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1. 发明授权

US06197918B1 Method for manufacturing aromatic carbonates 有权
标题翻译：芳香族碳酸酯的制造方法
公开(公告)号：US06197918B1
公开(公告)日：2001-03-06
申请号：US09458277
申请日：1999-12-09
申请人： Kazutoyo Uno , Masahide Tanaka , Tomoaki Shimoda
发明人： Kazutoyo Uno , Masahide Tanaka , Tomoaki Shimoda
IPC分类号： C08G6400
CPC分类号： C08G64/307 , C07C68/06 , C07C69/96
摘要： The present invention provides a method, which makes it possible to manufacture aromatic carbonates from dialkyl carbonates and aromatic hydroxy compounds inexpensively and with good efficiency. The method uses a titanium catalyst in a particular amount relative to aromatic polyhydric hydroxy compound impurities in a crude aromatic hydroxy compound solution.
摘要翻译：本发明提供一种能够以低成本，高效率从碳酸二烷基酯和芳香族羟基化合物制造芳香族碳酸酯的方法。该方法在粗芳族羟基化合物溶液中使用相对于芳族多羟基化合物杂质的特定量的钛催化剂。

2. 发明授权

US06635710B2 Manufacturing method for polycarbonate 失效
标题翻译：聚碳酸酯的制造方法
公开(公告)号：US06635710B2
公开(公告)日：2003-10-21
申请号：US09208356
申请日：1998-12-10
申请人： Kiyoshi Kono , Kazutoyo Uno , Satoru Minami , Tomoaki Shimoda
发明人： Kiyoshi Kono , Kazutoyo Uno , Satoru Minami , Tomoaki Shimoda
IPC分类号： C08L5300
CPC分类号： C08G64/307
摘要： A method for manufacturing polycarbonate by melt-polycondensing bisphenol and carbonic acid diester uses as catalyst an alkali metal compound and/or alkaline earth metal compound (a). The catalyst is added to the bisphenol prior to the melt polycondensation, in an effective amount, i.e., the amount of alkali metal compound and/or alkaline earth metal compound (a) that acts effectively as a catalyst, is contained in said bisphenol, and is controlled to have the same catalytic activity as 1×10−8 to 1×10−6 mole of bisphenol disodium salt per mole of pure bisphenol A. The method conducts the reaction efficiently from the initial stage in a stable manner to obtain polycarbonate with good color, good heat stability and color stability during molding and the like.
摘要翻译：通过双酚和碳酸二酯的熔融缩聚制备聚碳酸酯的方法使用碱金属化合物和/或碱土金属化合物（a）作为催化剂。在熔融缩聚之前，将催化剂加入到双酚中，有效量，即所述双酚中含有用作催化剂的碱金属化合物和/或碱土金属化合物（a）的量，以及被控制为具有与每摩尔纯双酚A 1x10 -8摩尔至1×10 -6摩尔的双酚二钠盐相同的催化活性。该方法以稳定的方式从初始阶段有效地进行反应以获得具有良好的颜色，良好的热稳定性和成型时的颜色稳定性等。

3. 发明授权

US5760156A Manufacturing method for polycarbonate 失效
标题翻译：聚碳酸酯的制造方法
公开(公告)号：US5760156A
公开(公告)日：1998-06-02
申请号：US764816
申请日：1996-12-12
申请人： Satoshi Inoki , Yoshio Motoyama , Hideto Matsuoka , Hajime Oyoshi , Michio Tanaka , Tomoaki Shimoda , Akio Kanezawa , Kazutoyo Uno
发明人： Satoshi Inoki , Yoshio Motoyama , Hideto Matsuoka , Hajime Oyoshi , Michio Tanaka , Tomoaki Shimoda , Akio Kanezawa , Kazutoyo Uno
IPC分类号： C08G64/20 , C08G64/30 , C08G18/70
CPC分类号： C08G64/307
摘要： A manufacturing method for polycarbonate comprising �I! a process for manufacturing diaryl carbonate from an aromatic hydroxy compound and an aromatic hydroxy compound, �II! a process for manufacturing polycarbonate by solution polymerization of the diaryl carbonate obtained in �II! and an aromatic dihydroxy compound in the presence of a catalyst comprising a nitrogen-containing basic compound, and �III! a process for separating and removing the nitrogen-containing compound from the aromatic hydroxy by-products in �II! and returning the resultant aromatic hydroxy compounds to process �I! effectively reuses aromatic hydroxy by-products (e.g., phenols) of polycarbonate manufacturing to manufacture diaryl carbonate, while suppressing the production of alkyl aromatic ethers and then uses this diaryl carbonate to manufacture polycarbonate with good productivity.
摘要翻译：一种聚碳酸酯的制造方法，其包含：[I]由芳香族羟基化合物和芳香族羟基化合物制造碳酸二芳基酯的方法，[II]通过在[II]中得到的碳酸二芳基酯的溶液聚合制造聚碳酸酯的方法和芳香族二羟基在含有含氮碱性化合物的催化剂存在下的化合物，和[III]从[II]中的芳族羟基副产物中分离除去含氮化合物并将所得芳族羟基化合物返回到方法 [I]有效地重复使用制造碳酸二甲酯的聚碳酸酯的芳族羟基副产物（例如酚），同时抑制烷基芳族醚的生产，然后使用该碳酸二芳基酯以高生产率制造聚碳酸酯。

4. 发明授权

US5057585A Oxygen-permeable article of fluorinated hydrocarbon group-grafted (meth)acrylate polymers 失效
标题翻译：氟化烃基（甲基）丙烯酸酯聚合物的含氧渗透性物品
公开(公告)号：US5057585A
公开(公告)日：1991-10-15
申请号：US554388
申请日：1990-07-19
申请人： Tokinori Agou , Takeshi Sakashita , Tomoaki Shimoda , Masaru Sudo , Masahiro Kuwabara , Masahide Tanaka
发明人： Tokinori Agou , Takeshi Sakashita , Tomoaki Shimoda , Masaru Sudo , Masahiro Kuwabara , Masahide Tanaka
IPC分类号： C08F20/28 , G02B1/04
CPC分类号： C08F20/28 , G02B1/043 , Y10S525/937
摘要： Hydrophilic gelled crosslinked polymers comprising as an essential constituent monomer component a (meth)acrylate ester monomer having a fluorine-substituted hydrocarbon group containing at least three fluorine atoms grafted thereto. The fluorine-containing polymers have excellent oxygen permeability, water swellability, wearing comfort and contamination resistance.

5. 发明授权

US4957985A Fluorine-substituted hydrocarbon group grafted (meth)acrylate polymers 失效
标题翻译：氟取代烃基接枝（甲基）丙烯酸酯聚合物
公开(公告)号：US4957985A
公开(公告)日：1990-09-18
申请号：US138653
申请日：1987-12-29
申请人： Tokinori Agou , Takeshi Sakashita , Tomoaki Shimoda , Masaru Sudo , Masahiro Kuwabara , Masahide Tanaka
发明人： Tokinori Agou , Takeshi Sakashita , Tomoaki Shimoda , Masaru Sudo , Masahiro Kuwabara , Masahide Tanaka
IPC分类号： C08F20/28 , G02B1/04
CPC分类号： C08F20/28 , G02B1/043 , Y10S525/937
摘要： Hydrophilic gelled crosslinked polymers comprising as an essential constituent monomer component a (meth)acrylate ester monomer having a fluorine-substituted hydrocarbon group containing at least three fluorine atoms grafted thereto. The fluorine-containing polymers have excellent oxygen permeability, water swellability, wearing comfort and contamination resistance.

6. 发明授权

US06458914B2 Method for manufacturing dialkyl carbonate 有权
标题翻译：碳酸二烷基酯的制造方法
公开(公告)号：US06458914B2
公开(公告)日：2002-10-01
申请号：US09882339
申请日：2001-06-14
申请人： Takato Kimura , Tomoaki Shimoda , Masahide Tanaka
发明人： Takato Kimura , Tomoaki Shimoda , Masahide Tanaka
IPC分类号： C08G6400
CPC分类号： C07C68/005 , C07C69/96
摘要： The specification describes a method for manufacturing dialkyl carbonate by reacting carbon monoxide, oxygen and alcohol in the presence of a catalyst. The catalyst is produced by reacting together ingredients including a cupric halide and an alkoxide compound of a group III through VII metal.
摘要翻译：本说明书描述了在催化剂存在下使一氧化碳，氧和醇反应制造碳酸二烷基酯的方法。催化剂是通过将包括卤化铜和III-VII族金属的醇盐化合物在内的成分进行反应来制备的。

7. 发明授权

US06258923B1 Method for manufacturing dialkyl carbonate 有权
标题翻译：碳酸二烷基酯的制造方法
公开(公告)号：US06258923B1
公开(公告)日：2001-07-10
申请号：US09584672
申请日：2000-05-31
申请人： Masahide Tanaka , Takato Kimura , Tomoaki Shimoda
发明人： Masahide Tanaka , Takato Kimura , Tomoaki Shimoda
IPC分类号： C08O6400
CPC分类号： C07C68/005 , C07C69/96
摘要： An efficient method for manufacturing a dialkyl carbonate from CO, O2, and an alcohol which uses a catalyst comprising: (i) a cupric halide; and (ii) a compound capable of producing a copper halide alkoxide by reaction with a cupric halide.
摘要翻译：一种从CO，O 2和使用催化剂的醇制造碳酸二烷基酯的有效方法，包括：（ⅰ）卤化铜; 和（ii）能够通过与卤化铜反应制备卤化铜醇盐的化合物。

8. 发明授权

US5068400A Fluorine-containing mono- or poly-alkylene glycol and method for producing same 失效
标题翻译：含氟单羟基或聚烷基甘氨酸及其生产方法
公开(公告)号：US5068400A
公开(公告)日：1991-11-26
申请号：US214188
申请日：1988-06-29
申请人： Masahide Tanaka , Tokinori Agou , Masahiro Kuwahara , Takeshi Sakashita , Tomoaki Shimoda , Masaru Sudou
发明人： Masahide Tanaka , Tokinori Agou , Masahiro Kuwahara , Takeshi Sakashita , Tomoaki Shimoda , Masaru Sudou
IPC分类号： C07C31/40 , C07C43/11 , C07C43/13 , C08F283/06
CPC分类号： C07C43/137 , C07C31/40 , C07C43/11 , C08F283/06
摘要： The novel fluorine-containing mono- or poly-alkylene glycol of this invention is a mono- or poly-alkylene glycol of the formula (I): ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 independently represent a hydrogen atom or an alkyl group having 1 to 30 carbon atoms, A represents a hydrogen atom, an unsaturated hydrocarbon group having 1 to 30 carbon atoms, a polar group or a polar group substituted with an unsaturated hydrocarbon group having 1 to 100 carbon atoms, B represents the same as the group selected from the group of A, provided that both A and B are not hydrogen atom, or a hydrocarbon group having 1 to 30 carbon atoms which may contain an oxygen atom or fluorine atom, x represents an integer of 0 to 100, and n represents an integer of 1 to 1000, the mono- or poly-oxyalkylene group in the main chain of the mono- or poly-alkylene glycol having at least one fluorine-substituted hydrocarbon group with 2 to 30 carbon atoms having at least 3 fluorine atoms bonded thereto graft-bonded onto the mono- or poly-oxyalkylene group in the main chain of the mono- or poly-alkylene glycol per one molecule of the mono- or poly-alkylene glycol.

9. 发明授权

US5514767A Hot-melt polycondensation method for manufacturing a polycarbonate composition 失效
标题翻译：用于制造聚碳酸酯组合物的热熔缩缩方法
公开(公告)号：US5514767A
公开(公告)日：1996-05-07
申请号：US281965
申请日：1994-07-28
申请人： Takeshi Sakashita , Tomoaki Shimoda , Takashi Nagai , Kenichi Tominari , Akio Kanezawa
发明人： Takeshi Sakashita , Tomoaki Shimoda , Takashi Nagai , Kenichi Tominari , Akio Kanezawa
IPC分类号： C08G64/04 , C08G64/00 , C08G64/20 , C08G64/30 , C08G64/40 , C08G64/42 , C08K3/00 , C08K3/20 , C08K5/36 , C08K5/41 , C08K5/42 , C08L69/00
CPC分类号： C08G64/307
摘要： The method of the present invention is a hot-melt polycondensation for an aromatic dihydroxy compound and a dicarbonate in the presence of a basic catalyst, adding sulfur-containing acid compound with a pKa value less than 3 or the derivative thereof, and 5-1,000 ppm of water, and additives as needed for the polycarbonate while the reaction product polycarbonate is still in a molten state, and kneading the material.
摘要翻译：本发明的方法是在碱性催化剂存在下加入芳族二羟基化合物和二碳酸酯的加热熔融缩聚反应，加入pKa值小于3的含硫酸化合物或其衍生物，5-1000 ppm的水和聚碳酸酯所需的添加剂，同时反应产物聚碳酸酯仍处于熔融状态，并捏合该材料。

10. 发明授权

US5484875A Copolymeric polycarbonate production method 失效
标题翻译：共聚聚碳酸酯生产方法
公开(公告)号：US5484875A
公开(公告)日：1996-01-16
申请号：US444703
申请日：1995-05-19
申请人： Takeshi Sakashita , Tomoaki Shimoda , Kotaro Kishimura , Shuichi Uchimura
发明人： Takeshi Sakashita , Tomoaki Shimoda , Kotaro Kishimura , Shuichi Uchimura
IPC分类号： C08G64/14 , C08G64/00 , C08G64/04 , C08G64/20 , C08G64/30 , C08G64/40 , C08K3/00 , C08K3/24 , C08K5/00 , C08K5/1515 , C08K5/36 , C08K5/42 , C08K5/52 , C08L69/00 , C08G63/02
CPC分类号： C08G64/307
摘要： The present invention relates to a method for preparing copolymeric polycarbonates which comprises melt polycondensing a mixture of an aromatic dihydroxy compound containing an amount of 2-90 mol % of hydroquinone or substituted hydroquinones and a diester carbonate in the presence of a catalyst containing an alkali metal compound or an alkaline earth metal compound in an amount of 1.times.10.sup.-8 to 5.times.10.sup.-6 mole per mole of the total amount of the aromatic dihydroxy compound, then adding an acidic compound to the melt polycondensation product.
摘要翻译：本发明涉及制备共聚聚碳酸酯的方法，该方法包括在含有碱金属的催化剂存在下熔融缩聚含有2-90mol％氢醌或取代的氢醌的二芳基二羟基化合物和二酯的混合物化合物或碱土金属化合物，其量为每摩尔芳族二羟基化合物总量为1×10 -8至5×10 -6摩尔，然后向熔融缩聚产物中加入酸性化合物。

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