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    • 2. 发明授权
    • Method for producing liquid-crystalline polyester
    • 液晶聚酯的制造方法
    • US08501897B2
    • 2013-08-06
    • US13556871
    • 2012-07-24
    • Tomoya HosodaEiji HosodaMasanobu Matsubara
    • Tomoya HosodaEiji HosodaMasanobu Matsubara
    • C08G63/02C08G64/00
    • C09K19/3809C08G63/605C08G63/87
    • The present invention provides a method for producing a liquid-crystalline polyester, which comprises melt-polymerizing monomers in a reactor having a draw outlet to obtain a polymer melt and drawing the polymer melt through the draw outlet, characterized in that the monomers comprise a compound selected from an aromatic hydroxycarboxylic acid and derivatives thereof, a compound selected from an aromatic dicarboxylic acid and derivatives thereof and a compound selected from an aromatic diol, an aromatic hydroxyamine, an aromatic diamine and derivatives thereof; the amount of units derived from a compound containing a 1,2-phenylene and/or a 1,3-phenylene skeleton(s) in the polyester is from 0 to 10 mol %; the melt polymerization is performed in the presence of a heterocyclic compound containing two or more nitrogen atoms; and the polymer melt has a flow initiation temperature of from 220 to 250° C.
    • 本发明提供一种液晶聚酯的制造方法,其包括在具有拉出口的反应器中使单体熔融聚合以获得聚合物熔体并通过拉出口拉伸聚合物熔体,其特征在于,所述单体包含化合物 选自芳族羟基羧酸及其衍生物,选自芳族二羧酸及其衍生物的化合物和选自芳族二醇,芳族羟胺,芳族二胺及其衍生物的化合物; 衍生自聚酯中含有1,2-亚苯基和/或1,3-亚苯基骨架的化合物的单元的量为0至10mol%; 在含有两个或更多个氮原子的杂环化合物的存在下进行熔融聚合; 聚合物熔体的起始温度为220-250℃。
    • 9. 发明授权
    • Surface treated steel sheet for welded can material
    • 表面处理钢板用于焊接罐头材料
    • US4816348A
    • 1989-03-28
    • US100560
    • 1987-09-24
    • Hiroaki KawamuraMasanobu MatsubaraOsamu YoshiokaTsuneo Inui
    • Hiroaki KawamuraMasanobu MatsubaraOsamu YoshiokaTsuneo Inui
    • C25D11/38C23C28/00C25D3/30C25D5/02C25D5/10C25D5/26C25D5/50B32B15/18
    • C25D3/30C25D11/38C25D5/02C25D5/505Y10T428/1259Y10T428/12722Y10T428/12854Y10T428/12993
    • A surface treated steel sheet having double layers consisting of a lower layer of metallic chromium and an upper layer of hydrated chromium oxide are formed on a low tin plated steel sheet in which 30 to 80% of the surface of the steel sheet is covered with plated tin. Also, the ratio of the area of tin, which actually combined with steel sheet, to the projected area of plated tin to the steel sheet is 20 to 90% and the size of the exposed steel surface units, after tinplating, is 0.5 to 20 .mu.m in diameter when expressing the irregularly exposed areas as circles, and a method for production of this surface treated steel sheet which comprises; (a) electroplating with a small amount of tin under restricted conditions in order to obtain the low tin plated steel sheet described above, (b) after reflowing or without reflowing of the plated tin, formation of said double layer or formation of the metallic chromium layer followed by formation of hydrated chromium oxide under restricted conditions.This surface treated steel sheet is suitable for producing a welded can body without removing the plated layer at high speed, since it is excellent in weldability, lacquer adhesion and corrosion resistance after lacquering.
    • 在低镀锡钢板上形成由金属铬的下层和水合氧化铬上层构成的双层的表面处理钢板,其中钢板的表面的30〜80%被镀覆 锡。 另外,与钢板实际组合的锡的面积与镀锡的投影面积相对于钢板的比例为20〜90%,镀锡后露出的钢表面单元的尺寸为0.5〜20 将不规则曝光区域表示为圆形时的直径为50μm的该表面处理钢板的制造方法,其特征在于, (a)在限制条件下用少量锡进行电镀以获得上述低镀锡钢板,(b)在回流或不回镀镀锡之后,形成所述双层或形成金属铬 层,然后在限制条件下形成水合氧化铬。 该表面处理钢板由于焊接性,漆附着性和涂漆后的耐腐蚀性优异,因此适合于高速除去镀层的焊接罐体的制造。