： C09D5/24 , C09D163/00 , C23C28/00 , Y10S428/931 , Y10T428/12014 , Y10T428/12569 , Y10T428/26 , Y10T428/30 , Y10T428/31504 , Y10T428/31678 , C08L2666/54
摘要： A conductive and weldable anti-corrosion composition for coating metal surfaces which contains: (a) 5 to 40 wt. % of an organic binder containing: (aa) at least one epoxide resin (ab) at least one hardener selected from cyanoguanidine, benzoguanamine and plasticised urea resin (ac) at least one amine adduct selected from polyoxyalkylenetriamine and epoxide resin/amine adducts (b) 0 to 15 wt. % of an anti-corrosion pigment (c) 40 to 70 wt. % of a conductive pigment selected from powdered zinc, aluminum, graphite, molybdenum sulfide, carbon black and iron phosphide (d) 0 to 45 wt. % of a solvent; and a lacquered metal structural part which has a conductive organic layer.

9. 发明授权

US09024057B2 Process for the preparation of isocyanates in the gas phase 有权
标题翻译：在气相中制备异氰酸酯的方法
公开(公告)号：US09024057B2
公开(公告)日：2015-05-05
申请号：US12632117
申请日：2009-12-07
申请人： Klaus Biskup , Rainer Bruns , Wolfgang Lorenz , Fritz Pohl , Friedhelm Steffens , Volker Michele
发明人： Klaus Biskup , Rainer Bruns , Wolfgang Lorenz , Fritz Pohl , Friedhelm Steffens , Volker Michele
IPC分类号： C07C263/00 , C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： Aromatic isocyanates are produced by reacting one or more aromatic primary amines with phosgene in the gas phase. The phosgene and primary aromatic amine(s) are reacted at a temperature above the boiling temperature of the amine(s) in a reactor having a reaction space which is essentially rotationally symmetric to the direction of flow. The flow fate, averaged over the cross-section, of the reaction mixture along the axis of the essentially rotationally symmetric reaction space in the section of the reaction space in which the conversion of the amine groups into isocyanate groups is between 4 and 80% is not more than 8 m/sec. The flow rate averaged over the cross-section of the reaction mixture along the axis of the essentially rotationally symmetric reaction space in the section of the reaction space in which the conversion of the amine groups into isocyanate groups is 4 to 80% is always below the flow rate averaged over the cross-section at the start of this section.
摘要翻译：通过一种或多种芳族伯胺与气相中的光气反应制备芳族异氰酸酯。光气和伯芳基胺在具有反应空间的反应器中在高于胺的沸点温度的温度下反应，反应空间基本上与流动方向旋转对称。反应混合物沿着反应空间部分中基本上旋转对称的反应空间轴线的横截面平均流动，其中胺基转化为异氰酸酯基的反应空间为4-80％不超过8米/秒。反应混合物的横截面上的平均流量在反应空间的基本上旋转对称的反应空间的轴上，其中胺基转化为异氰酸酯基团的部分总是低于在本节开头的横截面上平均流量。

10. 发明申请

US20120302785A1 METHOD FOR PRODUCING ISOCYANATES IN THE GAS PHASE 有权
标题翻译：在气相中生产异氰酸酯的方法
公开(公告)号：US20120302785A1
公开(公告)日：2012-11-29
申请号：US13382609
申请日：2010-06-26
申请人： Rainer Bruns , Wolfgang Lorenz , Knut Sommer
发明人： Rainer Bruns , Wolfgang Lorenz , Knut Sommer
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： An isocyanate is produced by continuously reacting an amine with phosgene in the presence of an inert substance in the gas phase. In this process, a phosgene-containing stream and a stream containing both the amine and the inert substance are fed into a reactor. The molar ratio of the inert substance to the amino groups in the stream is greater than 0 but less than 45 mol %. This molar ratio changes by no more than 99% during a 20 minute period.
摘要翻译：异氰酸酯是通过在气相中惰性物质存在下使胺与光气连续反应生成的。在该方法中，将含有光气的物流和含有胺和惰性物质的物流进料到反应器中。惰性物质与物流中氨基的摩尔比大于0但小于45摩尔％。该摩尔比在20分钟内变化不超过99％。

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