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1. 发明授权

US5440004A Method and apparatus for the production of alkylene carbonate 失效
标题翻译：用于生产碳酸亚烷基酯的方法和装置
公开(公告)号：US5440004A
公开(公告)日：1995-08-08
申请号：US238743
申请日：1994-05-05
申请人： Masaharu Doya , Yutaka Kanbara , Ken-ichi Kimizuka , Takashi Okawa
发明人： Masaharu Doya , Yutaka Kanbara , Ken-ichi Kimizuka , Takashi Okawa
IPC分类号： C07D317/36 , C08G64/00
CPC分类号： C07D317/36
摘要： A method for the production of an alkylene carbonate at high yields and high selectivity by a reaction between an alkylene glycol and urea, the method being capable to preventing the deposition of a white crystal in the reflux condenser used in a conventional method for the production of alkylene carbonate and the subsequent decrease in the yield, wherein:a gas washing member and a cooling member are disposed above a reaction portion where alkylene glycol and urea are allowed to react,ammonia-containing steam exhausted from the reaction portion is downwardly introduced into the cooling member through the gas washing member,condensate and ammonia gas exhausted from a bottom of the cooling member are gas-liquid separated,the condensate is introduced into the gas washing member, andthe ammonia gas is removed from the reaction system.
摘要翻译：一种通过亚烷基二醇和尿素之间的反应以高产率和高选择性生产碳酸亚烷基酯的方法，该方法能够防止白色结晶沉积在用于生产碳酸亚烷基酯和随后的产率降低，其中：气体洗涤部件和冷却部件设置在使亚烷基二醇和尿素反应的反应部分上方，从反应部分排出的含氨蒸气被向下引入通过气体洗涤部件的冷却部件，从冷却部件的底部排出的冷凝物和氨气体被气液分离，将冷凝物引入到气体洗涤部件中，从反应体系中除去氨气。

2. 发明授权

US5489702A Process for the production of dialkyl carbonate 失效
标题翻译：碳酸二烷基酯的制备方法
公开(公告)号：US5489702A
公开(公告)日：1996-02-06
申请号：US286203
申请日：1994-08-05
申请人： Masaharu Doya , Ken-ichi Kimizuka , Yutaka Kanbara
发明人： Masaharu Doya , Ken-ichi Kimizuka , Yutaka Kanbara
IPC分类号： B01J21/10 , B01J23/02 , B01J23/06 , B01J23/14 , C07B61/00 , C07C68/00 , C07C68/06 , C07C69/96 , C07D317/36
CPC分类号： C07D317/36 , C07C68/00 , C07C68/065
摘要： A process for the production of a dialkyl carbonate comprisinga first step of reacting an alkylene glycol, or an alkanediol, with urea in the presence of a catalyst to form an alkylene carbonate or a six-membered cyclic carbonate, anda second step of reacting the alkylene carbonate or the six-membered cyclic carbonate with an alcohol in the presence of a catalyst to obtain a dialkyl carbonate and an alkylene glycol, or a dialkyl carbonate and an alkanediol,wherein the alkylene glycol or the alkanediol obtained in the second step is recycled to the first step.
摘要翻译：一种制备碳酸二烷基酯的方法，包括在催化剂存在下使亚烷基二醇或链烷二醇与脲反应的第一步骤，以形成碳酸亚烃酯或六元环状碳酸酯，第二步是使碳酸亚烃酯或六元环状碳酸酯与醇在催化剂存在下反应，得到碳酸二烷基酯和亚烷基二醇或碳酸二烷基酯和链烷二醇，其中第二步得到的亚烷基二醇或链烷二醇是回收到第一步。

3. 发明授权

US5349077A Process for producing alkylene carbonates 失效
标题翻译：碳酸亚烷基酯的制备方法
公开(公告)号：US5349077A
公开(公告)日：1994-09-20
申请号：US99461
申请日：1993-07-30
申请人： Masaharu Doya , Takashi Ohkawa , Yutaka Kanbara , Aksushi Okamoto , Kenichi Kimizuka
发明人： Masaharu Doya , Takashi Ohkawa , Yutaka Kanbara , Aksushi Okamoto , Kenichi Kimizuka
IPC分类号： C07D317/36 , C07D317/38 , C07C69/96
CPC分类号： C07D317/38 , C07D317/36
摘要： A process for producing alkylene carbonates which comprises reacting urea and glycols described by the general formula RCH(OH) CH.sub.2 OH; wherein R represents hydrogen or an alkyl group containing 1 to 4 carbons, using a catalyst containing zinc, magnesium, lead or calcium at reduced pressures. The alkylene carbonates are produced with high yield easily using raw materials which are comparatively inexpensive with a mild reaction that does not involve explosive or hazardous materials.
摘要翻译：一种制备碳酸亚烷基酯的方法，其包括使通式RCH（OH）CH 2 OH描述的脲和二醇反应; 其中R表示氢或含有1至4个碳的烷基，在减压下使用含锌，镁，铅或钙的催化剂。碳酸亚烷基酯可以容易地使用相对便宜的不具有爆炸性或有害物质的轻度反应的原料而高产率地制备。

4. 发明授权

US5969187A Process for producing trans 1,4-bis(aminomethyl)cyclohexane 失效
标题翻译：制备反式1,4-双（氨基甲基）环己烷的方法
公开(公告)号：US5969187A
公开(公告)日：1999-10-19
申请号：US30794
申请日：1998-02-26
申请人： Takashi Okawa , Tomoo Tsujimoto , Hideo Ikarashi , Masaharu Doya , Yutaka Kanbara
发明人： Takashi Okawa , Tomoo Tsujimoto , Hideo Ikarashi , Masaharu Doya , Yutaka Kanbara
IPC分类号： C07C209/68 , C07C209/86 , C07C211/18 , C07C209/88
CPC分类号： C07C209/86 , C07C209/68
摘要： Provided a process for producing higher content of trans 1,4-bis(aminomethyl)cyclohexane which is used as the raw material for producing polyamides or polyurethanes having physically and chemically excellent properties from 1,4-bis(aminomethyl)cyclohexane which is generally produced by hydrogenation of p-xylylenediamine.That is, a mixture of cis and trans 1,4-bis(aminomethyl)cyclohexane is isomerized by heating at 120 to 250.degree. C. in the presence of a platinum group catalyst to change to trans isomer. 1,4-bis(aminomethyl)cyclohexane containing more than 80% trans isomer is produced by combining this isomerization technique and crystallization technique.
摘要翻译：提供了用于生产具有物理和化学性质优异的聚酰胺或聚氨酯的原料的反式1,4-双（氨基甲基）环己烷的较高含量的方法，其通常由1,4-双（氨基甲基）环己烷生产通过对苯二甲胺的氢化。也就是说，在铂族催化剂的存在下，通过在120-250℃下加热使顺式和反式1,4-双（氨基甲基）环己烷的混合物异构化，以变成反式异构体。通过组合这种异构化技术和结晶技术产生含有超过80％反式异构体的1,4-双（氨基甲基）环己烷。

5. 发明授权

US08993774B2 Process for production of aromatic alcohol or heterocyclic aromatic alcohol 有权
标题翻译：生产芳香醇或杂环芳香醇的方法
公开(公告)号：US08993774B2
公开(公告)日：2015-03-31
申请号：US13996759
申请日：2011-12-22
申请人： Yutaka Kanbara , Takafumi Abe , Norio Fushimi
发明人： Yutaka Kanbara , Takafumi Abe , Norio Fushimi
IPC分类号： C07D211/70 , C07B41/02 , C07C29/00 , C07C41/26 , C07C29/128 , C07D213/30 , C07C213/00 , C07C29/09 , B01J23/04
CPC分类号： C07B41/02 , B01J23/04 , C07C29/00 , C07C29/09 , C07C29/128 , C07C41/26 , C07C213/00 , C07D213/30 , C07C33/18 , C07C33/22 , C07C33/26 , C07C33/20 , C07C43/23 , C07C33/46 , C07C215/68
摘要： A process of production of an aromatic alcohol or a heterocyclic aromatic alcohol, containing a step of reacting an aromatic amine or a heterocyclic aromatic amine having an aromatic ring or a heterocyclic aromatic ring having thereon at least one substituent —CHR1NR2R3 (wherein R1, R2 and R3 each independently represent hydrogen, an alkyl group having from 1 to 4 carbon atoms, or a benzyl group), with an alcohol, in the presence of a basic catalyst.
摘要翻译：一种制备芳族醇或杂环芳族醇的方法，其包括使芳族胺或具有芳环的杂环芳族胺或其上具有至少一个取代基的杂环芳族环的芳基胺反应的步骤，其中R1，R2和 R 3各自独立地表示氢，具有1至4个碳原子的烷基或苄基）与醇在碱性催化剂的存在下反应。

6. 发明授权

US06784317B2 Production of quaternary ammonium salt of hydroxycarboxylic acid and quarternary ammonium salt of inorganic acid 失效
标题翻译：生产羟基羧酸季铵盐和无机酸季铵盐
公开(公告)号：US06784317B2
公开(公告)日：2004-08-31
申请号：US10125371
申请日：2002-04-19
申请人： Yutaka Kanbara , Yasushi Higuchi , Tomoo Tsujimoto , Genki Nogami
发明人： Yutaka Kanbara , Yasushi Higuchi , Tomoo Tsujimoto , Genki Nogami
IPC分类号： C07C21162
CPC分类号： C07C209/20 , C07C211/63
摘要： A quaternary ammonium hydroxycarboxylate is produced by quaternizing a tertiary amine with a hydroxycarboxylic ester represented by the following Formula 1: wherein R1 to R3 are as defined in the disclosure. By using only one tertiary amine having at least one substituent different from R1 of the ester moiety of the hydroxycarboxylic ester and by controlling the reaction conditions, a mixture of quaternary ammonium hydroxycarboxylates having different quaternary ammonium ions is produced. By reacting an inorganic acid with the quaternary ammonium hydroxycarboxylate or its mixture, a quaternary ammonium salt of inorganic acid or its mixture is produced.
摘要翻译：通过用下列通式1表示的羟基羧酸季铵化叔胺来制备羟基羧酸季铵盐：其中R 1至R 3如本公开所定义。通过仅使用一种具有至少一个与羟基羧酸酯的酯部分的R 1不同的取代基的叔胺，并且通过控制反应条件，产生具有不同季铵离子的季铵羟基羧酸盐的混合物。通过使无机酸与羟基羧酸季铵盐或其混合物反应，生成无机酸的季铵盐或其混合物。

7. 发明授权

US06222065B1 Process for the production of 1,5-naphtylenediisocyanate 失效
标题翻译： 1,5-萘二异氰酸酯的制备方法
公开(公告)号：US06222065B1
公开(公告)日：2001-04-24
申请号：US09614177
申请日：2000-07-11
申请人： Yutaka Okawa , Tomoo Tsujimoto , Yutaka Kanbara , Hiroshi Matsunaga
发明人： Yutaka Okawa , Tomoo Tsujimoto , Yutaka Kanbara , Hiroshi Matsunaga
IPC分类号： C07C26300
CPC分类号： C07C263/12 , C07C263/04 , C07C265/14
摘要： 1,5-naphthylenediisocyanate is industrially advantageously produced at high yields by pyrolyzing methyl 1,5-naphthylenecarbamate synthesized by providing 1,5-naphthylenedinitrile as a raw material and carrying out amidation, chlorination and Hofmann rearrangement.
摘要翻译：通过以1,5-萘二腈作原料合成并进行酰胺化，氯化和霍夫曼重排而合成的1,5-萘基癸氨酸甲酯，工业上有利于高产率制备1,5-萘二异氰酸酯。

8. 发明授权

US06967258B2 Production of quaternary ammonium salt of hydroxycarboxylic acid and quaternary ammonium salt of inorganic acid 失效
标题翻译：生产羟基羧酸季铵盐和无机酸季铵盐
公开(公告)号：US06967258B2
公开(公告)日：2005-11-22
申请号：US10840359
申请日：2004-05-07
申请人： Yutaka Kanbara , Yasushi Higuchi , Tomoo Tsujimoto , Genki Nogami
发明人： Yutaka Kanbara , Yasushi Higuchi , Tomoo Tsujimoto , Genki Nogami
IPC分类号： C07C211/63 , C07C209/20 , C07C209/00
CPC分类号： C07C209/20 , C07C211/63
摘要： A quaternary ammonium hydroxycarboxylate is produced by quaternizing a tertiary amine with a hydroxycarboxylic ester represented by the following Formula 1: wherein R1 to R3 are as defined in the disclosure. By using only one tertiary amine having at least one substituent different from R1 of the ester moiety of the hydroxycarboxylic ester and by controlling the reaction conditions, a mixture of quaternary ammonium hydroxycarboxylates having different quaternary ammonium ions is produced. By reacting an inorganic acid with the quaternary ammonium hydroxycarboxylate or its mixture, a quaternary ammonium salt of inorganic acid or its mixture is produced.
摘要翻译：季铵羟基羧酸盐是通过用下列通式1表示的羟基羧酸季铵化叔胺制备的：其中R 1至R 3如本公开所定义。通过仅使用一种具有至少一个不同于羟基羧酸酯的酯部分的R 1的取代基的叔胺并通过控制反应条件，产生具有不同季铵离子的季铵羟基羧酸盐的混合物。通过使无机酸与羟基羧酸季铵盐或其混合物反应，生成无机酸的季铵盐或其混合物。

9. 发明授权

US5870688A Misfire diagnostic system for internal combustion engine 失效
标题翻译：内燃机失火诊断系统
公开(公告)号：US5870688A
公开(公告)日：1999-02-09
申请号：US749396
申请日：1996-11-15
申请人： Yutaka Kanbara , Akira Uchikawa
发明人： Yutaka Kanbara , Akira Uchikawa
IPC分类号： G01M15/04 , F02D41/00 , F02D41/14 , F02D41/34 , F02D45/00 , F02P17/12 , G01M15/00
CPC分类号： F02D41/1498 , F02D2200/1015 , F02D41/0085
摘要： A misfire diagnostic system for an Internal combustion engine comprises a crank-shaft angle sensor for monitoring a crankshaft angular velocity reflecting a combusting condition of each of engine cylinders, and a control unit for calculating an angular-velocity correction factor of each of the engine cylinders on the basis of the angular velocity in every engine operating region only under a stable engine operating condition. The control unit corrects the angular velocity by the angular-velocity correction factor of each of the engine cylinders for every engine operating region. The presence of a misfire is accurately decided on the basis of the angular velocity corrected for every engine cylinder and for every engine operating region.
摘要翻译：用于内燃机的失火诊断系统包括用于监测反映每个发动机气缸的燃烧状态的曲轴角速度的曲柄轴角度传感器，以及用于计算每个发动机气缸的角速度校正系数的控制单元基于每个发动机运行区域的角速度，仅在稳定的发动机运行条件下。控制单元通过每个发动机工作区域的每个发动机气缸的角速度校正系数校正角速度。基于为每个发动机气缸和每个发动机工作区域校正的角速度准确地确定失火的存在。

10. 发明申请

US20130303775A1 PROCESS FOR PRODUCTION OF AROMATIC ALCOHOL OR HETEROCYCLIC AROMATIC ALCOHOL 有权
标题翻译：生产芳香醇或杂环芳香醇的方法
公开(公告)号：US20130303775A1
公开(公告)日：2013-11-14
申请号：US13996759
申请日：2011-12-22
申请人： Yutaka Kanbara , Takafumi Abe , Norio Fushimi
发明人： Yutaka Kanbara , Takafumi Abe , Norio Fushimi
IPC分类号： C07B41/02 , C07D213/30 , C07C29/00
CPC分类号： C07B41/02 , B01J23/04 , C07C29/00 , C07C29/09 , C07C29/128 , C07C41/26 , C07C213/00 , C07D213/30 , C07C33/18 , C07C33/22 , C07C33/26 , C07C33/20 , C07C43/23 , C07C33/46 , C07C215/68
摘要： A process of production of an aromatic alcohol or a heterocyclic aromatic alcohol, containing a step of reacting an aromatic amine or a heterocyclic aromatic amine having an aromatic ring or a heterocyclic aromatic ring having thereon at least one substituent —CHR1NR2R3 (wherein R1, R2 and R3 each independently represent hydrogen, an alkyl group having from 1 to 4 carbon atoms, or a benzyl group), with an alcohol, in the presence of a basic catalyst.
摘要翻译：一种制备芳族醇或杂环芳族醇的方法，其包括使芳族胺或具有芳环的杂环芳族胺或其上具有至少一个取代基的杂环芳族环的芳基胺反应的步骤，其中R1，R2和 R 3各自独立地表示氢，具有1至4个碳原子的烷基或苄基）与醇在碱性催化剂的存在下反应。

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