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1. 发明申请

US20120108782A1 DEVICE AND METHOD FOR DEGASSING SOLVENT-CONTAINING POLYCARBONATE SOLUTIONS 有权
标题翻译：用于溶解含溶剂的聚碳酸酯溶液的装置和方法
公开(公告)号：US20120108782A1
公开(公告)日：2012-05-03
申请号：US13318487
申请日：2010-05-26
申请人： Thomas König , Klemens Kohlgrüber , René De Cleyn , Johan Vaes , Johan Vanden Eynde , Dirk Van Meirvenne
发明人： Thomas König , Klemens Kohlgrüber , René De Cleyn , Johan Vaes , Johan Vanden Eynde , Dirk Van Meirvenne
IPC分类号： C08G64/40 , B29B13/00
CPC分类号： B01D19/0031 , B01D19/0005 , B01D19/0052 , B29C47/0009 , B29C47/10 , B29C47/1063 , B29C47/767 , B29K2069/00 , B29K2105/0005 , B29K2105/0008 , B29K2105/0026 , B29K2105/0032 , B29K2105/0038 , B29K2105/0044 , B29K2105/005 , B29K2105/06 , B29K2105/16
摘要： The invention relates to an apparatus and a process for devolatilizing solvent-containing polycarbonate solutions. By employing the inventive apparatus, polycarbonates with low residual values of volatile constituents are produced from solvent-containing polymer melts, which improved optical properties, especially yellowness index, with the aid of an apparatus combination of a heatable tubular devolatilizer and a vented extruder.
摘要翻译：本发明涉及一种使含溶剂的聚碳酸酯溶液脱挥发的装置和方法。通过采用本发明的装置，借助于可加热的管式脱挥发器和通风挤压机的装置组合，由含溶剂的聚合物熔体制备具有低残留值的挥发性成分的聚碳酸酯，其改善了光学性能，特别是黄度指数。

2. 发明授权

US08383757B2 Device and method for degassing solvent-containing polycarbonate solutions 有权
标题翻译：用于脱气含溶剂的聚碳酸酯溶液的装置和方法
公开(公告)号：US08383757B2
公开(公告)日：2013-02-26
申请号：US13318487
申请日：2010-05-26
申请人： Thomas König , Klemens Kohlgrüber , René De Cleyn , Johan Vaes , Johan Vanden Eynde , Dirk Van Meirvenne
发明人： Thomas König , Klemens Kohlgrüber , René De Cleyn , Johan Vaes , Johan Vanden Eynde , Dirk Van Meirvenne
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： B01D19/0031 , B01D19/0005 , B01D19/0052 , B29C47/0009 , B29C47/10 , B29C47/1063 , B29C47/767 , B29K2069/00 , B29K2105/0005 , B29K2105/0008 , B29K2105/0026 , B29K2105/0032 , B29K2105/0038 , B29K2105/0044 , B29K2105/005 , B29K2105/06 , B29K2105/16
摘要： The invention relates to an apparatus and a process for devolatilizing solvent-containing polycarbonate solutions. By employing the inventive apparatus, polycarbonates with low residual values of volatile constituents are produced from solvent-containing polymer melts, which improved optical properties, especially yellowness index, with the aid of an apparatus combination of a heatable tubular devolatilizer and a vented extruder.
摘要翻译：本发明涉及一种使含溶剂的聚碳酸酯溶液脱挥发的装置和方法。通过采用本发明的装置，借助于可加热的管式脱挥发器和通风挤压机的装置组合，由含溶剂的聚合物熔体制备具有低残留值的挥发性成分的聚碳酸酯，其改善了光学性能，特别是黄度指数。

3. 发明授权

US09828464B2 Ultra-high purity polycarbonates having good inherent color and thermal resistance and a device and a method for producing the same 有权
公开(公告)号：US09828464B2
公开(公告)日：2017-11-28
申请号：US13375052
申请日：2010-05-26
申请人： Thomas König , Jörg Kirchhoff , Michael Bierdel , Klemens Kohlgrüber , Johann Rechner , Ing. Johan Vaes , Johan Vanden Eynde , Frank Bruynseels , Bert Ruytinx
发明人： Thomas König , Jörg Kirchhoff , Michael Bierdel , Klemens Kohlgrüber , Johann Rechner , Ing. Johan Vaes , Johan Vanden Eynde , Frank Bruynseels , Bert Ruytinx
IPC分类号： C08G64/40 , B29C47/00 , B29C47/40 , B29C47/50 , B29C47/76 , C08G64/20 , B29C47/36 , B29K69/00
CPC分类号： C08G64/406 , B29C47/0019 , B29C47/0033 , B29C47/366 , B29C47/369 , B29C47/40 , B29C47/50 , B29C47/767 , B29K2069/00 , C08G64/205
摘要： The invention relates to polycarbonates with extremely low residual levels of volatile constituents and thermal degradation products, and also improved optical properties, especially Yellowness Index (YI) and good thermal stability, from solvent-containing polymer melts. The invention further relates to an apparatus and a process for preparing these polycarbonates with the aid of a devolatilizing extruder with at least three devolatilizing zones, and zones for introducing entraining agent into dispersion are present upstream of at least three devolatilizing zones.

4. 发明授权

US08497345B2 Device and method for degassing solvent-containing polycarbonate solutions 有权
标题翻译：用于脱气含溶剂的聚碳酸酯溶液的装置和方法
公开(公告)号：US08497345B2
公开(公告)日：2013-07-30
申请号：US13322731
申请日：2010-03-26
申请人： Thomas König , Klemens Kohlgrüber , Johan Vanden Eynde , Ing Johan Vaes , Stefaan De Vos
发明人： Thomas König , Klemens Kohlgrüber , Johan Vanden Eynde , Ing Johan Vaes , Stefaan De Vos
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： B01D19/0031 , B01D19/0005 , B01D19/0052 , B29C47/0009 , B29C47/10 , B29C47/1063 , B29C47/767 , B29K2069/00 , B29K2105/0005 , B29K2105/0008 , B29K2105/0026 , B29K2105/0032 , B29K2105/0038 , B29K2105/0044 , B29K2105/005 , B29K2105/06 , B29K2105/16
摘要： The invention relates to an apparatus and a process for devolatilizing solvent-containing polycarbonate solutions. By employing the inventive apparatus, polycarbonates with low residual values of volatile constituents are produced from solvent-containing polymer melts, which improved optical properties, especially yellowness index, with the aid of an apparatus combination of a flash devolatilizer and a vented extruder.
摘要翻译：本发明涉及一种使含溶剂的聚碳酸酯溶液脱挥发的装置和方法。通过采用本发明的装置，挥发性成分残留值低的聚碳酸酯由含溶剂的聚合物熔体制成，其借助于闪蒸脱挥发器和排气挤出机的装置组合来改善光学特性，特别是黄度指数。

5. 发明申请

US20120123084A1 DEVICE AND METHOD FOR DEGASSING SOLVENT-CONTAINING POLYCARBONATE SOLUTIONS 有权
标题翻译：用于溶解含溶剂的聚碳酸酯溶液的装置和方法
公开(公告)号：US20120123084A1
公开(公告)日：2012-05-17
申请号：US13322731
申请日：2010-03-26
申请人： Thomas König , Klemens Kohlgrüber , Johan Vanden Eynde , Johan Vaes , Stefaan De Vos
发明人： Thomas König , Klemens Kohlgrüber , Johan Vanden Eynde , Johan Vaes , Stefaan De Vos
IPC分类号： C08G64/40 , B01D1/00
CPC分类号： B01D19/0031 , B01D19/0005 , B01D19/0052 , B29C47/0009 , B29C47/10 , B29C47/1063 , B29C47/767 , B29K2069/00 , B29K2105/0005 , B29K2105/0008 , B29K2105/0026 , B29K2105/0032 , B29K2105/0038 , B29K2105/0044 , B29K2105/005 , B29K2105/06 , B29K2105/16
摘要： The invention relates to an apparatus and a process for devolatilizing solvent-containing polycarbonate solutions. By employing the inventive apparatus, polycarbonates with low residual values of volatile constituents are produced from solvent-containing polymer melts, which improved optical properties, especially yellowness index, with the aid of an apparatus combination of a flash devolatilizer and a vented extruder.
摘要翻译：本发明涉及一种使含溶剂的聚碳酸酯溶液脱挥发的装置和方法。通过采用本发明的装置，挥发性成分残留值低的聚碳酸酯由含溶剂的聚合物熔体制成，其借助于闪蒸脱挥发器和排气挤出机的装置组合来改善光学性能，特别是黄度指数。

6. 发明授权

US07129315B2 Process for the production of polycarbonate 有权
标题翻译：聚碳酸酯生产工艺
公开(公告)号：US07129315B2
公开(公告)日：2006-10-31
申请号：US11105680
申请日：2005-04-14
申请人： Jörg Kirchhoff , Thomas König , Klemens Kohlgrüber , Steffen Kühling , Dirk Van Meirvenne
发明人： Jörg Kirchhoff , Thomas König , Klemens Kohlgrüber , Steffen Kühling , Dirk Van Meirvenne
IPC分类号： C08G64/00
CPC分类号： C08G64/403 , C08G64/205
摘要： A process for the isolation of polycarbonate produced by the interfacial polymerization process is disclosed. Accordingly, the process entails (a) evaporating the organic solvent from the solution that contains solvent and polycarbonate to obtain a material system that contains 90 to 99.95% polycarbonate, the percent being relative to the weight of the system, and (b) passing the material system through inlet openings of a separating vessel to obtain a plurality of streams of polycarbonate, on entry into the inlet openings said material system being supersaturated with volatile constituents to an extent of at least 1 bar and having a temperature of 250° to 340° C. and a flow rate of 0.1 to 20 kg/hour, and (c) degassing the streams in the separating vessel wherein the pressure is 0.1 to 20 mbar to effect degassing of the polycarbonate.
摘要翻译：公开了通过界面聚合方法分离聚碳酸酯的方法。因此，该方法需要（a）从含有溶剂和聚碳酸酯的溶液中蒸发有机溶剂以获得含有90至99.95％聚碳酸酯的材料体系，其百分数相对于体系重量，和（b）使材料系统通过分离容器的入口开口，以获得多个聚碳酸酯流，在进入入口时，所述材料体系用挥发性成分过饱和至少1巴，温度为250°至340° 并且流速为0.1至20kg /小时，和（c）使分离容器中的气流脱气，其中压力为0.1至20毫巴，以实现聚碳酸酯脱气。

7. 发明授权

US07091302B2 Process for the preparation of polycarbonate 有权
标题翻译：制备聚碳酸酯的方法
公开(公告)号：US07091302B2
公开(公告)日：2006-08-15
申请号：US11105678
申请日：2005-04-14
申请人： Jörg Kirchhoff , Thomas König , Klemens Kohlgrüber , Steffen Kühling , Melanie Möthrath , Dirk Van Meirvenne
发明人： Jörg Kirchhoff , Thomas König , Klemens Kohlgrüber , Steffen Kühling , Melanie Möthrath , Dirk Van Meirvenne
IPC分类号： C08G64/00
CPC分类号： C08G64/205 , C08G64/307
摘要： The invention describes a process for the preparation of polycarbonate. The process includes (a) transesterifying at least one aromatic dihydroxyaryl compound and a diaryl carbonate in the melt in the presence of a catalyst, (b) mixing the melt obtained in step (a) with a foaming agent (c) passing the mixture at 250 to 340° C. through inlet openings of a separating vessel at a rate of 0.1 to 20 kg/hour, to obtain a plurality of streams of foamed polycarbonate and degassing the streams of foamed polycarbonate in the separating vessel wherein the pressure is 0.1 to 20 mbar.
摘要翻译：本发明描述了制备聚碳酸酯的方法。该方法包括（a）在催化剂存在下，在熔体中将至少一种芳族二羟基芳基化合物和碳酸二芳基酯酯交换反应，（b）将步骤（a）中获得的熔体与通过该混合物的发泡剂（c）通过分离容器的入口开口以0.1至20kg /小时的速度通过入口开口250至340℃，以获得多个发泡聚碳酸酯流并在分离容器中对发泡聚碳酸酯流进行脱气，其中压力为0.1至 20毫巴

8. 发明申请

US20120157653A1 ULTRA-HIGH PURITY POLYCARBONATES HAVING GOOD INHERENT COLOR AND THERMAL RESISTANCE AND A DEVICE AND A METHOD FOR PRODUCING THE SAME 有权
标题翻译：具有良好的颜色和耐热性的超高纯度聚碳酸酯及其制造方法
公开(公告)号：US20120157653A1
公开(公告)日：2012-06-21
申请号：US13375052
申请日：2010-05-26
申请人： Thomas König , Jörg Kirchhoff , Michael Bierdel , Klemens Kohlgrüber , Johann Rechner , Ing Johan Vaes , Johan Vander Eynde , Frank Bruynseels , Bert Ruytinx
发明人： Thomas König , Jörg Kirchhoff , Michael Bierdel , Klemens Kohlgrüber , Johann Rechner , Ing Johan Vaes , Johan Vander Eynde , Frank Bruynseels , Bert Ruytinx
IPC分类号： C08G64/40 , B01D1/00 , C08G64/20
CPC分类号： C08G64/406 , B29C47/0019 , B29C47/0033 , B29C47/366 , B29C47/369 , B29C47/40 , B29C47/50 , B29C47/767 , B29K2069/00 , C08G64/205
摘要： The invention relates to polycarbonates with extremely low residual levels of volatile constituents and thermal degradation products, and also improved optical properties, especially Yellowness Index (YI) and good thermal stability, from solvent-containing polymer melts. The invention further relates to an apparatus and a process for preparing these polycarbonates with the aid of a devolatilizing extruder with at least three devolatilizing zones, and zones for introducing entraining agent into dispersion are present upstream of at least three devolatilizing zones.
摘要翻译：本发明涉及具有极低残留水平的挥发性成分和热降解产物的聚碳酸酯，以及由含溶剂聚合物熔体改善的光学性能，特别是黄度指数（YI）和良好的热稳定性。本发明还涉及一种借助于具有至少三个脱挥发区的脱挥发分挤压机制备这些聚碳酸酯的装置和方法，并且在至少三个脱挥发区的上游存在用于将夹带剂引入分散体的区域。

9. 发明授权

US07144981B2 Process for separating volatile components from polymers 失效
标题翻译：挥发性组分与聚合物分离的方法
公开(公告)号：US07144981B2
公开(公告)日：2006-12-05
申请号：US10684600
申请日：2003-10-14
申请人： Thomas König , Klemens Kohlgrüber , Ulrich Liesenfelder , Michael Bierdel , Helmut Meyer , Richard Weider , Jörg Krüger
发明人： Thomas König , Klemens Kohlgrüber , Ulrich Liesenfelder , Michael Bierdel , Helmut Meyer , Richard Weider , Jörg Krüger
IPC分类号： C08F6/00
CPC分类号： C08F6/003
摘要： A process for concentrating polymers by evaporation is disclosed. The process entails (i) obtaining a mixture containing a polymer and volatile component, the volatile components being present in the mixture at an amount less than 20 wt. % relative to the weight of the mixture, and (ii) introducing the mixture in a downward direction under pressure through a plurality of nozzles arranged vertically and next to one another into a degassing container to form an extrudate. The volatile component contains at least one of residual monomers, oligomers and solvents, and the throughput of the mixture per nozzle is 0.3 to 2 kg/h. The vapor pressure of the volatile component of the extrudate is more than 2.5 bar, and the absolute pressure in the degassing container is 50 to 5000 Pa. The polymer prepared by the process is characterized in that it contains volatile components in an amount of less than 300 ppm.
摘要翻译：公开了通过蒸发浓缩聚合物的方法。该方法需要（i）获得含有聚合物和挥发性组分的混合物，所述挥发性组分以小于20重量％的量存在于混合物中。相对于混合物重量的％，和（ii）通过垂直且彼此相邻布置的多个喷嘴在压力下向下引入混合物到脱气容器中以形成挤出物。挥发性组分含有残留单体，低聚物和溶剂中的至少一种，并且每个喷嘴的混合物的生产量为0.3至2kg / h。挤出物的挥发性成分的蒸气压大于2.5巴，脱气容器中的绝对压力为50〜5000Pa。本方法制备的聚合物的特征在于，其含有挥发性成分的量小于 300 ppm。

10. 发明申请

US20110184089A1 METHOD FOR THE EXTRUSION OF PLASTIC MATERIALS 审中-公开
标题翻译：挤出塑料材料的方法
公开(公告)号：US20110184089A1
公开(公告)日：2011-07-28
申请号：US13000052
申请日：2009-06-12
申请人： Michael Bierdel , Thomas König , Carsten Conzen , Ulrich Liesenfelder , Klemens Kohlgrüber , Reiner Rudolf , Johann Rechner
发明人： Michael Bierdel , Thomas König , Carsten Conzen , Ulrich Liesenfelder , Klemens Kohlgrüber , Reiner Rudolf , Johann Rechner
IPC分类号： C08J3/20 , C08F14/22 , C08F120/18 , C08F220/44 , C08F14/06 , C08F12/08 , C08F110/06 , C08F110/02 , C08G18/82 , C08G75/23 , C08G64/40 , C08G65/46 , C08G4/00 , C08G63/88 , C08G69/46 , C08G75/14 , C08F299/00 , C08J3/00 , C08F236/10 , C08F236/08 , C08F236/06 , C08F210/16 , C08F236/12 , C08F236/16 , C08F136/18 , C08F218/08 , C08F14/28 , C08F8/38 , C08G77/32 , B29B7/80
CPC分类号： B29B7/489 , B29B7/481 , B29B7/483 , B29B7/484 , B29C48/03 , B29C48/2517 , B29C48/2715 , B29C48/395 , B29C48/402 , B29C48/507 , B29C48/57 , B29C48/64 , B29C48/65
摘要： The invention relates to a process for extruding plastic compositions, in particular polymer melts and mixtures of polymer melts, above all thermoplastics and elastomers, particularly preferably polycarbonate and polycarbonate blends, also with the incorporation of other substances such as for example solids, liquids, gases or other polymers or other polymer blends with improved optical characteristics, with the assistance of a multi-screw extruder with specific screw geometries.
摘要翻译：本发明涉及一种用于挤出塑料组合物，特别是聚合物熔体和聚合物熔体的混合物，尤其是热塑性塑料和弹性体，特别优选聚碳酸酯和聚碳酸酯共混物的方法，还包括其它物质，例如固体，液体，气体或具有改进的光学特性的其他聚合物或其它聚合物共混物，借助于具有特定螺杆几何形状的多螺杆挤出机。

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