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1. 发明申请

US20130197281A1 PROCESS FOR MANUFACTURING PERFLUOROOLEFINS BY PYROLYSIS OF PERFLUOROCARBONS IN THE PRESENCE OF HYDROGEN 有权
标题翻译：在氢存在下通过氟化氢热解制备全氟烯烃的方法
公开(公告)号：US20130197281A1
公开(公告)日：2013-08-01
申请号：US13805561
申请日：2011-06-27
申请人： Klaus Hintzer , André Streiter , Günther J. Kämpf , Kai Helmut Lochhaas , Michael Jürgens , Oleg Shyshkov , Tilman C. Zipplies , Jürgen Troe , Klaus Luther
发明人： Klaus Hintzer , André Streiter , Günther J. Kämpf , Kai Helmut Lochhaas , Michael Jürgens , Oleg Shyshkov , Tilman C. Zipplies , Jürgen Troe , Klaus Luther
IPC分类号： C07C17/25
CPC分类号： C07C17/25 , C07C17/23 , C07C17/278 , C07C17/281 , C07C17/361 , C07C21/185 , C07C21/18
摘要： A process is described of pyrolyzing at least one perfluorinated hydrocarbon, or a material containing at least one perfluorinated hydrocarbon, in the presence of hydrogen, to yield a reaction mixture containing difluorocarbene.
摘要翻译：描述了在氢的存在下热解至少一种全氟化烃或含有至少一种全氟化烃的材料的方法，得到含有二氟卡宾的反应混合物。

2. 发明授权

US09139496B2 Process for manufacturing perfluoroolefins by pyrolysis of perfluorocarbons in the presence of hydrogen 有权
标题翻译：通过在氢气存在下热解全氟化碳制备全氟烯烃的方法
公开(公告)号：US09139496B2
公开(公告)日：2015-09-22
申请号：US13805561
申请日：2011-06-27
申请人： Klaus Hintzer , André Streiter , Günther J. Kämpf , Kai Helmut Lochhaas , Michael Jürgens , Oleg Shyshkov , Tilman C. Zipplies , Jürgen Troe , Klaus Luther
发明人： Klaus Hintzer , André Streiter , Günther J. Kämpf , Kai Helmut Lochhaas , Michael Jürgens , Oleg Shyshkov , Tilman C. Zipplies , Jürgen Troe , Klaus Luther
IPC分类号： C07C17/23 , C07C21/18 , C07C21/185 , C07C17/25 , C07C17/278 , C07C17/281 , C07C17/361
CPC分类号： C07C17/25 , C07C17/23 , C07C17/278 , C07C17/281 , C07C17/361 , C07C21/185 , C07C21/18
摘要： A process is described of pyrolyzing at least one perfluorinated hydrocarbon, or a material containing at least one perfluorinated hydrocarbon, in the presence of hydrogen, to yield a reaction mixture containing difluorocarbene.
摘要翻译：描述了在氢的存在下热解至少一种全氟化烃或含有至少一种全氟化烃的材料的方法，得到含有二氟卡宾的反应混合物。

3. 发明申请

US20120245384A1 METHOD OF PREPARING HIGHLY FLUORINATED CARBOXYLIC ACIDS AND THEIR SALTS 有权
标题翻译：制备高度氟化的羧酸及其盐的方法
公开(公告)号：US20120245384A1
公开(公告)日：2012-09-27
申请号：US13511939
申请日：2010-11-18
申请人： Klaus Hintzer , Tilman C. Zipplies , Oleg Shyshkov
发明人： Klaus Hintzer , Tilman C. Zipplies , Oleg Shyshkov
IPC分类号： C07B39/00
CPC分类号： C07C51/353 , C07C67/347 , C07C231/12 , C07C53/21 , C07C69/708 , C07C235/06
摘要： A method for preparing highly fluorinated carboxylic acids and theirs salts and the precursors thereof.
摘要翻译：一种制备高度氟化的羧酸及其盐及其前体的方法。

4. 发明授权

US09453086B2 Fluoropolymer compositions and purification methods thereof 有权
标题翻译：含氟聚合物组合物及其纯化方法
公开(公告)号：US09453086B2
公开(公告)日：2016-09-27
申请号：US13995615
申请日：2011-12-21
申请人： Klaus Hintzer , Michael Juergens , Gunther J. Kaempf , Harald Kaspar , Kai H. Lochhaas , Andre Streiter , Oleg Shyshkov , Tilman C. Zipplies , Herbert Koenigsmann
发明人： Klaus Hintzer , Michael Juergens , Gunther J. Kaempf , Harald Kaspar , Kai H. Lochhaas , Andre Streiter , Oleg Shyshkov , Tilman C. Zipplies , Herbert Koenigsmann
IPC分类号： C08F14/18 , C02F1/461 , C02F1/26 , C08F14/08
CPC分类号： C08F6/003 , C02F1/26 , C02F1/461 , C02F2001/46138 , C02F2001/46147 , C08F2/10 , C08F2/20 , C08F14/08 , C08F14/18 , C08F2800/10 , Y02P20/582 , C08F2/24
摘要： Described herein is a composition comprising an aqueous polymerization reaction product of fluorinated monomers and wherein the polymerization is initiated (i) in the absence of a fluorinated emulsifier and whereby no fluorinated emulsifier is added during polymerization or (ii) in the presence of an fluorinated emulsifier selected from: [Rf—O-L-COO-]i Xi+ (I) wherein L represents a linear or branched, non-fluorinated, partially fluorinated, or fully fluorinated alkylene group, Rf represents a linear or branched partially or fully fluorinated aliphatic group or a linear or branched partially or fully fluorinated aliphatic group interrupted with at least one oxygen atom, Xi+ represents a cation having the valence i and i is 1, 2 or 3; wherein the reaction product and/or the resulting aqueous phase are substantially free of di- and tri-alkylamines and substantially free of low molecular weight fluoroorganic compounds and methods thereof.
摘要翻译：本文描述的是包含氟化单体的水性聚合反应产物的组合物，其中聚合反应开始于（i）在不存在氟化乳化剂的情况下，并且由此在聚合过程中不加入氟化乳化剂，或（ii）在氟化乳化剂存在下选自：[Rf-OL-COO-] i Xi +（I）其中L表示直链或支链，非氟化，部分氟化或完全氟化的亚烷基，Rf表示直链或支链部分或完全氟化的脂族基团或间隔有至少一个氧原子的直链或支链部分或完全氟化的脂肪族基团，X i +表示i为i且i为1,2或3的阳离子; 其中所述反应产物和/或所得水相基本上不含二烷基胺和三烷基胺，并且基本上不含低分子量氟代有机化合物及其方法。

5. 发明授权

US08809580B2 Methods of preparing fluorinated carboxylic acids and their salts 有权
标题翻译：制备氟化羧酸及其盐的方法
公开(公告)号：US08809580B2
公开(公告)日：2014-08-19
申请号：US13497173
申请日：2010-10-21
申请人： Klaus Hintzer , Dennis E. Vogel , Miguel A. Guerra , Jolanta Ignatowska , Gerd-Volker Röschenthaler , Oleg Shyshkov , Kim M. Vogel , Tilman C. Zipplies
发明人： Klaus Hintzer , Dennis E. Vogel , Miguel A. Guerra , Jolanta Ignatowska , Gerd-Volker Röschenthaler , Oleg Shyshkov , Kim M. Vogel , Tilman C. Zipplies
IPC分类号： C07C51/27
CPC分类号： C07C51/27 , C07C53/21 , C07C59/135
摘要： A method for preparing fluorinated carboxylic acids and theirs salts is described comprising subjecting a fluorinated to at least one first and at least one second oxidizing agent to produce a highly fluorinated carboxylic acid or their salts. The first oxidizing agent is a compound that can be converted, by action of the second oxidizing agent, into a reactive species capable of oxidizing the fluorinated alcohol.
摘要翻译：描述了制备氟化羧酸及其盐的方法，其包括使氟化至少一种第一和至少一种第二氧化剂以产生高度氟化的羧酸或其盐。第一氧化剂是可以通过第二氧化剂的作用转化为能够氧化氟化醇的反应性物质的化合物。

6. 发明授权

US08710257B2 Method of preparing highly fluorinated carboxylic acids and their salts 有权
标题翻译：制备高度氟化的羧酸及其盐的方法
公开(公告)号：US08710257B2
公开(公告)日：2014-04-29
申请号：US13511939
申请日：2010-11-18
申请人： Klaus Hintzer , Tilman C. Zipplies , Oleg Shyshkov
发明人： Klaus Hintzer , Tilman C. Zipplies , Oleg Shyshkov
IPC分类号： C07C69/66 , C07C59/135 , C07C235/06
CPC分类号： C07C51/353 , C07C67/347 , C07C231/12 , C07C53/21 , C07C69/708 , C07C235/06
摘要： A method for preparing highly fluorinated carboxylic acids and theirs salts and the precursors thereof.
摘要翻译：一种制备高度氟化的羧酸及其盐及其前体的方法。

7. 发明申请

US20130281607A1 FLUOROPOLYMER COMPOSITIONS AND PURIFICATION METHODS THEREOF 有权
标题翻译：氟聚合物组合物及其纯化方法
公开(公告)号：US20130281607A1
公开(公告)日：2013-10-24
申请号：US13995615
申请日：2011-12-21
申请人： Klaus Hintzer , Michael Juergens , Gunther J. Kaempf , Harald Kaspar , Kai H. Lochhaas , Andre Streiter , Oleg Shyshkov , Tilman C. Zipplies , Herbert Koenigsmann
发明人： Klaus Hintzer , Michael Juergens , Gunther J. Kaempf , Harald Kaspar , Kai H. Lochhaas , Andre Streiter , Oleg Shyshkov , Tilman C. Zipplies , Herbert Koenigsmann
IPC分类号： C25B3/08
CPC分类号： C08F6/003 , C02F1/26 , C02F1/461 , C02F2001/46138 , C02F2001/46147 , C08F2/10 , C08F2/20 , C08F14/08 , C08F14/18 , C08F2800/10 , Y02P20/582 , C08F2/24
摘要： Described herein is a composition comprising an aqueous polymerization reaction product of fluorinated monomers and wherein the polymerization is initiated (i) in the absence of a fluorinated emulsifier and whereby no fluorinated emulsifier is added during polymerization or (ii) in the presence of an fluorinated emulsifier selected from: [Rf—O-L-COO-]i Xi+ (I) wherein L represents a linear or branched, non-fluorinated, partially fluorinated, or fully fluorinated alkylene group, Rf represents a linear or branched partially or fully fluorinated aliphatic group or a linear or branched partially or fully fluorinated aliphatic group interrupted with at least one oxygen atom, Xi+ represents a cation having the valence i and i is 1, 2 or 3; wherein the reaction product and/or the resulting aqueous phase are substantially free of di- and tri-alkylamines and substantially free of low molecular weight fluoroorganic compounds and methods thereof.
摘要翻译：本文描述的是包含氟化单体的水性聚合反应产物的组合物，其中聚合反应开始于（i）在不存在氟化乳化剂的情况下，并且由此在聚合过程中不加入氟化乳化剂，或（ii）在氟化乳化剂存在下选自：[Rf-OL-COO-] i Xi +（I）其中L表示直链或支链，非氟化，部分氟化或完全氟化的亚烷基，Rf表示直链或支链部分或完全氟化的脂族基团或间隔有至少一个氧原子的直链或支链部分或完全氟化的脂肪族基团，X i +表示i为i且i为1,2或3的阳离子; 其中所述反应产物和/或所得水相基本上不含二烷基胺和三烷基胺，并且基本上不含低分子量氟代有机化合物及其方法。

8. 发明授权

US08637608B2 Azide-containing fluoropolymers and their preparation 有权
标题翻译：含叠氮的含氟聚合物及其制备方法
公开(公告)号：US08637608B2
公开(公告)日：2014-01-28
申请号：US13058063
申请日：2009-08-17
申请人： Klaus Hintzer , Michael Juergens , Harald Kaspar , Kai H. Lochhaas , Oleg Shyshkov , Andre Streiter , Tilman C. Zipplies , Sabine H. G. Beuermann , Muhammad Imran ul-haq
发明人： Klaus Hintzer , Michael Juergens , Harald Kaspar , Kai H. Lochhaas , Oleg Shyshkov , Andre Streiter , Tilman C. Zipplies , Sabine H. G. Beuermann , Muhammad Imran ul-haq
IPC分类号： C08L27/12 , C08F214/26 , C08F12/20 , C08F14/18 , C07C241/00 , B32B1/08 , B32B15/08
CPC分类号： C08F8/30 , C08F4/00 , C08F4/02 , C08F114/20 , C08F114/22 , C08G73/00 , Y10T428/139 , Y10T428/1397 , C08F14/18
摘要： Fluoropolymers containing one or more azide group wherein the azide group is not a sulfonyl-azide group and processes of preparing them.
摘要翻译：含有一个或多个叠氮基的含氟聚合物及其制备方法，其中叠氮基不是磺酰基叠氮基。

9. 发明申请

US20120184770A1 METHODS OF PREPARING FLUORINATED CARBOXYLIC ACIDS AND THEIR SALTS 有权
标题翻译：制备氟化羧酸及其盐的方法
公开(公告)号：US20120184770A1
公开(公告)日：2012-07-19
申请号：US13497173
申请日：2010-10-21
申请人： Klaus Hintzer , Dennis E. Vogel , Miguel A. Guerra , Jolanta Ignatowska , Gerd-Volker Röschenthaler , Oleg Shyshkov , Kim M Vogel , Tilman C. Zipplies
发明人： Klaus Hintzer , Dennis E. Vogel , Miguel A. Guerra , Jolanta Ignatowska , Gerd-Volker Röschenthaler , Oleg Shyshkov , Kim M Vogel , Tilman C. Zipplies
IPC分类号： C07C51/16 , C07C51/285 , C07C51/305 , C07C51/23 , C25B3/02 , C07C51/27 , C07C51/29
CPC分类号： C07C51/27 , C07C53/21 , C07C59/135
摘要： A method for preparing fluorinated carboxylic acids and theirs salts is described comprising subjecting a fluorinated alcohol of the general formula (A): A-CH2—OH to at least one first and at least one second oxidizing agent to produce a highly fluorinated carboxylic acid or their salts of the general formula (B): A-COO M+, wherein M+ represents a cation and wherein A in formulas (A) and (B) is the same and A represents the residue: Rf-[0]p-CX″Y″-[0]m-CX′Y′-[0]n-CXY— wherein Rf represents a fluorinated alkyl residue which may or may not contain one or more catenary oxygen atoms, p, m and n are independently from each other either 1 or O, X, X′, X″, Y, Y′ and Y″ are independently from each other H, F, CF3, or C2F5 with the proviso that not all of X, X′, X″, Y, Y′ and Y″ are H; or A represents the residue: R—CFX— wherein X and R are independently selected from a hydrogen, a halogen, or an alkyl, alkenyl, cycloalkyl, or aryl residue, which may or may not contain one or more fluorine atoms and which may or may not contain one or more catenary oxygen atoms; wherein said at least one first oxidizing agent is a compound that can be converted, by action of the second oxidizing agent, into a reactive species capable of oxidizing the fluorinated alcohol.
摘要翻译：描述了制备氟化羧酸及其盐的方法，其包括将通式（A）的氟化醇：A-CH 2 -OH置于至少一种第一和至少一种第二氧化剂中以产生高度氟化的羧酸或其通式（B）的盐：A-COO M +，其中M +表示阳离子，式（A）和（B）中的A相同，A表示残基：Rf- [0] p-CX“ Y“ - [0] m-CX'Y' - [0] n-CXY-其中Rf表示可以或可以不含有一个或多个链状氧原子的氟化烷基残基，p，m和n彼此独立地 1或O，X，X'，X“，Y，Y'和Y”彼此独立地为H，F，CF 3或C 2 F 5，条件是不是全部X，X'，X“，Y， Y'和Y“为H; 或A表示残基：R-CFX-，其中X和R独立地选自氢，卤素或烷基，烯基，环烷基或芳基残基，其可以含有或不含有一个或多个氟原子，或者可以不包含一个或多个链状氧原子; 其中所述至少一种第一氧化剂是可以通过第二氧化剂的作用转化成能够氧化氟化醇的反应性物质的化合物。

10. 发明申请

US20110218305A1 AZIDE-CONTAINING FLUOROPOLYMERS AND THEIR PREPARATION 有权
标题翻译：含AZIO的氟聚合物及其制备
公开(公告)号：US20110218305A1
公开(公告)日：2011-09-08
申请号：US13058063
申请日：2009-08-17
申请人： Klaus Hintzer , Michael Juergens , Harald Kaspar , Kai J. Lochhaas , Oleg Shyshkov , Andre Streiter , Tilman C. Zipplies , Sabine H.G. Beuermann , Muhammad Imran ul-haq
发明人： Klaus Hintzer , Michael Juergens , Harald Kaspar , Kai J. Lochhaas , Oleg Shyshkov , Andre Streiter , Tilman C. Zipplies , Sabine H.G. Beuermann , Muhammad Imran ul-haq
IPC分类号： C08F8/30 , C08G73/00
CPC分类号： C08F8/30 , C08F4/00 , C08F4/02 , C08F114/20 , C08F114/22 , C08G73/00 , Y10T428/139 , Y10T428/1397 , C08F14/18
摘要： Fluoropolymers containing one or more azide group wherein the azide group is not a sulfonyl-azide group and processes of preparing them.
摘要翻译：含有一个或多个叠氮基的含氟聚合物及其制备方法，其中叠氮基不是磺酰基叠氮基。

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