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1. 发明授权

US06858678B2 Continuous bulk polymerization and esterification process and compositions including the polymeric product 有权
标题翻译：连续本体聚合和酯化方法以及包括聚合物产品的组合物
公开(公告)号：US06858678B2
公开(公告)日：2005-02-22
申请号：US10013752
申请日：2001-10-29
申请人： Kevin M. Andrist , John E. Blasko , Glenn C. Calhoun , Frederick C. Hansen , Dean R. Hellwig , Kurt A. Hessenius , Steven M. Hurley , D. Sunil Jayasuriya , Matthew G. Lee , Stephen J. Maccani , H. Thomas Mills, Jr. , Gregory R. Peterson , Paul E. Sandvick , Dennis M. Wilson , John P. Wiruth
发明人： Kevin M. Andrist , John E. Blasko , Glenn C. Calhoun , Frederick C. Hansen , Dean R. Hellwig , Kurt A. Hessenius , Steven M. Hurley , D. Sunil Jayasuriya , Matthew G. Lee , Stephen J. Maccani , H. Thomas Mills, Jr. , Gregory R. Peterson , Paul E. Sandvick , Dennis M. Wilson , John P. Wiruth
IPC分类号： C08L23/00 , B01F17/00 , C08F2/02 , C08F20/04 , C08F22/06 , C08F220/06 , C08F220/18 , C09D133/04 , C09G1/16 , C09J133/04 , D21H17/28 , D21H17/37 , D21H21/16 , C08F8/14
CPC分类号： B01F17/0085 , B01F17/0028 , B01F17/005 , C08F2/02 , C08F20/04 , C08F22/06 , C08F220/06 , C08F220/18 , C09G1/16 , D21H17/28 , D21H17/37 , D21H21/16
摘要： A continuous bulk polymerization and esterification process includes continuously charging into a reaction zone at least one ethylenically unsaturated acid-functional monomer and at least one linear or branched chain alkanol having greater than 11 carbon atoms. The process includes maintaining a flow rate through the reaction zone sufficient to provide an average residence time of less than 60 minutes and maintaining a temperature in the reaction zone sufficient to produce a polymeric product incorporating at least some of the alkanol as an ester of the polymerized ethylenically unsaturated acid-functional monomer. The polymeric product is used in various processes to produce water-based compositions including emulsions and dispersions such as oil emulsions, wax dispersions, pigment dispersions, surfactants and coatings which contain the polymeric product. A polymeric surfactant includes at least one ethylenically unsaturated acid-functional monomer which has been radically incorporated into the polymeric surfactant and at least one ester of the incorporated ethylenically unsaturated acid-functional monomer which has a linear or branched chain alkyl group with greater than 11 carbon atoms. The molar critical micelle concentration of the polymeric surfactant is less than 1.0×10−2 moles/liter. Aqueous 2 percent solutions of certain polymeric surfactants have a surface tension of less than 45 mN/m at 30° C. and exhibit a decrease in surface tension of at least 5 mN/m as the temperature warms from 30° C. to 50° C.
摘要翻译：连续本体聚合和酯化方法包括将至少一种烯属不饱和酸官能单体和至少一种具有大于11个碳原子的直链或支链链烷醇连续地加入到反应区中。该方法包括保持通过反应区的流速足以提供小于60分钟的平均停留时间，并保持反应区中的温度足以产生聚合产物，该聚合物与至少一些烷醇作为聚合的烯键式不饱和酸官能单体。聚合物产品用于各种工艺中以生产水性组合物，包括乳液和分散体，例如油乳剂，蜡分散体，颜料分散体，表面活性剂和含有聚合产物的涂料。聚合物表面活性剂包括至少一种烯键式不饱和酸官能单体，其已经自由地掺入聚合物表面活性剂和至少一种具有直链或支链烷基与大于11个碳的烯键式不饱和酸官能单体的酯原子聚合物表面活性剂的摩尔临界胶束浓度小于1.0×10 -2摩尔/升。某些聚合物表面活性剂的2％水溶液在30℃下的表面张力小于45mN / m，并且随着温度从30℃升温到50℃，表面张力降低至少5mN / m C。

2. 发明授权

US06355727B1 Continuous bulk polymerization and esterification process 有权
标题翻译：连续本体聚合和酯化过程
公开(公告)号：US06355727B1
公开(公告)日：2002-03-12
申请号：US09347035
申请日：1999-07-02
申请人： Kevin M. Andrist , John E. Blasko , Glenn C. Calhoun , Frederick C. Hansen , Dean R. Hellwig , Kurt A. Hessenius , Steven M. Hurley , D. Sunil Jayasuriya , Matthew G. Lee , Stephen J. Maccani , H. Thomas Mills, Jr. , Gregory R. Peterson , Paul E. Sandvick , Dennis M. Wilson , John P. Wiruth
发明人： Kevin M. Andrist , John E. Blasko , Glenn C. Calhoun , Frederick C. Hansen , Dean R. Hellwig , Kurt A. Hessenius , Steven M. Hurley , D. Sunil Jayasuriya , Matthew G. Lee , Stephen J. Maccani , H. Thomas Mills, Jr. , Gregory R. Peterson , Paul E. Sandvick , Dennis M. Wilson , John P. Wiruth
IPC分类号： C08F2004
CPC分类号： B01F17/0085 , B01F17/0028 , B01F17/005 , C08F2/02 , C08F20/04 , C08F22/06 , C08F220/06 , C08F220/18 , C09G1/16 , D21H17/28 , D21H17/37 , D21H21/16
摘要： A continuous bulk polymerization and esterification process includes continuously charging into a reaction zone at least one ethylenically unsaturated acid-functional monomer and at least one linear or branched chain alkanol having greater than 11 carbon atoms. The process includes including maintaining a flow rate through the reaction zone sufficient to provide an average residence time of less than 60 minutes and maintaining a temperature in the reaction zone sufficient to produce a polymeric product incorporating at least some of the alkanol as an ester of the polymerized ethylenically unsaturated acid-functional monomer. The polymeric product is used in various processes to produce water-based compositions including emulsions and dispersions such as oil emulsions, wax dispersions, pigment dispersions, surfactants and coatings which contain the polymeric product. A polymeric surfactant includes at least one ethylenically unsaturated acid-functional monomer which has been radically incorporated into the polymeric surfactant and at least one ester of the incorporated ethylenically unsaturated acid-functional monomer which has a linear or branched chain alkyl group with greater than 11 carbon atoms. The molar critical micelle concentration of the polymeric surfactant is less than 1.0×10−2 moles/liter. Aqueous 2 percent neutralized solutions of certain polymeric surfactants have a surface tension of less than 45 mN/m at 30° C. and exhibit a decrease in surface tension of at least 5 mN/m as the temperature warms from 30° C. to 50° C.
摘要翻译：连续本体聚合和酯化方法包括将至少一种烯属不饱和酸官能单体和至少一种具有大于11个碳原子的直链或支链链烷醇连续地加入到反应区中。该方法包括保持通过反应区的流速足以提供小于60分钟的平均停留时间，并保持反应区中的温度足以产生聚合产物，该聚合物与至少一些烷醇作为聚合的烯键式不饱和酸官能单体。聚合物产品用于各种工艺中以生产水性组合物，包括乳液和分散体，例如油乳剂，蜡分散体，颜料分散体，表面活性剂和含有聚合产物的涂料。聚合物表面活性剂包括至少一种烯键式不饱和酸官能单体，其已经自由地掺入聚合物表面活性剂和至少一种具有直链或支链烷基与大于11个碳的烯键式不饱和酸官能单体的酯原子聚合物表面活性剂的摩尔临界胶束浓度小于1.0×10 -2摩尔/升。某些聚合物表面活性剂的2％中和水溶液的表面张力在30℃时的表面张力小于45mN / m，并且随着温度从30℃升至50℃，表面张力降低至少5mN / m C。

3. 发明授权

US6020061A Emulsion polymerization using polymeric surfactants 失效
标题翻译：使用聚合物表面活性剂的乳液聚合
公开(公告)号：US6020061A
公开(公告)日：2000-02-01
申请号：US842696
申请日：1997-04-15
申请人： Steven M. Hurley , Frederick C. Hansen
发明人： Steven M. Hurley , Frederick C. Hansen
IPC分类号： C08L101/00 , C08F2/24 , C08F2/26 , C08F20/10 , B32B7/12
CPC分类号： C08F2/26 , Y10T428/265
摘要： An emulsion polymerization system comprising a polymeric stabilizer, wherein the polymeric stabilizer comprises one or more alpha olefin/maleic anhydride copolymers and is present in the emulsion polymerization system in an amount greater than 0 and less than 5% by weight.
摘要翻译：包含聚合物稳定剂的乳液聚合体系，其中所述聚合物稳定剂包含一种或多种α-烯烃/马来酸酐共聚物，并且以大于0且小于5重量％的量存在于所述乳液聚合体系中。

4. 发明授权

US5058523A Warning device 失效
标题翻译：警告装置
公开(公告)号：US5058523A
公开(公告)日：1991-10-22
申请号：US504632
申请日：1990-04-04
申请人： John W. Mikkonen , Frederick C. Hansen
发明人： John W. Mikkonen , Frederick C. Hansen
IPC分类号： B60Q9/00
CPC分类号： B60Q9/001
摘要： A device for preventing inadvertent headlight illumination includes a first panel for securing the device to an interior surface of a vehicle. A second panel is attached to the first panel and is movable with respect thereto for exposing a warning legend. The warning legend is disposed on one or both of the panels and is exposed to the view of the operator when the second panel is moved. The warning device also includes a motor vehicle door from within the vehicle. A cavity is formed in the door and a panel is received in the cavity. The panel is movable from a repose position to a warning position in which it also interferes with access to the interior door handle.
摘要翻译：用于防止无意的前照灯照明的装置包括用于将装置固定到车辆的内表面的第一面板。第二面板附接到第一面板并且可相对于其移动以暴露警告图例。警告图例设置在一个或两个面板上，并且当第二面板移动时暴露于操作者的视野。警告装置还包括车内的机动车门。在门中形成空腔，并且将面板容纳在空腔中。面板可以从休止位置移动到警告位置，在此警告位置也会妨碍进入内部门把手。

5. 发明授权

US4936244A Warning device 失效
标题翻译：警告装置
公开(公告)号：US4936244A
公开(公告)日：1990-06-26
申请号：US374764
申请日：1989-07-03
申请人： Frederick C. Hansen , John W. Mikkonen
发明人： Frederick C. Hansen , John W. Mikkonen
IPC分类号： B60Q9/00
CPC分类号： B60Q9/001
摘要： A device for preventing inadvertent headlight illumination includes a first panel for securing the device to an interior surface of a vehicle. A second panel is attached to the first panel and is moveable with respect thereto for exposing a warning legend. The warning legend is disposed on one or both of the panels and is exposed to the view of the operator when the second panel is moved. Several embodiments are disclosed.
摘要翻译：用于防止无意的前照灯照明的装置包括用于将装置固定到车辆的内表面的第一面板。第二面板附接到第一面板并且可相对于其移动以暴露警告图例。警告图例设置在一个或两个面板上，并且当第二面板移动时暴露于操作者的视野。公开了几个实施例。

6. 发明授权

US4598118A Coatings containing an alphaolefin terpolymer 失效
标题翻译：含有α-烯烃三元共聚物的涂料
公开(公告)号：US4598118A
公开(公告)日：1986-07-01
申请号：US508698
申请日：1983-06-28
申请人： Frederick C. Hansen , Richard A. Kiehlbauch
发明人： Frederick C. Hansen , Richard A. Kiehlbauch
IPC分类号： C08F210/14 , C08F222/04 , C08L37/00
CPC分类号： C08F210/14 , C08F222/04
摘要： A coating composition which produces glossy, clear coatings comprises a terpolymer of an anhydride, a higher alphaolefin and either a lower alphaolefin or a mono-alkenyl aromatic compound; an acrylic emulsion polymer and the balance of the composition being an aqueous vehicle.
摘要翻译：产生光泽，透明涂层的涂料组合物包括酸酐，高级α-烯烃和低级α-烯烃或单烯基芳族化合物的三元共聚物; 丙烯酸乳液聚合物，其余组成为水性载体。

7. 发明授权

US4623692A Process for preparing an aqueous cut of a ligand-free monomer/maleic anhydride polymer and product 失效
标题翻译：制备不含配体的单体/马来酸酐聚合物和产物的水性切口的方法
公开(公告)号：US4623692A
公开(公告)日：1986-11-18
申请号：US711895
申请日：1985-03-14
申请人： Frederick C. Hansen
发明人： Frederick C. Hansen
IPC分类号： C08F8/44 , C09D123/02 , C09D135/06 , C09D201/02 , C08L37/00
CPC分类号： C09D135/06 , C09D123/025
摘要： A process for solubilizing a ligand-free monomer/maleic anhydride polymer into an aqueous medium employing a metal fugitive ligand complex to disperse the polymer.
摘要翻译：使用金属逸散配体络合物将无配体的单体/马来酸酐聚合物溶解到含水介质中以分散聚合物的方法。

8. 发明授权

US3971315A Macroporous microporous marking structure 失效
标题翻译：大孔微孔标记结构
公开(公告)号：US3971315A
公开(公告)日：1976-07-27
申请号：US496677
申请日：1974-08-12
申请人： Frederick C. Hansen
发明人： Frederick C. Hansen
IPC分类号： B41C1/00 , B41F31/26 , B41K1/50 , B41N1/00 , B41N1/12 , C08J9/00 , B41K1/42
CPC分类号： B41N1/12 , Y10T428/24996 , Y10T428/249975 , Y10T428/249978 , Y10T428/249979 , Y10T428/249981 , Y10T428/249996
摘要： A marking structure for various uses, such as in hand stamps or other printing members, or in ink pads, ink rolls or other inking members. The marking structure is characterized by at least two layers, including an outer layer and an underlying reservoir layer. The outer layer has interconnected aggregates of thermoplastic resin, forming a microporous network of pores, and a marking fluid contained within the network. The reservoir layer has an open-pored macroporous structure, such as an open-cell polyurethane foam, impregnated with a microporous thermoplastic resin, in the form of interconnected aggregates, and an additional amount of the marking fluid. The resin aggregates of the outer and reservoir layers are joined at the interface of the layers to form a cohesive structure.
摘要翻译：用于各种用途的标记结构，例如手印或其他印刷部件，或在油墨垫，油墨辊或其它上墨构件中。标记结构的特征在于至少两层，包括外层和下层储层。外层具有热塑性树脂的互连聚集体，形成孔的微孔网络和包含在网络内的标记液。储层具有开孔大孔结构，例如开孔聚氨酯泡沫，浸渍有微孔热塑性树脂，呈互连聚集体的形式，以及额外量的标记液。外层和储层的树脂聚集体在层的界面处连接以形成粘结结构。

9. 发明授权

US4730019A Process for preparing an aqueous cut of a ligand-free monomer/maleic anhydride polymer and product 失效
标题翻译：制备不含配体的单体/马来酸酐聚合物和产物的水性切口的方法
公开(公告)号：US4730019A
公开(公告)日：1988-03-08
申请号：US862084
申请日：1986-05-12
申请人： Frederick C. Hansen
发明人： Frederick C. Hansen
IPC分类号： C09D123/02 , C09D135/06 , C08L37/00
CPC分类号： C09D123/025 , C09D135/06
摘要： A coating composition having improved heat resistance is disclosed. The coating composition comprises a ligand-free monomer/maleic anhydride polymer, and an effective amount of a metal ion-containing fugitive ligand complex to solubilize the polymer in an aqueous medium.
摘要翻译：公开了具有改进的耐热性的涂料组合物。涂料组合物包含不含配体的单体/马来酸酐聚合物和有效量的含金属离子的挥发性配体络合物，以将聚合物溶解在水性介质中。

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