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1. 发明授权

US07138478B2 Process for mixing polymer melts with additives 有权
标题翻译：聚合物熔体与添加剂混合的方法
公开(公告)号：US07138478B2
公开(公告)日：2006-11-21
申请号：US10825887
申请日：2004-04-16
申请人： Klemens Kohlgrüber , Günther Holdenried , Christian Kords , Jürgen Heuser , Thomas König
发明人： Klemens Kohlgrüber , Günther Holdenried , Christian Kords , Jürgen Heuser , Thomas König
IPC分类号： C08G64/00
CPC分类号： B29B7/94 , B29B7/325 , B29C47/64 , B29K2069/00 , C08L69/00
摘要： A continuous process for mixing polymer melts with additives, in particular polycarbonate melts with additives in liquid form, in solution or in dispersion is described. The additives are added to a main stream of polymer melt and are then mixed, preferably directly, with the main stream in a static mixer.
摘要翻译：描述了将聚合物熔体与添加剂，特别是具有液体形式的添加剂的聚碳酸酯熔体在溶液或分散体中混合的连续方法。将添加剂加入到聚合物熔体的主流中，然后优选直接与主流在静态混合器中混合。

2. 发明授权

US06534619B1 Method for evaporating polymer solutions of thermoplastic polymers 失效
标题翻译：蒸发热塑性聚合物聚合物溶液的方法
公开(公告)号：US06534619B1
公开(公告)日：2003-03-18
申请号：US09762366
申请日：2001-02-05
申请人： Thomas Elsner , Jürgen Heuser , Klemens Kohlgrüber , Christian Kords
发明人： Thomas Elsner , Jürgen Heuser , Klemens Kohlgrüber , Christian Kords
IPC分类号： C08G8102
CPC分类号： B01D19/0047 , B01D3/06 , B01D3/065 , C08F6/003 , C08G64/406
摘要： This invention relates to a multistep process for evaporating polymer solutions of thermoplastic polymers and for removing volatile constituents from thermoplastic polymers by indirect heat exchange. The invention relates in particular to a process for evaporating volatile constituents out of polymer solutions using shell-and-tube heat exchangers having a special geometry, coiled-tube evaporators and extrusion evaporators.
摘要翻译：本发明涉及用于蒸发热塑性聚合物的聚合物溶液并通过间接热交换从热塑性聚合物中除去挥发性成分的多步法。本发明特别涉及一种使用具有特殊几何形状的管壳式热交换器，螺旋管式蒸发器和挤出蒸发器从聚合物溶液中蒸发挥发性成分的方法。

3. 发明授权

US06506281B1 Method for isolating polymers from solutions 失效
标题翻译：从溶液中分离聚合物的方法
公开(公告)号：US06506281B1
公开(公告)日：2003-01-14
申请号：US09719891
申请日：2001-03-02
申请人： Clemens Casper , Jörgen Weinschenck , Klemens Kohlgrüber , Jürgen Heuser , Christian Kords , Thomas Elsner
发明人： Clemens Casper , Jörgen Weinschenck , Klemens Kohlgrüber , Jürgen Heuser , Christian Kords , Thomas Elsner
IPC分类号： B01D122
CPC分类号： B01D3/06 , C08G64/406 , Y10S159/08 , Y10S159/10
摘要： A process of evaporating a viscous polymer solution is described. The process includes: (a) providing a viscous polymer solution including at least 30 wt. % of solvents and monomers; (b) introducing the viscous polymer solution into a heated helix (5), the heated helix having a vapor exit velocity of 200 to 300 m/s, (a film flow including a two-phase mixture of polymer melt, and solvent vapors and monomer vapors being formed within the helix); (c) forwarding the film flow from helix (5) into a heated vapor separator (6); (d) expanding the two-phase mixture of polymer melt, and solvent vapors and monomer vapors of the film flow within vapor separator (6) at an absolute pressure of 10 mbar to 800 mbar, (a bottom product including a concentrated melt of the polymer is formed within the vapor separator); and (e) withdrawing the bottom product from vapor separator (6). Each of the helix (5) and vapor separator (6) have a separate heating device, and each of heating device independently provides a temperature that is above the softening point of the polymer.
摘要翻译：描述蒸发粘性聚合物溶液的方法。该方法包括：（a）提供粘性聚合物溶液，其包含至少30wt。％的溶剂和单体; （b）将粘性聚合物溶液引入加热的螺旋（5）中，加热的螺旋具有200-300m / s的蒸气出口速度（包括聚合物熔体和溶剂蒸气的两相混合物的膜流和单体蒸气在螺旋内形成）; （c）将膜流从螺旋（5）转移到加热的蒸气分离器（6）中; （d）在10毫巴至800毫巴的绝对压力下，将蒸气分离器（6）内的聚合物熔体和溶剂蒸气和单体蒸气的溶剂蒸气和单体蒸气膨胀（包括含有聚合物形成在蒸气分离器内）; 和（e）从蒸气分离器（6）中取出底部产物。螺旋（5）和蒸汽分离器（6）中的每一个具有单独的加热装置，并且每个加热装置独立地提供高于聚合物软化点的温度。

4. 发明授权

US06780281B1 Strand evaporator 失效
标题翻译：绞线蒸发器
公开(公告)号：US06780281B1
公开(公告)日：2004-08-24
申请号：US10130757
申请日：2002-05-22
申请人： Thomas Elsner , Jürgen Heuser , Christian Kords , Klemens Kohlgrüber
发明人： Thomas Elsner , Jürgen Heuser , Christian Kords , Klemens Kohlgrüber
IPC分类号： B01D108
CPC分类号： B01D1/06 , B01D1/04 , B01D3/008 , B01D19/0021 , B29C47/0019 , B29C47/003 , B29C47/76 , C08F6/003 , Y10S159/10 , Y10S159/15
摘要： A strand devolatilizer that includes a degassing container, a product inlet, a product distributor, a product outlet and a vapor outlet is disclosed. The product distributor is in the form of a tube distributor with at least one distributor tube (1) and a plurality of die tubes (2) arranged in parallel, each containing a plurality of apertures (15) in the tube wall. The die tubes (2) are preferably arranged in several planes one above the other and staggered laterally relative to one another.
摘要翻译：公开了一种包含脱气容器，产品入口，产品分配器，产品出口和蒸汽出口的脱脂剂。产品分配器是具有管分配器的形式，具有至少一个分配器管（1）和平行布置的多个模具管（2），每个在管壁中包含多个孔（15）。模具管（2）优选地布置在多个平面中，并且彼此相对并且彼此横向错开。

5. 发明授权

US07144981B2 Process for separating volatile components from polymers 失效
标题翻译：挥发性组分与聚合物分离的方法
公开(公告)号：US07144981B2
公开(公告)日：2006-12-05
申请号：US10684600
申请日：2003-10-14
申请人： Thomas König , Klemens Kohlgrüber , Ulrich Liesenfelder , Michael Bierdel , Helmut Meyer , Richard Weider , Jörg Krüger
发明人： Thomas König , Klemens Kohlgrüber , Ulrich Liesenfelder , Michael Bierdel , Helmut Meyer , Richard Weider , Jörg Krüger
IPC分类号： C08F6/00
CPC分类号： C08F6/003
摘要： A process for concentrating polymers by evaporation is disclosed. The process entails (i) obtaining a mixture containing a polymer and volatile component, the volatile components being present in the mixture at an amount less than 20 wt. % relative to the weight of the mixture, and (ii) introducing the mixture in a downward direction under pressure through a plurality of nozzles arranged vertically and next to one another into a degassing container to form an extrudate. The volatile component contains at least one of residual monomers, oligomers and solvents, and the throughput of the mixture per nozzle is 0.3 to 2 kg/h. The vapor pressure of the volatile component of the extrudate is more than 2.5 bar, and the absolute pressure in the degassing container is 50 to 5000 Pa. The polymer prepared by the process is characterized in that it contains volatile components in an amount of less than 300 ppm.
摘要翻译：公开了通过蒸发浓缩聚合物的方法。该方法需要（i）获得含有聚合物和挥发性组分的混合物，所述挥发性组分以小于20重量％的量存在于混合物中。相对于混合物重量的％，和（ii）通过垂直且彼此相邻布置的多个喷嘴在压力下向下引入混合物到脱气容器中以形成挤出物。挥发性组分含有残留单体，低聚物和溶剂中的至少一种，并且每个喷嘴的混合物的生产量为0.3至2kg / h。挤出物的挥发性成分的蒸气压大于2.5巴，脱气容器中的绝对压力为50〜5000Pa。本方法制备的聚合物的特征在于，其含有挥发性成分的量小于 300 ppm。

6. 发明授权

US09828464B2 Ultra-high purity polycarbonates having good inherent color and thermal resistance and a device and a method for producing the same 有权
公开(公告)号：US09828464B2
公开(公告)日：2017-11-28
申请号：US13375052
申请日：2010-05-26
申请人： Thomas König , Jörg Kirchhoff , Michael Bierdel , Klemens Kohlgrüber , Johann Rechner , Ing. Johan Vaes , Johan Vanden Eynde , Frank Bruynseels , Bert Ruytinx
发明人： Thomas König , Jörg Kirchhoff , Michael Bierdel , Klemens Kohlgrüber , Johann Rechner , Ing. Johan Vaes , Johan Vanden Eynde , Frank Bruynseels , Bert Ruytinx
IPC分类号： C08G64/40 , B29C47/00 , B29C47/40 , B29C47/50 , B29C47/76 , C08G64/20 , B29C47/36 , B29K69/00
CPC分类号： C08G64/406 , B29C47/0019 , B29C47/0033 , B29C47/366 , B29C47/369 , B29C47/40 , B29C47/50 , B29C47/767 , B29K2069/00 , C08G64/205
摘要： The invention relates to polycarbonates with extremely low residual levels of volatile constituents and thermal degradation products, and also improved optical properties, especially Yellowness Index (YI) and good thermal stability, from solvent-containing polymer melts. The invention further relates to an apparatus and a process for preparing these polycarbonates with the aid of a devolatilizing extruder with at least three devolatilizing zones, and zones for introducing entraining agent into dispersion are present upstream of at least three devolatilizing zones.

7. 发明授权

US08497345B2 Device and method for degassing solvent-containing polycarbonate solutions 有权
标题翻译：用于脱气含溶剂的聚碳酸酯溶液的装置和方法
公开(公告)号：US08497345B2
公开(公告)日：2013-07-30
申请号：US13322731
申请日：2010-03-26
申请人： Thomas König , Klemens Kohlgrüber , Johan Vanden Eynde , Ing Johan Vaes , Stefaan De Vos
发明人： Thomas König , Klemens Kohlgrüber , Johan Vanden Eynde , Ing Johan Vaes , Stefaan De Vos
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： B01D19/0031 , B01D19/0005 , B01D19/0052 , B29C47/0009 , B29C47/10 , B29C47/1063 , B29C47/767 , B29K2069/00 , B29K2105/0005 , B29K2105/0008 , B29K2105/0026 , B29K2105/0032 , B29K2105/0038 , B29K2105/0044 , B29K2105/005 , B29K2105/06 , B29K2105/16
摘要： The invention relates to an apparatus and a process for devolatilizing solvent-containing polycarbonate solutions. By employing the inventive apparatus, polycarbonates with low residual values of volatile constituents are produced from solvent-containing polymer melts, which improved optical properties, especially yellowness index, with the aid of an apparatus combination of a flash devolatilizer and a vented extruder.
摘要翻译：本发明涉及一种使含溶剂的聚碳酸酯溶液脱挥发的装置和方法。通过采用本发明的装置，挥发性成分残留值低的聚碳酸酯由含溶剂的聚合物熔体制成，其借助于闪蒸脱挥发器和排气挤出机的装置组合来改善光学特性，特别是黄度指数。

8. 发明授权

US08383757B2 Device and method for degassing solvent-containing polycarbonate solutions 有权
标题翻译：用于脱气含溶剂的聚碳酸酯溶液的装置和方法
公开(公告)号：US08383757B2
公开(公告)日：2013-02-26
申请号：US13318487
申请日：2010-05-26
申请人： Thomas König , Klemens Kohlgrüber , René De Cleyn , Johan Vaes , Johan Vanden Eynde , Dirk Van Meirvenne
发明人： Thomas König , Klemens Kohlgrüber , René De Cleyn , Johan Vaes , Johan Vanden Eynde , Dirk Van Meirvenne
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： B01D19/0031 , B01D19/0005 , B01D19/0052 , B29C47/0009 , B29C47/10 , B29C47/1063 , B29C47/767 , B29K2069/00 , B29K2105/0005 , B29K2105/0008 , B29K2105/0026 , B29K2105/0032 , B29K2105/0038 , B29K2105/0044 , B29K2105/005 , B29K2105/06 , B29K2105/16
摘要： The invention relates to an apparatus and a process for devolatilizing solvent-containing polycarbonate solutions. By employing the inventive apparatus, polycarbonates with low residual values of volatile constituents are produced from solvent-containing polymer melts, which improved optical properties, especially yellowness index, with the aid of an apparatus combination of a heatable tubular devolatilizer and a vented extruder.
摘要翻译：本发明涉及一种使含溶剂的聚碳酸酯溶液脱挥发的装置和方法。通过采用本发明的装置，借助于可加热的管式脱挥发器和通风挤压机的装置组合，由含溶剂的聚合物熔体制备具有低残留值的挥发性成分的聚碳酸酯，其改善了光学性能，特别是黄度指数。

9. 发明申请

US20110184089A1 METHOD FOR THE EXTRUSION OF PLASTIC MATERIALS 审中-公开
标题翻译：挤出塑料材料的方法
公开(公告)号：US20110184089A1
公开(公告)日：2011-07-28
申请号：US13000052
申请日：2009-06-12
申请人： Michael Bierdel , Thomas König , Carsten Conzen , Ulrich Liesenfelder , Klemens Kohlgrüber , Reiner Rudolf , Johann Rechner
发明人： Michael Bierdel , Thomas König , Carsten Conzen , Ulrich Liesenfelder , Klemens Kohlgrüber , Reiner Rudolf , Johann Rechner
IPC分类号： C08J3/20 , C08F14/22 , C08F120/18 , C08F220/44 , C08F14/06 , C08F12/08 , C08F110/06 , C08F110/02 , C08G18/82 , C08G75/23 , C08G64/40 , C08G65/46 , C08G4/00 , C08G63/88 , C08G69/46 , C08G75/14 , C08F299/00 , C08J3/00 , C08F236/10 , C08F236/08 , C08F236/06 , C08F210/16 , C08F236/12 , C08F236/16 , C08F136/18 , C08F218/08 , C08F14/28 , C08F8/38 , C08G77/32 , B29B7/80
CPC分类号： B29B7/489 , B29B7/481 , B29B7/483 , B29B7/484 , B29C48/03 , B29C48/2517 , B29C48/2715 , B29C48/395 , B29C48/402 , B29C48/507 , B29C48/57 , B29C48/64 , B29C48/65
摘要： The invention relates to a process for extruding plastic compositions, in particular polymer melts and mixtures of polymer melts, above all thermoplastics and elastomers, particularly preferably polycarbonate and polycarbonate blends, also with the incorporation of other substances such as for example solids, liquids, gases or other polymers or other polymer blends with improved optical characteristics, with the assistance of a multi-screw extruder with specific screw geometries.
摘要翻译：本发明涉及一种用于挤出塑料组合物，特别是聚合物熔体和聚合物熔体的混合物，尤其是热塑性塑料和弹性体，特别优选聚碳酸酯和聚碳酸酯共混物的方法，还包括其它物质，例如固体，液体，气体或具有改进的光学特性的其他聚合物或其它聚合物共混物，借助于具有特定螺杆几何形状的多螺杆挤出机。

10. 发明授权

US09738025B2 Method for extruding plastic masses 有权
公开(公告)号：US09738025B2
公开(公告)日：2017-08-22
申请号：US13000057
申请日：2009-05-30
申请人： Thomas König , Michael Bierdel , Carsten Conzen , Ulrich Liesenfelder , Klemens Kohlgrüber , Reiner Rudolf , Johann Rechner
发明人： Thomas König , Michael Bierdel , Carsten Conzen , Ulrich Liesenfelder , Klemens Kohlgrüber , Reiner Rudolf , Johann Rechner
IPC分类号： B29C47/08 , B29B7/48 , B29C47/38 , B29C47/40 , B29C47/64 , B29C47/62 , B29C47/60 , B29C47/00
CPC分类号： B29C47/0861 , B29B7/481 , B29C47/0009 , B29C47/0881 , B29C47/38 , B29C47/402 , B29C47/6056 , B29C47/6075 , B29C47/625 , B29C47/627 , B29C47/64 , Y02P70/263
摘要： The invention relates to a process for extruding plastic compositions. The process in particular relates to the conveying, kneading and/or mixing of plastic compositions, in particular of polymer melts and mixtures of polymer melts, above all thermoplastics and elastomers, particularly preferably polycarbonate and polycarbonate blends, also with the incorporation of other substances such as for example solids, liquids, gases or other polymers or other polymer blends.

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