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1. 发明授权

US09034976B2 Hydrogenated petroleum resin pellet production method 有权
标题翻译：氢化石油树脂颗粒生产方法
公开(公告)号：US09034976B2
公开(公告)日：2015-05-19
申请号：US14115040
申请日：2012-05-31
申请人： Makoto Kashima
发明人： Makoto Kashima
IPC分类号： C08L65/00 , C08F212/08 , C08F8/04 , C08F232/06
CPC分类号： C08L65/00 , C08F8/04 , C08F212/08 , C08F232/06
摘要： After a cyclopentadiene compound and a vinyl aromatic compound are thermally polymerized, the obtained copolymer is subjected to a hydrogenation reaction to form a hydrogenated product. After most of the hydrogenation solvent is separated by a solvent evaporation tank from the hydrogenated product, an additive separately prepared by dissolving an antioxidant is added to the hydrogenated product to form a mixture. While the hydrogenation solvent is a naphthenic solvent, the additive is prepared by dissolving the antioxidant in an aromatic additive solvent having the same carbon atoms as those of the hydrogenation solvent. Then, the low-molecular-weight component as well as the remaining hydrogenation solution and the additive solvent are separated by a thin-film evaporator from the mixture. The obtained molten resin is pelletized to produce hydrogenated petroleum resin pellets. The time for uniformly blending the antioxidant can be shortened.
摘要翻译：在环戊二烯化合物和乙烯基芳族化合物热聚合之后，将所得共聚物进行氢化反应以形成氢化产物。在通过溶剂蒸发槽从氢化产物中分离大部分氢化溶剂后，将通过溶解抗氧化剂分开制备的添加剂加入到氢化产物中以形成混合物。虽然氢化溶剂是环烷溶剂，但是通过将抗氧化剂溶解在与氢化溶剂的碳原子相同的芳族添加剂溶剂中来制备添加剂。然后，通过薄膜蒸发器从混合物中分离低分子量组分以及剩余的氢化溶液和添加剂溶剂。将得到的熔融树脂造粒，生成氢化石油树脂颗粒。可以缩短均匀混合抗氧化剂的时间。

2. 发明授权

US09023944B2 Process for producing hydrogenated petroleum resin 有权
标题翻译：生产氢化石油树脂的方法
公开(公告)号：US09023944B2
公开(公告)日：2015-05-05
申请号：US14116262
申请日：2012-05-31
申请人： Takanori Hayashi , Hajime Takasugi , Makoto Kashima
发明人： Takanori Hayashi , Hajime Takasugi , Makoto Kashima
IPC分类号： C08F8/04 , C08F112/08 , C08F240/00 , C08L65/00
CPC分类号： C08F8/04 , C08F240/00
摘要： A method including measuring a near-infrared absorption spectrum of a hydrogenated compound in the form of a molten resin from which a hydrogenation solvent is separated to calculate an aromatic content ratio and a softening point as physical property values of the hydrogenated compound based on analytical curve data. At least one of a temperature, pressure, reaction time and hydrogen content in a hydrogenating portion is controlled such that a difference between the aromatic content ratio and the bromine number measured in the near-infrared spectrometry and an aromatic content ratio and bromine number of a target hydrogenated petroleum resin pellet becomes small.
摘要翻译：一种方法，包括测量氢化溶剂形式的氢化化合物的近红外吸收光谱，氢化溶剂从其分离，以计算芳族含量比和软化点作为氢化化合物的物理性能值，基于分析曲线数据。控制加氢部分中的温度，压力，反应时间和氢含量中的至少一个，使得在近红外光谱中测量的芳族含量比和溴数之间的差异以及芳族含量比和溴数目标氢化石油树脂颗粒变小。

3. 发明授权

US08748659B2 Method for producing alpha,beta-unsaturated carboxylic acid-N,N-disubstituted amide and method for producing 3-alkoxycarboxylic acid-N,N-disubstituted amide 失效
标题翻译：制备α，β-不饱和羧酸-N，N-二取代酰胺的方法及其制备3-烷氧基羧酸-N，N-二取代酰胺的方法
公开(公告)号：US08748659B2
公开(公告)日：2014-06-10
申请号：US13266899
申请日：2010-04-28
申请人： Hironori Tashiro , Yasushi Shiraki , Makoto Kashima
发明人： Hironori Tashiro , Yasushi Shiraki , Makoto Kashima
IPC分类号： C07C231/02
CPC分类号： C07C231/02 , C07C227/06 , C07C227/08 , C07C231/12 , C07C231/22 , C07C229/12 , C07C233/05 , C07C233/09
摘要： The invention is directed to a technique for effectively producing an amide compound suitable for use as a solvent or a detergent on a large scale and at low cost.
摘要翻译：本发明涉及一种有效地生产适合用作大规模和低成本的溶剂或洗涤剂的酰胺化合物的技术。

4. 发明授权

US09120615B2 Storage device for granular material 有权
标题翻译：颗粒材料储存装置
公开(公告)号：US09120615B2
公开(公告)日：2015-09-01
申请号：US14116012
申请日：2012-05-31
申请人： Makoto Kashima , Hajime Takasugi
发明人： Makoto Kashima , Hajime Takasugi
IPC分类号： B65G11/00 , B65D88/54 , B65G11/08 , B65D88/26 , B65G69/16 , B65G47/72 , B65G11/20
CPC分类号： B65D88/54 , B65D88/26 , B65G11/088 , B65G11/206 , B65G47/72 , B65G69/16
摘要： A groove inclined path for diagonally downwardly delivering hydrogenated petroleum resin pellets loaded through a loading port is provided in a storage hopper for storing the hydrogenated petroleum resin pellets. The groove inclined path is defined by a plurality of groove-inclined-path members each having an inclined plate and side plates to define a groove structure, the groove-inclined-path members being vertically disposed so that flow directions of the hydrogenated petroleum resin pellets become opposite. The vertically adjacent ones of the groove-inclined-path members are disposed so that the hydrogenated petroleum resin pellets dropped from upper one of the groove-inclined-path members are brought into contact with the plate member of immediately lower one of the groove-inclined-path members to reverse a flow direction thereof, thereby reducing a flow speed of the hydrogenated petroleum resin pellets.
摘要翻译：在用于储存氢化石油树脂颗粒的存储料斗中设置有用于斜向下输送通过装载口装载的氢化石油树脂颗粒的槽倾斜路径。槽倾斜路径由多个倾斜板和侧板形成的沟槽倾斜路径构件限定沟槽结构，槽倾斜路径构件垂直设置，使得氢化石油树脂颗粒的流动方向变得相反。凹槽倾斜路径构件中的垂直相邻的槽倾斜路径构件被设置成使得从上部一个槽倾斜路径构件落下的氢化石油树脂颗粒与立即下降的槽倾斜的板构件接触反转其流动方向，从而降低氢化石油树脂颗粒的流速。

5. 发明申请

US20140093340A1 STORAGE DEVICE FOR GRANULAR MATERIAL 有权
标题翻译：颗粒材料储存装置
公开(公告)号：US20140093340A1
公开(公告)日：2014-04-03
申请号：US14116012
申请日：2012-05-31
申请人： Makoto Kashima , Hajime Takasugi
发明人： Makoto Kashima , Hajime Takasugi
IPC分类号： B65D88/54
CPC分类号： B65D88/54 , B65D88/26 , B65G11/088 , B65G11/206 , B65G47/72 , B65G69/16
摘要： A groove inclined path for diagonally downwardly delivering hydrogenated petroleum resin pellets loaded through a loading port is provided in a storage hopper for storing the hydrogenated petroleum resin pellets. The groove inclined path is defined by a plurality of groove-inclined-path members each having an inclined plate and side plates to define a groove structure, the groove-inclined-path members being vertically disposed so that flow directions of the hydrogenated petroleum resin pellets become opposite. The vertically adjacent ones of the groove-inclined-path members are disposed so that the hydrogenated petroleum resin pellets dropped from upper one of the groove-inclined-path members are brought into contact with the plate member of immediately lower one of the groove-inclined-path members to reverse a flow direction thereof, thereby reducing a flow speed of the hydrogenated petroleum resin pellets.
摘要翻译：在用于储存氢化石油树脂颗粒的存储料斗中设置有用于斜向下输送通过装载口装载的氢化石油树脂颗粒的槽倾斜路径。槽倾斜路径由多个倾斜板和侧板形成的沟槽倾斜路径构件限定沟槽结构，槽倾斜路径构件垂直设置，使得氢化石油树脂颗粒的流动方向变得相反。凹槽倾斜路径构件中的垂直相邻的槽倾斜路径构件被设置成使得从上部一个槽倾斜路径构件落下的氢化石油树脂颗粒与立即下降的槽倾斜的板构件接触反转其流动方向，从而降低氢化石油树脂颗粒的流速。

6. 发明申请

US20140058033A1 HYDROGENATED PETROLEUM RESIN PELLET PRODUCTION METHOD 有权
标题翻译：氢化石油树脂生产方法
公开(公告)号：US20140058033A1
公开(公告)日：2014-02-27
申请号：US14115040
申请日：2012-05-31
申请人： Makoto Kashima
发明人： Makoto Kashima
IPC分类号： C08L65/00
CPC分类号： C08L65/00 , C08F8/04 , C08F212/08 , C08F232/06
摘要： After a cyclopentadiene compound and a vinyl aromatic compound are thermally polymerized, the obtained copolymer is subjected to a hydrogenation reaction to form a hydrogenated product. After most of the hydrogenation solvent is separated by a solvent evaporation tank from the hydrogenated product, an additive separately prepared by dissolving an antioxidant is added to the hydrogenated product to form a mixture. While the hydrogenation solvent is a naphthenic solvent, the additive is prepared by dissolving the antioxidant in an aromatic additive solvent having the same carbon atoms as those of the hydrogenation solvent. Then, the low-molecular-weight component as well as the remaining hydrogenation solution and the additive solvent are separated by a thin-film evaporator from the mixture. The obtained molten resin is pelletized to produce hydrogenated petroleum resin pellets. The time for uniformly blending the antioxidant can be shortened.
摘要翻译：在环戊二烯化合物和乙烯基芳族化合物热聚合之后，将所得共聚物进行氢化反应以形成氢化产物。在通过溶剂蒸发槽从氢化产物中分离大部分氢化溶剂后，将通过溶解抗氧化剂分开制备的添加剂加入到氢化产物中以形成混合物。虽然氢化溶剂是环烷溶剂，但是通过将抗氧化剂溶解在与氢化溶剂的碳原子相同的芳族添加剂溶剂中来制备添加剂。然后，通过薄膜蒸发器从混合物中分离低分子量组分以及剩余的氢化溶液和添加剂溶剂。将得到的熔融树脂造粒，生成氢化石油树脂颗粒。可以缩短均匀混合抗氧化剂的时间。

7. 发明申请

US20120088931A1 METHOD FOR PRODUCING ALPHA,BETA-UNSATURATED CARBOXYLIC ACID-N,N-DISUBSTITUTED AMIDE AND METHOD FOR PRODUCING 3-ALKOXYCARBOXYLIC ACID-N,N-DISUBSTITUTED AMIDE 失效
标题翻译：用于制备ALPHA，不饱和羧酸，N，N-取代的酰胺的方法和用于生产3-烷氧羰基氧基-N，N-取代的酰胺的方法
公开(公告)号：US20120088931A1
公开(公告)日：2012-04-12
申请号：US13266899
申请日：2010-04-28
申请人： Hironori Tashiro , Yasushi Shiraki , Makoto Kashima
发明人： Hironori Tashiro , Yasushi Shiraki , Makoto Kashima
IPC分类号： C07C231/02 , C07C227/18
CPC分类号： C07C231/02 , C07C227/06 , C07C227/08 , C07C231/12 , C07C231/22 , C07C229/12 , C07C233/05 , C07C233/09
摘要： The invention is directed to a technique for effectively producing an amide compound suitable for use as a solvent or a detergent on a large scale and at low cost.
摘要翻译：本发明涉及一种有效地生产适合用作大规模和低成本的溶剂或洗涤剂的酰胺化合物的技术。

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