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1. 发明授权

US06534619B1 Method for evaporating polymer solutions of thermoplastic polymers 失效
标题翻译：蒸发热塑性聚合物聚合物溶液的方法
公开(公告)号：US06534619B1
公开(公告)日：2003-03-18
申请号：US09762366
申请日：2001-02-05
申请人： Thomas Elsner , Jürgen Heuser , Klemens Kohlgrüber , Christian Kords
发明人： Thomas Elsner , Jürgen Heuser , Klemens Kohlgrüber , Christian Kords
IPC分类号： C08G8102
CPC分类号： B01D19/0047 , B01D3/06 , B01D3/065 , C08F6/003 , C08G64/406
摘要： This invention relates to a multistep process for evaporating polymer solutions of thermoplastic polymers and for removing volatile constituents from thermoplastic polymers by indirect heat exchange. The invention relates in particular to a process for evaporating volatile constituents out of polymer solutions using shell-and-tube heat exchangers having a special geometry, coiled-tube evaporators and extrusion evaporators.
摘要翻译：本发明涉及用于蒸发热塑性聚合物的聚合物溶液并通过间接热交换从热塑性聚合物中除去挥发性成分的多步法。本发明特别涉及一种使用具有特殊几何形状的管壳式热交换器，螺旋管式蒸发器和挤出蒸发器从聚合物溶液中蒸发挥发性成分的方法。

2. 发明授权

US06506281B1 Method for isolating polymers from solutions 失效
标题翻译：从溶液中分离聚合物的方法
公开(公告)号：US06506281B1
公开(公告)日：2003-01-14
申请号：US09719891
申请日：2001-03-02
申请人： Clemens Casper , Jörgen Weinschenck , Klemens Kohlgrüber , Jürgen Heuser , Christian Kords , Thomas Elsner
发明人： Clemens Casper , Jörgen Weinschenck , Klemens Kohlgrüber , Jürgen Heuser , Christian Kords , Thomas Elsner
IPC分类号： B01D122
CPC分类号： B01D3/06 , C08G64/406 , Y10S159/08 , Y10S159/10
摘要： A process of evaporating a viscous polymer solution is described. The process includes: (a) providing a viscous polymer solution including at least 30 wt. % of solvents and monomers; (b) introducing the viscous polymer solution into a heated helix (5), the heated helix having a vapor exit velocity of 200 to 300 m/s, (a film flow including a two-phase mixture of polymer melt, and solvent vapors and monomer vapors being formed within the helix); (c) forwarding the film flow from helix (5) into a heated vapor separator (6); (d) expanding the two-phase mixture of polymer melt, and solvent vapors and monomer vapors of the film flow within vapor separator (6) at an absolute pressure of 10 mbar to 800 mbar, (a bottom product including a concentrated melt of the polymer is formed within the vapor separator); and (e) withdrawing the bottom product from vapor separator (6). Each of the helix (5) and vapor separator (6) have a separate heating device, and each of heating device independently provides a temperature that is above the softening point of the polymer.
摘要翻译：描述蒸发粘性聚合物溶液的方法。该方法包括：（a）提供粘性聚合物溶液，其包含至少30wt。％的溶剂和单体; （b）将粘性聚合物溶液引入加热的螺旋（5）中，加热的螺旋具有200-300m / s的蒸气出口速度（包括聚合物熔体和溶剂蒸气的两相混合物的膜流和单体蒸气在螺旋内形成）; （c）将膜流从螺旋（5）转移到加热的蒸气分离器（6）中; （d）在10毫巴至800毫巴的绝对压力下，将蒸气分离器（6）内的聚合物熔体和溶剂蒸气和单体蒸气的溶剂蒸气和单体蒸气膨胀（包括含有聚合物形成在蒸气分离器内）; 和（e）从蒸气分离器（6）中取出底部产物。螺旋（5）和蒸汽分离器（6）中的每一个具有单独的加热装置，并且每个加热装置独立地提供高于聚合物软化点的温度。

3. 发明授权

US06780281B1 Strand evaporator 失效
标题翻译：绞线蒸发器
公开(公告)号：US06780281B1
公开(公告)日：2004-08-24
申请号：US10130757
申请日：2002-05-22
申请人： Thomas Elsner , Jürgen Heuser , Christian Kords , Klemens Kohlgrüber
发明人： Thomas Elsner , Jürgen Heuser , Christian Kords , Klemens Kohlgrüber
IPC分类号： B01D108
CPC分类号： B01D1/06 , B01D1/04 , B01D3/008 , B01D19/0021 , B29C47/0019 , B29C47/003 , B29C47/76 , C08F6/003 , Y10S159/10 , Y10S159/15
摘要： A strand devolatilizer that includes a degassing container, a product inlet, a product distributor, a product outlet and a vapor outlet is disclosed. The product distributor is in the form of a tube distributor with at least one distributor tube (1) and a plurality of die tubes (2) arranged in parallel, each containing a plurality of apertures (15) in the tube wall. The die tubes (2) are preferably arranged in several planes one above the other and staggered laterally relative to one another.
摘要翻译：公开了一种包含脱气容器，产品入口，产品分配器，产品出口和蒸汽出口的脱脂剂。产品分配器是具有管分配器的形式，具有至少一个分配器管（1）和平行布置的多个模具管（2），每个在管壁中包含多个孔（15）。模具管（2）优选地布置在多个平面中，并且彼此相对并且彼此横向错开。

4. 发明授权

US07138478B2 Process for mixing polymer melts with additives 有权
标题翻译：聚合物熔体与添加剂混合的方法
公开(公告)号：US07138478B2
公开(公告)日：2006-11-21
申请号：US10825887
申请日：2004-04-16
申请人： Klemens Kohlgrüber , Günther Holdenried , Christian Kords , Jürgen Heuser , Thomas König
发明人： Klemens Kohlgrüber , Günther Holdenried , Christian Kords , Jürgen Heuser , Thomas König
IPC分类号： C08G64/00
CPC分类号： B29B7/94 , B29B7/325 , B29C47/64 , B29K2069/00 , C08L69/00
摘要： A continuous process for mixing polymer melts with additives, in particular polycarbonate melts with additives in liquid form, in solution or in dispersion is described. The additives are added to a main stream of polymer melt and are then mixed, preferably directly, with the main stream in a static mixer.
摘要翻译：描述了将聚合物熔体与添加剂，特别是具有液体形式的添加剂的聚碳酸酯熔体在溶液或分散体中混合的连续方法。将添加剂加入到聚合物熔体的主流中，然后优选直接与主流在静态混合器中混合。

5. 发明授权

US06811294B1 Device and method for degassing plastics 有权
标题翻译：塑料脱气装置及方法
公开(公告)号：US06811294B1
公开(公告)日：2004-11-02
申请号：US09937467
申请日：2001-09-25
申请人： Thomas Elsner , Jürgen Heuser , Christian Kords
发明人： Thomas Elsner , Jürgen Heuser , Christian Kords
IPC分类号： B29B748
CPC分类号： B29C47/767 , B29C47/0009 , B29C47/762 , B29C47/825 , C08G64/406
摘要： An apparatus for degassing plastic materials, e.g., high molecular weight polycarbonate solutions, is described. The apparatus includes a double-shaft extruder having a length-to-diameter ratio of less than or equal to 40, which comprises: (i) two co-rotating and meshing shafts; (ii) an intake opening; and (iii) upstream and downstream portions relative to the intake opening. The shafts of the extruder are designed with a double lead in a degassing zone, and with a triple lead in a pressure build-up zone. Each of the degassing and the pressure build-up zones are down-stream from the intake opening, and the pressure build-up zone is further down-stream than the degassing zone. Also described is a process for degassing plastic materials, which involves providing the described double-shaft co-rotating extruder, into which plastic material is fed, processed and degassed. Entraining agents, such as nitrogen, and other processing additives may be introduced into an extruder during the process of the present invention.
摘要翻译：描述了用于对塑料材料（例如高分子量聚碳酸酯溶液）进行脱气的设备。该设备包括长径比小于或等于40的双轴挤出机，其包括：（i）两个共同旋转和啮合的轴; （ii）进气口; 和（iii）相对于进气口的上游和下游部分。挤出机的轴设计为具有脱气区域中的双引线，并且在压力增加区域中具有三重引线。每个脱气和压力积聚区域从进气口向下游，并且压力积聚区域比脱气区域进一步下游。还描述了一种用于对塑料材料进行脱气的方法，其涉及提供所描述的双轴同向旋转挤出机，塑料进料，加工和脱气。在本发明的方法中，可将引入剂如氮气和其它加工添加剂引入挤出机中。

6. 发明授权

US06720406B1 High-purity polymer granules and method for the production thereof 失效
标题翻译：高纯度聚合物颗粒及其制备方法
公开(公告)号：US06720406B1
公开(公告)日：2004-04-13
申请号：US10111999
申请日：2002-04-30
申请人： Thomas Elsner , Jürgen Heuser , Christian Kords , Steffen Kühling , Paul Viroux
发明人： Thomas Elsner , Jürgen Heuser , Christian Kords , Steffen Kühling , Paul Viroux
IPC分类号： C08F600
CPC分类号： C08J3/12 , B29B9/06 , B29C2791/005 , B29K2069/00 , C08J2369/00 , G11B7/2534
摘要： A process for producing polymer pellets is disclosed. The process that is particular suitable for making polycarbonate pellets entails extruding a polymer melt, cooling the extrudate by contacting it with a cooling fluid and pelletizing the solidified polymer. The process is characterized in that the cooling fluid has a solids particle content of at most 10 ppm.
摘要翻译：公开了制备聚合物颗粒的方法。特别适用于制备聚碳酸酯颗粒的方法需要挤出聚合物熔体，通过使其与冷却流体接触并使固化的聚合物造粒来冷却挤出物。该方法的特征在于冷却流体的固体颗粒含量至多为10ppm。

7. 发明授权

US06627040B1 Device and method for removing volatile components from polymer solutions 失效
标题翻译：用于从聚合物溶液中除去挥发性组分的装置和方法
公开(公告)号：US06627040B1
公开(公告)日：2003-09-30
申请号：US09673225
申请日：2000-10-13
申请人： Thomas Elsner , Jürgen Heuser , Christian Kords
发明人： Thomas Elsner , Jürgen Heuser , Christian Kords
IPC分类号： B01D306
CPC分类号： C08F6/003 , F28D9/0018 , Y10S159/10 , Y10S159/15
摘要： A device and process for the removal of volatile constituents from polymers is disclosed. The device entails a container having an inlet for a polymer solution, an outlet for the volatile components, an outflow for the polymer from which the volatile components have been removed and a heat exchanger. The heat exchanger is characterized in that it contains a plurality of specially structured channels.
摘要翻译：公开了用于从聚合物中除去挥发性成分的装置和方法。该装置需要具有用于聚合物溶液的入口，用于挥发性组分的出口，已经除去挥发性组分的聚合物的流出物和热交换器的容器。热交换器的特征在于它包含多个特别结构的通道。

8. 发明授权

US06551538B1 Vacuole-free polymer granulates 失效
标题翻译：无空气聚合物颗粒
公开(公告)号：US06551538B1
公开(公告)日：2003-04-22
申请号：US09647227
申请日：2000-09-27
申请人： Thomas Elsner , Jürgen Heuser , Christian Kords
发明人： Thomas Elsner , Jürgen Heuser , Christian Kords
IPC分类号： B29C4700
CPC分类号： C08J3/12 , B29C2035/1616 , B29K2069/00 , C08J2369/00
摘要： A process for preparing a vacuole-free polymer is disclosed. Extruded polymer resin is cooled at a rate of less than 50° C./sec. to a temperature that is 1 to 20° C. above the glass transition temperature of the polymer resin and the resin is then cut.
摘要翻译：公开了一种制备无液泡聚合物的方法。挤出的聚合物树脂以小于50℃/秒的速率冷却。达到高于聚合物树脂的玻璃化转变温度1℃至20℃的温度，然后切割树脂。

9. 发明授权

US06485607B1 Methods for removing volatile components from polymer solutions 失效
标题翻译：从聚合物溶液中除去挥发性组分的方法
公开(公告)号：US06485607B1
公开(公告)日：2002-11-26
申请号：US09673227
申请日：2000-10-13
申请人： Thomas Elsner , Jürgen Heuser , Christian Kords
发明人： Thomas Elsner , Jürgen Heuser , Christian Kords
IPC分类号： B01D130
CPC分类号： C08G64/406 , C08F6/003 , Y10S159/08 , Y10S159/15
摘要： A method for removing volatile components from polymer solutions is disclosed. The method, yielding products having low content of residual volatile components and causing no thermal damage to the polymer, entails using apparatuses in which surfaces which come into contact with the product are made from materials which are low in iron content.
摘要翻译：公开了从聚合物溶液中除去挥发性组分的方法。产生具有低残留挥发性成分含量且不对聚合物造成热损伤的产品需要使用与产品接触的表面由铁含量低的材料制成的设备。

10. 发明授权

US06620906B1 Method for the production of highly pure polycarbonate and ultrapure polycarbonate 失效
标题翻译：生产高纯度聚碳酸酯和超纯聚碳酸酯的方法
公开(公告)号：US06620906B1
公开(公告)日：2003-09-16
申请号：US10182964
申请日：2002-08-02
申请人： Thomas Elsner , Jürgen Heuser , Christian Kords
发明人： Thomas Elsner , Jürgen Heuser , Christian Kords
IPC分类号： C08G6400
CPC分类号： B01D3/06 , C08G64/403 , C08G64/406
摘要： The present invention provides a polycarbonate having a low particle content, a process for producing high-purity polycarbonate and polycarbonate of maximum purity and molded products made from such polycarbonate.
摘要翻译：本发明提供了具有低颗粒含量的聚碳酸酯，用于生产高纯度聚碳酸酯的方法和最高纯度的聚碳酸酯以及由这种聚碳酸酯制成的模塑产品。

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