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1. 发明授权

US09169449B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US09169449B2
公开(公告)日：2015-10-27
申请号：US13330925
申请日：2011-12-20
申请人： Bruce E. Reynolds , Julie Chabot , Erin Maris , Sean Solberg , Kaidong Chen
发明人： Bruce E. Reynolds , Julie Chabot , Erin Maris , Sean Solberg , Kaidong Chen
IPC分类号： C10G47/26 , C10G49/00 , C10G49/02 , B01J37/20 , B01J35/00 , B01J23/883 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/02 , C10G49/12
CPC分类号： C10G49/02 , B01J23/883 , B01J35/0006 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1052 , B01J35/1066 , B01J35/1076 , B01J37/0036 , B01J37/0201 , B01J37/20 , C10G49/12 , C10G2300/208 , C10G2300/4056 , C10G2300/70 , C10G2300/708 , C10G2300/802
摘要： A method to upgrade heavy oil feedstock using an ebullated bed reactor and a novel catalyst system is provided. The ebullated bed reactor system includes two different catalyst with different characteristics: an expanded catalyst zone containing particulate catalyst having a particle size of greater than 0.65 mm; and a slurry catalyst having an average particle size ranging from 1 to 300 μm. The slurry catalyst is introduced to the ebullated bed system with the heavy oil feedstock, and entrained in the upflowing hydrocarbon liquid passing through the ebullated bed reaction zone. The slurry catalyst reduces the formation of sediment and coke precursors in the ebullating bed reactor system. The slurry catalyst is prepared from at least a water-soluble metal precursor and pre-sulfided prior to being introduced with the heavy oil feedstock to the reactor system, or sulfided in-situ in the ebullated bed reactor in another embodiment.
摘要翻译：提供了一种使用沸腾床反应器和新型催化剂体系升级重油原料的方法。沸腾床反应器系统包括具有不同特性的两种不同的催化剂：包含粒度大于0.65mm的颗粒催化剂的膨胀催化剂区; 和平均粒度为1〜300μm的浆料催化剂。将浆料催化剂与重油原料引入沸腾床系统，并夹带在通过沸腾床反应区的向上流动的烃液中。浆料催化剂减少沸腾床反应器系统中沉淀物和焦炭前体的形成。浆料催化剂由至少一种水溶性金属前体制备，并在将重油原料引入反应器系统之前进行预硫化，或在另一个实施方案中在沸腾床反应器中原位硫化。

2. 发明申请

US20060054533A1 Process for recycling an active slurry catalyst composition in heavy oil upgrading 有权
标题翻译：在重油升级中回收活性淤浆催化剂组合物的方法
公开(公告)号：US20060054533A1
公开(公告)日：2006-03-16
申请号：US10938438
申请日：2004-09-10
申请人： Kaidong Chen , Julie Chabot
发明人： Kaidong Chen , Julie Chabot
IPC分类号： C10G47/24
CPC分类号： B01J27/051 , B01J27/30 , B01J35/12 , C10G2300/1003 , C10G2300/1022 , C10G2300/1033 , C10G2300/107 , C10G2300/1074 , C10G2300/1088 , C10G2300/202 , C10G2300/301 , C10G2400/06
摘要： The instant invention is directed to a process employing slurry catalyst compositions in the upgrading of heavy oils. The slurry catalyst composition is not permitted to settle, which would result in possible deactivation. The slurry is recycled to an upgrading reactor for repeated use and products require no further separation procedures for catalyst removal.
摘要翻译：本发明涉及在重油改质中使用浆料催化剂组合物的方法。不允许淤浆催化剂组合物沉降，这将导致可能的失活。将浆料再循环到升级反应器中以重复使用，并且产物不需要进一步的分离方法来除去催化剂。

3. 发明申请

US20120152806A1 Hydroprocessing Catalysts and Methods for Making Thereof 有权
标题翻译：加氢催化剂及其制备方法
公开(公告)号：US20120152806A1
公开(公告)日：2012-06-21
申请号：US13330925
申请日：2011-12-20
申请人： Bruce E. Reynolds , Julie Chabot , Erin Maris , Sean Solberg , Kaidong Chen
发明人： Bruce E. Reynolds , Julie Chabot , Erin Maris , Sean Solberg , Kaidong Chen
IPC分类号： C10G47/06 , C10G45/00 , C10G35/085 , B01J31/28 , B01J27/043 , B01J27/24 , B01J27/053 , B01J31/34 , C10G35/06 , B01J27/047
CPC分类号： C10G49/02 , B01J23/883 , B01J35/0006 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1052 , B01J35/1066 , B01J35/1076 , B01J37/0036 , B01J37/0201 , B01J37/20 , C10G49/12 , C10G2300/208 , C10G2300/4056 , C10G2300/70 , C10G2300/708 , C10G2300/802
摘要： A method to upgrade heavy oil feedstock using an ebullated bed reactor and a novel catalyst system is provided. The ebullated bed reactor system includes two different catalyst with different characteristics: an expanded catalyst zone containing particulate catalyst having a particle size of greater than 0.65 mm; and a slurry catalyst having an average particle size ranging from 1 to 300 μm. The slurry catalyst is introduced to the ebullated bed system with the heavy oil feedstock, and entrained in the upflowing hydrocarbon liquid passing through the ebullated bed reaction zone. The slurry catalyst reduces the formation of sediment and coke precursors in the ebullating bed reactor system. The slurry catalyst is prepared from at least a water-soluble metal precursor and pre-sulfided prior to being introduced with the heavy oil feedstock to the reactor system, or sulfided in-situ in the ebullated bed reactor in another embodiment.
摘要翻译：提供了一种使用沸腾床反应器和新型催化剂体系升级重油原料的方法。沸腾床反应器系统包括具有不同特性的两种不同的催化剂：包含粒度大于0.65mm的颗粒催化剂的膨胀催化剂区; 和平均粒度为1〜300μm的浆料催化剂。将浆料催化剂与重油原料引入沸腾床系统，并夹带在通过沸腾床反应区的向上流动的烃液中。浆料催化剂减少沸腾床反应器系统中沉淀物和焦炭前体的形成。浆料催化剂由至少一种水溶性金属前体制备，并在将重油原料引入反应器系统之前进行预硫化，或在另一个实施方案中在沸腾床反应器中原位硫化。

4. 发明授权

US07972499B2 Process for recycling an active slurry catalyst composition in heavy oil upgrading 有权
标题翻译：在重油升级中回收活性淤浆催化剂组合物的方法
公开(公告)号：US07972499B2
公开(公告)日：2011-07-05
申请号：US12212881
申请日：2008-09-18
申请人： Kaidong Chen , Julie Chabot
发明人： Kaidong Chen , Julie Chabot
IPC分类号： C10G47/02
CPC分类号： C10G45/16 , C10G2300/107
摘要： The instant invention is directed to a process employing slurry catalyst compositions in the upgrading of heavy oils. The slurry catalyst composition is not permitted to settle, which would result in possible deactivation. The slurry is recycled to an upgrading reactor for repeated use and products require no further separation procedures for catalyst removal.
摘要翻译：本发明涉及在重油改质中使用浆料催化剂组合物的方法。不允许淤浆催化剂组合物沉降，这将导致可能的失活。将浆料再循环到升级反应器中以重复使用，并且产物不需要进一步的分离方法来除去催化剂。

5. 发明授权

US07931796B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US07931796B2
公开(公告)日：2011-04-26
申请号：US12212737
申请日：2008-09-18
申请人： Julie Chabot , Kaidong Chen , Bruce Reynolds
发明人： Julie Chabot , Kaidong Chen , Bruce Reynolds
IPC分类号： C10G49/18
CPC分类号： C10G65/10 , C10G47/26 , C10G65/12
摘要： Systems and methods for hydroprocessing a heavy oil feedstock, the system employs a plurality of contacting zones and separation zones with at least some of the fresh slurry catalyst being supplied to at least a contacting zone other than the first contacting zone. The contacting zones operate under hydrocracking conditions, employing the slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and optionally, further treated in an in-line hydrotreater. A least a portion of the non-volatile fractions recovered from the separation zones is recycled back to the first contacting zone in the system.
摘要翻译：用于加氢处理重油原料的系统和方法，该系统采用多个接触区域和分离区域，其中至少一些新鲜浆料催化剂被供给至少是除了第一接触区域之外的接触区域。接触区在加氢裂化条件下运行，使用浆料催化剂来提升重油原料，形成较低沸点烃的升级产物。在分离区中，升级产物在顶部除去，任选地，在直列加氢处理机中进一步处理。从分离区回收的至少一部分非挥发性馏分被循环回系统中的第一接触区。

6. 发明申请

US20100065471A1 Systems and Methods for Producing a Crude Product 有权
标题翻译：生产原油产品的系统和方法
公开(公告)号：US20100065471A1
公开(公告)日：2010-03-18
申请号：US12212737
申请日：2008-09-18
申请人： Julie Chabot , Kaidong Chen , Bruce Reynolds
发明人： Julie Chabot , Kaidong Chen , Bruce Reynolds
IPC分类号： C10G49/18
CPC分类号： C10G65/10 , C10G47/26 , C10G65/12
摘要： Systems and methods for hydroprocessing a heavy oil feedstock, the system employs a plurality of contacting zones and separation zones with at least some of the fresh slurry catalyst being supplied to at least a contacting zone other than the first contacting zone. The contacting zones operate under hydrocracking conditions, employing the slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and optionally, further treated in an in-line hydrotreater. A least a portion of the non-volatile fractions recovered from the separation zones is recycled back to the first contacting zone in the system.
摘要翻译：用于加氢处理重油原料的系统和方法，该系统采用多个接触区域和分离区域，其中至少一些新鲜浆料催化剂被供给至少是除了第一接触区域之外的接触区域。接触区在加氢裂化条件下运行，使用浆料催化剂来改质重油原料，形成较低沸点沸点烃的升级产物。在分离区中，升级产物在顶部除去，任选地，在直列加氢处理机中进一步处理。从分离区回收的至少一部分非挥发性馏分被循环回系统中的第一接触区。

7. 发明申请

US20060054534A1 Process for upgrading heavy oil using a highly active slurry catalyst compositon 有权
标题翻译：使用高活性浆液催化剂组合物对重油进行改质的方法
公开(公告)号：US20060054534A1
公开(公告)日：2006-03-16
申请号：US10938200
申请日：2004-09-10
申请人： Kaidong Chen , Pak Leung , Bruce Reynolds , Julie Chabot
发明人： Kaidong Chen , Pak Leung , Bruce Reynolds , Julie Chabot
IPC分类号： C10G47/02 , C10G45/04
CPC分类号： C10G45/08 , B01J27/0515 , B01J27/053 , B01J35/12 , B01J37/20 , C10G45/16 , C10G47/02 , C10G47/06 , C10G47/26 , C10G49/12 , C10G2300/1003 , C10G2300/1022 , C10G2300/1033 , C10G2300/1074 , C10G2300/1088 , C10G2300/207 , C10G2300/703
摘要： The instant invention is directed to a process for upgrading heavy oils using a slurry composition. The slurry composition is prepared in a series of steps, involving mixing a Group VIB metal oxide with aqueous ammonia to form an aqueous mixture and sulfiding the mixture to form a slurry. The slurry is then promoted with a Group VIII metal compound. Subsequent steps involve mixing the slurry with a hydrocarbon oil, and combining the resulting mixture with hydrogen gas (under conditions which maintain the water in a liquid phase) to produce the active slurry catalyst.
摘要翻译：本发明涉及使用浆料组合物对重油进行改质的方法。浆料组合物是以一系列步骤制备的，包括将VIB族金属氧化物与氨水混合以形成含水混合物并硫化混合物形成浆料。然后用VIII族金属化合物促进该浆料。随后的步骤包括将浆料与烃油混合，并将所得混合物与氢气（在将水保持在液相中的条件下）组合以产生活性淤浆催化剂。

8. 发明申请

US20090050526A1 Process for Recycling an Active Slurry Catalyst Composition in Heavy Oil Upgrading 有权
标题翻译：在重油升级中回收活性浆料催化剂组合物的方法
公开(公告)号：US20090050526A1
公开(公告)日：2009-02-26
申请号：US12212881
申请日：2008-09-18
申请人： Kaidong Chen , Julie Chabot
发明人： Kaidong Chen , Julie Chabot
IPC分类号： C10G47/24 , C10G65/00
CPC分类号： C10G45/16 , C10G2300/107
摘要： The instant invention is directed to a process employing slurry catalyst compositions in the upgrading of heavy oils. The slurry catalyst composition is not permitted to settle, which would result in possible deactivation. The slurry is recycled to an upgrading reactor for repeated use and products require no further separation procedures for catalyst removal.
摘要翻译：本发明涉及在重油改质中使用浆料催化剂组合物的方法。不允许淤浆催化剂组合物沉降，这将导致可能的失活。将浆料再循环到升级反应器中以重复使用，并且产物不需要进一步的分离方法来除去催化剂。

9. 发明授权

US07431824B2 Process for recycling an active slurry catalyst composition in heavy oil upgrading 有权
标题翻译：在重油升级中回收活性淤浆催化剂组合物的方法
公开(公告)号：US07431824B2
公开(公告)日：2008-10-07
申请号：US10938438
申请日：2004-09-10
申请人： Kaidong Chen , Julie Chabot
发明人： Kaidong Chen , Julie Chabot
IPC分类号： C10G47/02
CPC分类号： B01J27/051 , B01J27/30 , B01J35/12 , C10G2300/1003 , C10G2300/1022 , C10G2300/1033 , C10G2300/107 , C10G2300/1074 , C10G2300/1088 , C10G2300/202 , C10G2300/301 , C10G2400/06
摘要： The instant invention is directed to a process employing slurry catalyst compositions in the upgrading of heavy oils. The slurry catalyst composition is not permitted to settle, which would result in possible deactivation. The slurry is recycled to an upgrading reactor for repeated use and products require no further separation procedures for catalyst removal.
摘要翻译：本发明涉及在重油改质中使用浆料催化剂组合物的方法。不允许淤浆催化剂组合物沉降，这将导致可能的失活。将浆料再循环到升级反应器中以重复使用，并且产物不需要进一步的分离方法来除去催化剂。

10. 发明授权

US07214309B2 Process for upgrading heavy oil using a highly active slurry catalyst composition 有权
标题翻译：使用高活性浆料催化剂组合物对重油进行改质的方法
公开(公告)号：US07214309B2
公开(公告)日：2007-05-08
申请号：US10938200
申请日：2004-09-10
申请人： Kaidong Chen , Pak C. Leung , Bruce E. Reynolds , Julie Chabot
发明人： Kaidong Chen , Pak C. Leung , Bruce E. Reynolds , Julie Chabot
IPC分类号： C10G47/02 , C10G45/04
CPC分类号： C10G45/08 , B01J27/0515 , B01J27/053 , B01J35/12 , B01J37/20 , C10G45/16 , C10G47/02 , C10G47/06 , C10G47/26 , C10G49/12 , C10G2300/1003 , C10G2300/1022 , C10G2300/1033 , C10G2300/1074 , C10G2300/1088 , C10G2300/207 , C10G2300/703
摘要： The instant invention is directed to a process for upgrading heavy oils using a slurry composition. The slurry composition is prepared in a series of steps, involving mixing a Group VIB metal oxide with aqueous ammonia to form an aqueous mixture and sulfiding the mixture to form a slurry. The slurry is then promoted with a Group VIII metal compound. Subsequent steps involve mixing the slurry with a hydrocarbon oil, and combining the resulting mixture with hydrogen gas (under conditions which maintain the water in a liquid phase) to produce the active slurry catalyst.
摘要翻译：本发明涉及使用浆料组合物对重油进行改质的方法。浆料组合物是以一系列步骤制备的，包括将VIB族金属氧化物与氨水混合以形成含水混合物并硫化混合物形成浆料。然后用VIII族金属化合物促进该浆料。随后的步骤包括将浆料与烃油混合，并将所得混合物与氢气（在将水保持在液相中的条件下）组合以产生活性浆料催化剂。

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