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1. 发明申请

US20110201846A1 METHOD FOR PRODUCING ALKYLATED AROMATICE COMPOUND, METHOD FOR PRODUCING CUMENE, AND METHOD FOR PRODUCING PHENOL 有权
标题翻译：用于生产烷基化芳构化合物的方法，生产碳酸钙的方法和生产酚醛的方法
公开(公告)号：US20110201846A1
公开(公告)日：2011-08-18
申请号：US13125163
申请日：2009-10-22
申请人： Kenji Fujiwara , Tsuneyuki Ohkubo , Terunori Fujita , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Kozo Yasuda
发明人： Kenji Fujiwara , Tsuneyuki Ohkubo , Terunori Fujita , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Kozo Yasuda
IPC分类号： C07C37/08 , C07C1/20
CPC分类号： C07C37/08 , B01J23/80 , B01J29/7007 , B01J29/7038 , C07C2/867 , C07C15/085 , C07C407/00 , C07C409/10 , Y02P20/52 , Y02P20/588 , C07C39/04
摘要： It is an object of the present invention to provide a method for producing an alkylated aromatic compound and a method for producing cumene that can greatly reduce the amount of solid acid substance, and a method for producing phenol including a step of producing cumene by the method for producing cumene. A method for producing an alkylated aromatic compound according to the present invention includes a step (i) of producing a reaction product (a1) containing the alkylated aromatic compound and water by the reaction of an aromatic compound, a ketone, and hydrogen using a metal component containing at least one metallic element selected from the group consisting of copper, nickel, cobalt, and rhenium and a solid acid substance; a step (ii) of forming a dehydrated product (a2) from at least a portion of the reaction product (a1) by removing at least a portion of the water in the reaction product (a1); and a step (iii) of producing a reaction product (a3) containing the alkylated aromatic compound by bringing at least a portion of the dehydrated product (a2) into contact with a solid acid substance.
摘要翻译：本发明的目的是提供一种烷基化芳族化合物的制造方法和能够大幅度减少固体酸性物质的量的异丙基苯的制造方法，以及生产苯酚的方法，其包括通过该方法制造枯烯的工序用于生产异丙基苯。根据本发明的烷基化芳族化合物的制造方法包括使用金属制造含有烷基化芳香族化合物和水的反应产物（a1）的步骤（i），所述反应产物通过芳族化合物，酮和氢的反应而生成含有选自铜，镍，钴和铼中的至少一种金属元素的组分和固体酸物质; 通过除去反应产物（a1）中的至少一部分水，从至少一部分反应产物（a1）形成脱水产物（a2）的步骤（ii）; 和通过使脱水产物（a2）的至少一部分与固体酸物质接触来制造含有烷基化芳香族化合物的反应产物（a3）的步骤（iii）。

2. 发明授权

US08546633B2 Method for producing alkylated aromatic compound, method for producing cumene, and method for producing phenol 有权
标题翻译：烷基化芳香族化合物的制造方法，异丙基苯的制造方法以及苯酚的制造方法
公开(公告)号：US08546633B2
公开(公告)日：2013-10-01
申请号：US13125163
申请日：2009-10-22
申请人： Kenji Fujiwara , Tsuneyuki Ohkubo , Terunori Fujita , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Kozo Yasuda
发明人： Kenji Fujiwara , Tsuneyuki Ohkubo , Terunori Fujita , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Kozo Yasuda
IPC分类号： C07C2/86 , C07C37/08
CPC分类号： C07C37/08 , B01J23/80 , B01J29/7007 , B01J29/7038 , C07C2/867 , C07C15/085 , C07C407/00 , C07C409/10 , Y02P20/52 , Y02P20/588 , C07C39/04
摘要： A method for producing an alkylated aromatic compound includes a step (i) of producing a reaction product (a1) containing the alkylated aromatic compound and water by the reaction of an aromatic compound, a ketone, and hydrogen using a metal component containing at least one metallic element of copper, nickel, cobalt, and rhenium and a solid acid substance; a step (ii) of forming a dehydrated product (a2) from at least a portion of the reaction product (a1) by removing at least a portion of the water in the reaction product (a1); and a step (iii) of producing a reaction product (a3) containing the alkylated aromatic compound by bringing at least a portion of the dehydrated product (a2) into contact with a solid acid substance.
摘要翻译：烷基化芳香族化合物的制造方法包括使用含有至少一种以上的金属成分，通过芳香族化合物，酮和氢的反应来制造含有烷基化芳香族化合物和水的反应产物（a1）的工序（i）铜，镍，钴和铼的金属元素和固体酸物质; 通过除去反应产物（a1）中的至少一部分水，从至少一部分反应产物（a1）形成脱水产物（a2）的步骤（ii）; 和通过使脱水产物（a2）的至少一部分与固体酸物质接触来制造含有烷基化芳香族化合物的反应产物（a3）的步骤（iii）。

3. 发明授权

US08536394B2 Process for producing alkylated aromatic compounds and process for producing phenols 有权
标题翻译：烷基化芳香族化合物的制造方法和酚类的制造方法
公开(公告)号：US08536394B2
公开(公告)日：2013-09-17
申请号：US13256626
申请日：2010-03-12
申请人： Tsuneyuki Ohkubo , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Terunori Fujita , Kenji Fujiwara
发明人： Tsuneyuki Ohkubo , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Terunori Fujita , Kenji Fujiwara
IPC分类号： C07C2/86 , C07C37/08
CPC分类号： C07C2/867 , B01J21/08 , B01J23/50 , B01J29/7007 , B01J35/0006 , B01J37/0201 , B01J37/0205 , B01J37/04 , C07C37/08 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2521/12 , C07C2521/18 , C07C2523/42 , C07C2523/44 , C07C2523/50 , C07C2523/68 , C07C2527/08 , C07C2527/10 , C07C2527/232 , C07C2527/25 , C07C2527/26 , C07C2529/08 , C07C2529/18 , C07C2529/70 , C07C2531/04 , Y02P20/52 , C07C15/085 , C07C39/04
摘要： According to a process of the invention, a ketone, an aromatic compound and hydrogen as starting materials are reacted together in a single reaction step to produce an alkylaromatic compound in high yield. A process for producing phenols in the invention includes a step of performing the above alkylation process and does not increase the number of steps compared to the conventional cumene process. The process for producing alkylated aromatic compounds includes reacting an aromatic compound such as benzene, a ketone such as acetone and hydrogen in the presence of a solid acid substance, preferably a zeolite, and a silver-containing catalyst.
摘要翻译：根据本发明的方法，将酮，芳族化合物和作为原料的氢在单一反应步骤中一起反应，以高产率生成烷基芳族化合物。在本发明中生产酚类的方法包括进行上述烷基化方法并且不增加与常规异丙苯法相比的步骤数量的步骤。制备烷基化芳族化合物的方法包括在固体酸物质，优选沸石和含银催化剂存在下使芳香化合物如苯，丙酮和氢等酮反应。

4. 发明申请

US20120004471A1 PROCESS FOR PRODUCING ALKYLATED AROMATIC COMPOUNDS AND PROCESS FOR PRODUCING PHENOLS 有权
标题翻译：生产碱性芳族化合物的方法和生产酚醛的方法
公开(公告)号：US20120004471A1
公开(公告)日：2012-01-05
申请号：US13256626
申请日：2010-03-12
申请人： Tsuneyuki Ohkubo , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Terunori Fujita , Kenji Fujiwara
发明人： Tsuneyuki Ohkubo , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Terunori Fujita , Kenji Fujiwara
IPC分类号： C07C37/08 , C07C1/207
CPC分类号： C07C2/867 , B01J21/08 , B01J23/50 , B01J29/7007 , B01J35/0006 , B01J37/0201 , B01J37/0205 , B01J37/04 , C07C37/08 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2521/12 , C07C2521/18 , C07C2523/42 , C07C2523/44 , C07C2523/50 , C07C2523/68 , C07C2527/08 , C07C2527/10 , C07C2527/232 , C07C2527/25 , C07C2527/26 , C07C2529/08 , C07C2529/18 , C07C2529/70 , C07C2531/04 , Y02P20/52 , C07C15/085 , C07C39/04
摘要： According to a process of the invention, a ketone, an aromatic compound and hydrogen as starting materials are reacted together in a single reaction step to produce an alkylaromatic compound in high yield. A process for producing phenols in the invention includes a step of performing the above alkylation process and does not increase the number of steps compared to the conventional cumene process.The process for producing alkylated aromatic compounds includes reacting an aromatic compound such as benzene, a ketone such as acetone and hydrogen in the presence of a solid acid substance, preferably a zeolite, and a silver-containing catalyst.
摘要翻译：根据本发明的方法，将酮，芳族化合物和作为原料的氢在单一反应步骤中一起反应，以高产率生成烷基芳族化合物。在本发明中生产酚类的方法包括进行上述烷基化方法并且不增加与常规异丙苯法相比的步骤数量的步骤。制备烷基化芳族化合物的方法包括在固体酸物质，优选沸石和含银催化剂存在下使芳香化合物如苯，丙酮和氢等酮反应。

5. 发明授权

US08552239B2 Olefin production process 有权
标题翻译：烯烃生产过程
公开(公告)号：US08552239B2
公开(公告)日：2013-10-08
申请号：US13255239
申请日：2010-03-12
申请人： Tsuneyuki Ohkubo , Kenji Fujiwara , Terunori Fujita , Masayasu Ishibashi
发明人： Tsuneyuki Ohkubo , Kenji Fujiwara , Terunori Fujita , Masayasu Ishibashi
IPC分类号： C07C1/20
CPC分类号： B01J35/0006 , B01J23/002 , B01J23/30 , B01J23/50 , B01J23/66 , B01J23/687 , B01J27/188 , B01J29/068 , B01J29/7415 , B01J29/7815 , B01J37/04 , B01J2229/20 , B01J2523/00 , C07C1/24 , C07C2521/04 , C07C2521/08 , C07C2523/28 , C07C2523/30 , C07C2527/182 , C07C2527/188 , C12P7/04 , C12P7/28 , Y02P20/52 , C07C11/06 , B01J2523/18 , B01J2523/33 , B01J2523/41
摘要： A novel olefin production process is provided which can be established as an industrial and practical process capable of producing olefins by directly reacting a ketone and hydrogen in a single reaction step. In particular, a novel olefin production process is provided in which propylene is obtained with high selectivity by directly reacting acetone and hydrogen.The olefin production process according to the present invention includes reacting a ketone and hydrogen in the presence of at least one dehydration catalyst and a silver-containing catalyst, and the at least one dehydration catalyst is selected from metal oxide catalysts containing a Group 6 element, zeolites, aluminas and heteropoly acid salts in which part or all the protons in heteropoly acids are exchanged with metal cations.
摘要翻译：提供了一种新的烯烃生产方法，其可以建立为能够通过在单一反应步骤中使酮和氢直接反应制备烯烃的工业和实际方法。特别地，提供了一种新的烯烃生产方法，其中通过使丙酮和氢气直接反应，通过高选择性获得丙烯。根据本发明的烯烃制备方法包括在至少一种脱水催化剂和含银催化剂的存在下使酮和氢反应，并且所述至少一种脱水催化剂选自含有第6族元素的金属氧化物催化剂，沸石，氧化铝和杂多酸盐，其中杂多酸中的部分或全部质子与金属阳离子交换。

6. 发明申请

US20120010453A1 OLEFIN PRODUCTION PROCESS 有权
标题翻译： OLEFIN生产过程
公开(公告)号：US20120010453A1
公开(公告)日：2012-01-12
申请号：US13255239
申请日：2010-03-12
申请人： Tsuneyuki Ohkubo , Kenji Fujiwara , Terunori Fujita , Masayasu Ishibashi
发明人： Tsuneyuki Ohkubo , Kenji Fujiwara , Terunori Fujita , Masayasu Ishibashi
IPC分类号： C07C1/00
CPC分类号： B01J35/0006 , B01J23/002 , B01J23/30 , B01J23/50 , B01J23/66 , B01J23/687 , B01J27/188 , B01J29/068 , B01J29/7415 , B01J29/7815 , B01J37/04 , B01J2229/20 , B01J2523/00 , C07C1/24 , C07C2521/04 , C07C2521/08 , C07C2523/28 , C07C2523/30 , C07C2527/182 , C07C2527/188 , C12P7/04 , C12P7/28 , Y02P20/52 , C07C11/06 , B01J2523/18 , B01J2523/33 , B01J2523/41
摘要： A novel olefin production process is provided which can be established as an industrial and practical process capable of producing olefins by directly reacting a ketone and hydrogen in a single reaction step. In particular, a novel olefin production process is provided in which propylene is obtained with high selectivity by directly reacting acetone and hydrogen.The olefin production process according to the present invention includes reacting a ketone and hydrogen in the presence of at least one dehydration catalyst and a silver-containing catalyst, and the at least one dehydration catalyst is selected from metal oxide catalysts containing a Group 6 element, zeolites, aluminas and heteropoly acid salts in which part or all the protons in heteropoly acids are exchanged with metal cations.
摘要翻译：提供了一种新的烯烃生产方法，其可以建立为能够通过在单一反应步骤中使酮和氢直接反应制备烯烃的工业和实际方法。特别地，提供了一种新的烯烃生产方法，其中通过使丙酮和氢气直接反应，通过高选择性获得丙烯。根据本发明的烯烃制备方法包括在至少一种脱水催化剂和含银催化剂的存在下使酮和氢反应，并且所述至少一种脱水催化剂选自含有第6族元素的金属氧化物催化剂，沸石，氧化铝和杂多酸盐，其中杂多酸中的部分或全部质子与金属阳离子交换。

7. 发明授权

US08680355B2 Olefin production process 有权
标题翻译：烯烃生产过程
公开(公告)号：US08680355B2
公开(公告)日：2014-03-25
申请号：US13131905
申请日：2009-10-22
申请人： Tsuneyuki Ohkubo , Kenji Fujiwara , Terunori Fujita
发明人： Tsuneyuki Ohkubo , Kenji Fujiwara , Terunori Fujita
IPC分类号： C07C1/20
CPC分类号： C07C1/24 , B01J23/72 , B01J23/78 , B01J23/868 , B01J23/885 , B01J29/7615 , C07C2529/76 , Y02P20/52 , C07C11/06
摘要： A novel olefin production process of the invention can be established as an industrial and practical process of producing an olefin with high selectivity by directly reacting a ketone and hydrogen in a single reaction step. In particular, a novel olefin production process is provided in which propylene is obtained with high selectivity by directly reacting acetone and hydrogen. An olefin production process of the invention includes reacting a ketone and hydrogen at a reaction temperature in the range of 50 to 300° C. in the presence of a Cu-containing hydrogenation catalyst and a solid acid substance.
摘要翻译：本发明的新型烯烃生产方法可以建立为在单一反应步骤中通过使酮和氢直接反应制备具有高选择性的烯烃的工业和实际工艺。特别地，提供了一种新的烯烃生产方法，其中通过使丙酮和氢气直接反应，通过高选择性获得丙烯。本发明的烯烃制备方法包括在含Cu氢化催化剂和固体酸物质的存在下，在50至300℃的反应温度下使酮和氢反应。

8. 发明申请

US20110230696A1 OLEFIN PRODUCTION PROCESS 有权
标题翻译： OLEFIN生产过程
公开(公告)号：US20110230696A1
公开(公告)日：2011-09-22
申请号：US13131905
申请日：2009-10-22
申请人： Tsuneyuki Ohkubo , Kenji Fujiwara , Terunori Fujita
发明人： Tsuneyuki Ohkubo , Kenji Fujiwara , Terunori Fujita
IPC分类号： C07C1/20
CPC分类号： C07C1/24 , B01J23/72 , B01J23/78 , B01J23/868 , B01J23/885 , B01J29/7615 , C07C2529/76 , Y02P20/52 , C07C11/06
摘要： A novel olefin production process of the invention can be established as an industrial and practical process of producing an olefin with high selectivity by directly reacting a ketone and hydrogen in a single reaction step. In particular, a novel olefin production process is provided in which propylene is obtained with high selectivity by directly reacting acetone and hydrogen. An olefin production process of the invention includes reacting a ketone and hydrogen at a reaction temperature in the range of 50 to 300° C. in the presence of a Cu-containing hydrogenation catalyst and a solid acid substance.
摘要翻译：本发明的新型烯烃生产方法可以建立为在单一反应步骤中通过使酮和氢直接反应制备具有高选择性的烯烃的工业和实际工艺。特别地，提供了一种新的烯烃生产方法，其中通过使丙酮和氢气直接反应，通过高选择性获得丙烯。本发明的烯烃制备方法包括在含Cu氢化催化剂和固体酸物质的存在下，在50至300℃的反应温度下使酮和氢反应。

9. 发明申请

US20140016745A1 METHOD OF STEEL GRADE DETERMINATION FOR STEEL MATERIAL 有权
标题翻译：钢材质量等级测定方法
公开(公告)号：US20140016745A1
公开(公告)日：2014-01-16
申请号：US13981965
申请日：2012-01-19
申请人： Kenji Fujiwara , Hiroshi Kubota
发明人： Kenji Fujiwara , Hiroshi Kubota
IPC分类号： G01N23/223
CPC分类号： G01N23/223 , G01N2223/076
摘要： The method of steel grade determination for a steel material having a substantially circular cross-section comprise: a detection step in which while a measurement section 2 including an irradiation section 21 for performing X-ray irradiation and a detection section 22 for detecting fluorescent X-rays is relatively moved along an outer peripheral surface of the steel material 4 with respect to the steel material for a predetermined time period necessary for analysis, the steel material is irradiated with X-rays from the irradiation section, and fluorescent X-rays radiated from the steel material are detected by the detection section; a calculation step of calculating a composition of the steel material based on fluorescent X-rays detected in the detection step; and a determination step of determining a steel grade of the steel material according to the composition calculated in the calculation step.
摘要翻译：具有大致圆形横截面的钢材的钢种等级测定方法包括：检测步骤，其中在包括用于进行X射线照射的照射部21的测量部2和用于检测荧光X射线的检测部22中，沿着钢材4的外周面相对于钢材相对移动预定时间段进行分析，钢材用照射部分的X射线照射，荧光X射线从钢材由检测部检测; 计算步骤，基于在检测步骤中检测到的荧光X射线计算钢材的成分; 以及根据在计算步骤中计算的组成来确定钢材的钢种的确定步骤。

10. 发明授权

US08436055B2 Modified acidic ion-exchange resin and method for preparing bisphenol 有权
标题翻译：改性酸性离子交换树脂及其制备方法
公开(公告)号：US08436055B2
公开(公告)日：2013-05-07
申请号：US12875016
申请日：2010-09-02
申请人： Takashi Terajima , Toshihiro Takai , Kenji Fujiwara
发明人： Takashi Terajima , Toshihiro Takai , Kenji Fujiwara
IPC分类号： C08J5/20
CPC分类号： B01J31/0239 , B01J31/0268 , B01J31/08 , B01J31/10 , B01J2231/342 , C07C37/20 , Y02P20/52 , C07C39/16
摘要： The present invention provides an ion-exchange resin catalyst, as a catalyst for preparing bisphenol from phenol compounds and ketone, which has a higher selectivity to bisphenol and a longer life time, as compared to a conventional ion-exchange resin, and a method for preparing the same.The present invention also provides a method for preparing bisphenol comprising reacting phenol compounds with ketone, wherein the modified acidic ion-exchange resin in which at least one kind of cationic compound selected from the following (a), (b), (c) and (d) ionically binds to an acidic functional group, is used as a catalyst: (a) a quaternary phosphonium ion, (b) a quaternary ammonium ion, (c) a bis(phosphoranylidene) ammonium ion, and (d) an N-substituted nitrogen-containing aromatic cation.
摘要翻译：本发明提供一种离子交换树脂催化剂，作为与常规离子交换树脂相比，具有较高的双酚选择性和较长使用寿命的酚类化合物和酮制备双酚的催化剂，准备一样本发明还提供一种制备双酚的方法，其包括使酚化合物与酮反应，其中所述改性酸性离子交换树脂其中至少一种选自以下（a），（b），（c）和（d）与酸性官能团离子键合，用作催化剂：（a）季鏻离子，（b）季铵离子，（c）双（亚正膦基）铵离子，和（d）N 取代的含氮芳族阳离子。

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