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1. 发明授权

US4187302A 1-[N-(4-chloro-2-trifluoromethylphenyl)phenylacetimidoyl]imidazole, metal complexes thereof, and fungicidal compositions 失效
标题翻译： 1- [N-（4-氯-2-三氟甲基苯基）苯基亚氨代乙基]咪唑，其金属络合物和杀真菌组合物
公开(公告)号：US4187302A
公开(公告)日：1980-02-05
申请号：US886358
申请日：1978-03-14
申请人： Katsuyata Ikura , Kiyoshi Katsuura , Masaaki Kataoka
发明人： Katsuyata Ikura , Kiyoshi Katsuura , Masaaki Kataoka
IPC分类号： A01N43/50 , C07D233/56 , C07D233/61 , C07D521/00 , A01N9/22 , A01N11/04
CPC分类号： C07D231/12 , A01N43/50 , C07D233/56 , C07D249/08
摘要： The compound of the formula and metal complexes thereof ##STR1## are useful as fungicide.
摘要翻译：式的化合物及其金属络合物可用作杀真菌剂。

2. 发明授权

US4208411A Imidazole derivatives having fungicidal activity 失效
标题翻译：具有杀真菌活性的咪唑衍生物
公开(公告)号：US4208411A
公开(公告)日：1980-06-17
申请号：US886558
申请日：1978-03-14
申请人： Katsuyata Ikura , Kiyoshi Katsuura , Akira Nakada , Masami Mizuno
发明人： Katsuyata Ikura , Kiyoshi Katsuura , Akira Nakada , Masami Mizuno
IPC分类号： A01N43/50 , C07D233/56 , C07D233/61 , C07D521/00 , A01N9/22 , C07F1/08 , C07F3/06
CPC分类号： C07D231/12 , A01N43/50 , C07D233/56 , C07D249/08
摘要： Compounds of the general formula ##STR1## wherein X is a same or different substituent which is halogen, lower alkyl, nitro or lower haloalkyl;n is 1 or 2;Y is alkoxyalkyl, lower alkenyloxyalkyl, phenoxyalkyl or substituted phenoxyalkyl;or metal complexes of the compounds defined herein above.The compounds are useful as fungicides.
摘要翻译：通式“IMAGE”的化合物，其中X是相同或不同的取代基，它是卤素，低级烷基，硝基或低级卤代烷基; n为1或2; Y是烷氧基烷基，低级烯氧基烷基，苯氧基烷基或取代的苯氧基烷基; 或上文定义的化合物的金属络合物。这些化合物可用作杀真菌剂。

3. 发明授权

US07943803B2 Clathrate compound, method for controlling concentration of aqueous agricultural chemical active ingredient solution, and agricultural chemical formulation 有权
标题翻译：包合化合物，农药化学活性成分溶液浓度控制方法，农药配方
公开(公告)号：US07943803B2
公开(公告)日：2011-05-17
申请号：US12662809
申请日：2010-05-04
申请人： Natsuki Amanokura , Tetsuya Sahara , Hiroshi Suzuki , Yuichi Maekawa , Kiyoshi Katsuura , Yoshihiro Enomoto
发明人： Natsuki Amanokura , Tetsuya Sahara , Hiroshi Suzuki , Yuichi Maekawa , Kiyoshi Katsuura , Yoshihiro Enomoto
IPC分类号： C07C39/15 , C07C49/784 , C07D307/02 , C07D277/28 , C07D417/06 , C07D401/06 , C07D213/57 , C07D213/26 , C07D273/04
CPC分类号： A01N51/00 , A01N25/30 , A01N47/40 , A01N53/00 , A01N25/02 , A01N25/14 , A01N31/08 , A01N35/04 , A01N2300/00
摘要： A clathrate compound containing a polymolecular host compound as a host compound and an agricultural chemical active ingredient having a saturated solubility in water at 25° C. of not less than 500 ppm as a guest compound.
摘要翻译：含有作为主体化合物的多分子宿主化合物和在25℃下在水中饱和溶解度为500ppm以上的客制化合物的农药化学活性成分的包合物化合物。

4. 发明申请

US20070281929A1 Clathrate Compound, Method for Controlling Concentration of Aqueous Agricultural Chemical Active Ingredient Solution, and Agricultural Chemical Formulation 有权
标题翻译：含水农药化学活性成分溶液浓缩方法和农药配方
公开(公告)号：US20070281929A1
公开(公告)日：2007-12-06
申请号：US11571975
申请日：2005-07-12
申请人： Natsuki Amanokura , Tetsuya Sahara , Hiroshi Suzuki , Yuichi Maekawa , Kiyoshi Katsuura , Yoshihiro Enomoto
发明人： Natsuki Amanokura , Tetsuya Sahara , Hiroshi Suzuki , Yuichi Maekawa , Kiyoshi Katsuura , Yoshihiro Enomoto
IPC分类号： A01N25/00 , A01N25/22 , A01N43/34 , A01N43/40 , A01N47/40 , A01N47/42 , A01N51/00 , A01P3/00 , A01P5/00 , A01P7/00
CPC分类号： A01N51/00 , A01N25/30 , A01N47/40 , A01N53/00 , A01N25/02 , A01N25/14 , A01N31/08 , A01N35/04 , A01N2300/00
摘要： The present invention provides a clathrate compound characterized by containing: a polymolecular host compound as a host compound; and an agricultural chemical active ingredient having a saturated solubility in water at 25° C. of not less than 500 ppm as a guest compound. The present invention also provides a method for controlling the concentration of an aqueous agricultural chemical active ingredient solution, characterized by containings a step of including an agricultural chemical active ingredient having high saturated solubility in an interior space formed of a polymolecular host compound, thereby maintaining the saturated solubility of the agricultural chemical active ingredient in water within a predetermined concentration range. The present invention also provides an agricultural chemical formulation containing the clathrate compound. The present invention also provides an agricultural active composition containing the clathrate compound and a synthetic pyrethroid.
摘要翻译：本发明提供一种包合物，其特征在于含有：作为主体化合物的多分子宿主化合物; 以及作为客体化合物，在25℃下在水中饱和溶解度不低于500ppm的农药活性成分。本发明还提供了一种控制含水农药活性成分溶液浓度的方法，其特征在于包含在由多分子宿主化合物形成的内部空间中具有高饱和溶解度的农药活性成分的步骤，从而保持农业化学活性成分在水中的饱和溶解度在预定浓度范围内。本发明还提供含有包合物化合物的农药组合物。本发明还提供含有包合物和合成拟除虫菊酯的农业活性组合物。

5. 发明授权

US07619120B2 Processes for the preparation of diphenylsulfone compounds 有权
标题翻译：二苯砜化合物的制备方法
公开(公告)号：US07619120B2
公开(公告)日：2009-11-17
申请号：US10950889
申请日：2004-09-27
申请人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
发明人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
IPC分类号： C07C315/06
CPC分类号： C07C315/04 , C07C315/06 , C07C317/22
摘要： The present invention is to provide methods for producing highly pure 4,4′-dihydroxydiphenyl sulfone monoethers advantageously in industrial production.In a process for producing a compound represented by Formula (I) (wherein, R1 and R2 are each independently halogen, alkyl having 1 to 8 carbons or alkenyl having 2 to 8 carbons; m and n are each independently 0 or an integer of 1 to 4; and R3 is alkyl having 1 to 8 carbons, alkenyl having 2 to 8 carbons, cycloalkyl having 3 to 8 carbons or optionally substituted aralkyl), (1) a pH adjustment is carried out twice or more in the purification process, (2) an excessive amount of alkyl halide used is removed, (3) a solvent, such as water, containing 0.05 ppm or less of iron components is used, (4) tanks with corrosion-resistant layers over the inner walls are used, (6) a chelating agent is added, and (7) a means of drying with mechanical stir is applied.
摘要翻译：本发明提供在工业生产中有利地生产高纯度4,4'-二羟基二苯砜单醚的方法。在制备由式（I）表示的化合物的方法中（其中，R 1和R 2各自独立地为卤素，具有1至8个碳的烷基或具有2至8个碳的烯基; m和n各自独立地为0或整数1 至4; R3为具有1至8个碳的烷基，具有2至8个碳的烯基，3至8个碳原子的环烷基或任选取代的芳烷基），（1）在纯化过程中进行两次或更多次的pH调节（ 2）除去过量的烷基卤，（3）使用含有0.05ppm以下铁组分的溶剂如水，（4）使用内壁上具有耐腐蚀层的罐（ 6）加入螯合剂，（7）用机械搅拌干燥的方法。

6. 发明授权

US4355184A Synthesis of .alpha., .beta.-unsaturated-ketones 失效
标题翻译： α，β-不饱和酮的合成
公开(公告)号：US4355184A
公开(公告)日：1982-10-19
申请号：US257639
申请日：1981-04-27
申请人： Tsutomu Kaku , Kiyoshi Katsuura , Mikio Sawaki
发明人： Tsutomu Kaku , Kiyoshi Katsuura , Mikio Sawaki
IPC分类号： C07C49/203 , B01J31/00 , B01J31/02 , C07C45/00 , C07C45/72 , C07C49/213 , C07C67/00 , C07C313/00 , C07C315/04 , C07C317/24 , C07C319/20 , C07C323/22 , C07C49/20
CPC分类号： C07C317/24 , C07C323/22 , C07C45/72
摘要： .alpha., .beta.-unsaturated-ketones are synthesized by reacting with an aldehyde and an alkali metal salt of acetoacetic acid in the presence of an aliphatic secondary amine in the mixture of heterogeneous solvents producing an oil layer and a water layer.
摘要翻译： α，β-不饱和酮通过在产生油层和水层的非均相溶剂的混合物中的脂族仲胺存在下与醛和乙酰乙酸的碱金属盐反应来合成。

7. 发明授权

US06831201B2 Process for producing diphenyl sulfone compound 有权
标题翻译：二苯砜化合物的制备方法
公开(公告)号：US06831201B2
公开(公告)日：2004-12-14
申请号：US10239483
申请日：2002-09-20
申请人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
发明人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
IPC分类号： C07C31506
CPC分类号： C07C315/04 , C07C315/06 , C07C317/22
摘要： The present invention is to provide methods for producing highly pure 4,4′-dihydroxydiphenyl sulfone monoethers advantageously in industrial production. In a process for producing a compound represented by Formula (1) (wherein, R1 and R2 are each independently halogen, alkyl having 1 to 8 carbons or alkenyl having 2 to 8 carbons; m and n are each independently 0 or an integer of 1 to 4; and R3 is alkyl having 1 to 8 carbons, alkenyl having 2 to 8 carbons, cycloalkyl having 3 to 8 carbons or optionally substituted aralkyl), (1) a pH adjustment is carried out twice or more in the purification process, (2) an excessive amount of alkyl halide used is removed, (3) a solvent, such as water, containing 0.05 ppm or less of iron components is used, (4) tanks with corrosion-resistant layers over the inner walls are used, (6) a chelating agent is added, and (7) a means of drying with mechanical stir is applied.
摘要翻译：本发明提供了在工业生产中有利地生产高纯度4,4'-二羟基二苯基砜单醚的方法。在制备由式（1）表示的化合物（其中R 1和R 2为各自独立地为卤素，具有1至8个碳的烷基或具有2至8个碳的烯基; m和n各自独立地为0或1至4的整数;并且R 3为具有1至8个碳的烷基，具有2至 8个碳原子数为3〜8的环烷基或任意取代的芳烷基），（1）在纯化工序中进行两次以上的pH调节，（2）除去过量的烷基卤，（3）溶剂使用含有0.05ppm以下的铁成分的水，（4）使用内壁具有耐腐蚀层的罐，（6）添加螯合剂，（7）使用应用机械搅拌。

8. 发明申请

US20100274006A1 Clathrate compound, method for controlling concentration of aqueous agricultural chemical active ingredient solution, and agricultural chemical formulation 有权
标题翻译：包合化合物，农药化学活性成分溶液浓度控制方法，农药配方
公开(公告)号：US20100274006A1
公开(公告)日：2010-10-28
申请号：US12662809
申请日：2010-05-04
申请人： Natsuki Amanokura , Tetsuya Sahara , Hiroshi Suzuki , Yuichi Maekawa , Kiyoshi Katsuura , Yoshihiro Enomoto
发明人： Natsuki Amanokura , Tetsuya Sahara , Hiroshi Suzuki , Yuichi Maekawa , Kiyoshi Katsuura , Yoshihiro Enomoto
IPC分类号： C07D273/04 , C07C39/367 , C07C39/15 , C07C49/825 , C07D213/53 , C07D277/28 , C07D307/14 , C07D417/06
CPC分类号： A01N51/00 , A01N25/30 , A01N47/40 , A01N53/00 , A01N25/02 , A01N25/14 , A01N31/08 , A01N35/04 , A01N2300/00
摘要： A clathrate compound containing a polymolecular host compound as a host compound and an agricultural chemical active ingredient having a saturated solubility in water at 25° C. of not less than 500 ppm as a guest compound.
摘要翻译：含有作为主体化合物的多分子宿主化合物和在25℃下在水中饱和溶解度为500ppm以上的客制化合物的农药化学活性成分的包合物化合物。

9. 发明授权

US07737309B2 Clathrate compound, method for controlling concentration of aqueous agricultural chemical active ingredient solution, and agricultural chemical formulation 有权
标题翻译：包合化合物，农药化学活性成分溶液浓度控制方法，农药配方
公开(公告)号：US07737309B2
公开(公告)日：2010-06-15
申请号：US11571975
申请日：2005-07-12
申请人： Natsuki Amanokura , Tetsuya Sahara , Hiroshi Suzuki , Yuichi Maekawa , Kiyoshi Katsuura , Yoshihiro Enomoto
发明人： Natsuki Amanokura , Tetsuya Sahara , Hiroshi Suzuki , Yuichi Maekawa , Kiyoshi Katsuura , Yoshihiro Enomoto
IPC分类号： C07C39/15 , A01N25/22 , A01N25/00 , A01N43/40 , A01N47/40 , A01N47/42 , A01N51/00
CPC分类号： A01N51/00 , A01N25/30 , A01N47/40 , A01N53/00 , A01N25/02 , A01N25/14 , A01N31/08 , A01N35/04 , A01N2300/00
摘要： The present invention provides a clathrate compound characterized by containing: a polymolecular host compound as a host compound; and an agricultural chemical active ingredient having a saturated solubility in water at 25° C. of not less than 500 ppm as a guest compound. The present invention also provides a method for controlling the concentration of an aqueous agricultural chemical active ingredient solution, characterized by containings a step of including an agricultural chemical active ingredient having high saturated solubility in an interior space formed of a polymolecular host compound, thereby maintaining the saturated solubility of the agricultural chemical active ingredient in water within a predetermined concentration range. The present invention also provides an agricultural chemical formulation containing the clathrate compound. The present invention also provides an agricultural active composition containing the clathrate compound and a synthetic pyrethroid.
摘要翻译：本发明提供一种包合物，其特征在于含有：作为主体化合物的多分子宿主化合物; 以及作为客体化合物，在25℃下在水中饱和溶解度不低于500ppm的农药活性成分。本发明还提供了一种控制含水农药活性成分溶液浓度的方法，其特征在于包含在由多分子宿主化合物形成的内部空间中具有高饱和溶解度的农药活性成分的步骤，从而保持农业化学活性成分在水中的饱和溶解度在预定浓度范围内。本发明还提供含有包合物化合物的农药组合物。本发明还提供含有包合物和合成拟除虫菊酯的农业活性组合物。

10. 发明申请

US20050065377A1 Processes for the preparation of diphenylsulfone compounds 有权
标题翻译：二苯砜化合物的制备方法
公开(公告)号：US20050065377A1
公开(公告)日：2005-03-24
申请号：US10950889
申请日：2004-09-27
申请人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
发明人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
IPC分类号： C07C315/06 , C07C317/22 , C07C317/16
CPC分类号： C07C315/04 , C07C315/06 , C07C317/22
摘要： The present invention is to provide methods for producing highly pure 4,4′-dihydroxydiphenyl sulfone monoethers advantageously in industrial production. In a process for producing a compound represented by Formula (I) (wherein, R1 and R2 are each independently halogen, alkyl having 1 to 8 carbons or alkenyl having 2 to 8 carbons; m and n are each independently 0 or an integer of 1 to 4; and R3 is alkyl having 1 to 8 carbons, alkenyl having 2 to 8 carbons, cycloalkyl having 3 to 8 carbons or optionally substituted aralkyl), (1) a pH adjustment is carried out twice or more in the purification process, (2) an excessive amount of alkyl halide used is removed, (3) a solvent, such as water, containing 0.05 ppm or less of iron components is used, (4) tanks with corrosion-resistant layers over the inner walls are used, (6) a chelating agent is added, and (7) a means of drying with mechanical stir is applied.
摘要翻译：本发明提供在工业生产中有利地生产高纯度4,4'-二羟基二苯砜单醚的方法。在制备由式（I）表示的化合物（其中R 1和R 2各自独立地为卤素，具有1至8个碳的烷基或具有2至8个碳的烯基的化合物的方法中，m和n各自独立地为 0或1〜4的整数，R 3为碳数为1〜8的烷基，碳原子数为2〜8的烯基，碳原子数为3〜8的烷基或任意取代的芳烷基），（1）进行pH调整两次以上，（2）过量使用的烷基卤被除去，（3）使用含有0.05ppm以下铁成分的溶剂，如水，（4）耐腐蚀罐使用内壁上的层，（6）加入螯合剂，和（7）应用机械搅拌干燥的方法。

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