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1. 发明授权

US09206361B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US09206361B2
公开(公告)日：2015-12-08
申请号：US13330910
申请日：2011-12-20
申请人： Julie Chabot , Bruce E. Reynolds , Erin Maris , Shuwu Yang
发明人： Julie Chabot , Bruce E. Reynolds , Erin Maris , Shuwu Yang
IPC分类号： C10G47/26 , C10G49/02 , B01J37/20 , B01J35/00 , B01J23/883 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/02 , C10G49/12
CPC分类号： C10G49/02 , B01J23/883 , B01J35/0006 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1052 , B01J35/1066 , B01J35/1076 , B01J37/0036 , B01J37/0201 , B01J37/20 , C10G49/12 , C10G2300/208 , C10G2300/4056 , C10G2300/70 , C10G2300/708 , C10G2300/802
摘要： A method to upgrade heavy oil feedstock using an ebullated bed reactor and a novel catalyst system is provided. The ebullated bed reactor system includes two different catalyst with different characteristics: an expanded catalyst zone containing particulate catalyst having a particle size of greater than 0.65 mm; and a slurry catalyst having an average particle size ranging from 1 to 300 μm. The slurry catalyst is provided to the ebullated bed system containing the heavy oil feedstock, and entrained in the upflowing hydrocarbon liquid passing through the ebullated bed reaction zone. The slurry catalyst reduces the formation of sediment and coke precursors in the ebullating bed reactor system. The slurry catalyst is prepared from rework materials, which form a slurry catalyst in-situ upon mixing with the heavy oil feedstock.
摘要翻译：提供了一种使用沸腾床反应器和新型催化剂体系升级重油原料的方法。沸腾床反应器系统包括具有不同特性的两种不同的催化剂：包含粒度大于0.65mm的颗粒催化剂的膨胀催化剂区; 和平均粒度为1〜300μm的浆料催化剂。将浆料催化剂提供给含有重油原料的沸腾床系统，并夹带在通过沸腾床反应区的向上流动的烃液中。浆料催化剂减少沸腾床反应器系统中沉淀物和焦炭前体的形成。浆料催化剂由返工材料制备，其在与重油原料混合时原位形成浆料催化剂。

2. 发明申请

US20120152805A1 Hydroprocessing Catalysts and Methods for Making Thereof 有权
标题翻译：加氢催化剂及其制备方法
公开(公告)号：US20120152805A1
公开(公告)日：2012-06-21
申请号：US13330910
申请日：2011-12-20
申请人： Julie Chabot , Bruce E. Reynolds , Erin Maris , Shuwu Yang
发明人： Julie Chabot , Bruce E. Reynolds , Erin Maris , Shuwu Yang
IPC分类号： C10G47/00 , B01J35/10 , B01J31/02 , B01J27/02 , C10G45/02 , B01J35/02
CPC分类号： C10G49/02 , B01J23/883 , B01J35/0006 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1052 , B01J35/1066 , B01J35/1076 , B01J37/0036 , B01J37/0201 , B01J37/20 , C10G49/12 , C10G2300/208 , C10G2300/4056 , C10G2300/70 , C10G2300/708 , C10G2300/802
摘要： A method to upgrade heavy oil feedstock using an ebullated bed reactor and a novel catalyst system is provided. The ebullated bed reactor system includes two different catalyst with different characteristics: an expanded catalyst zone containing particulate catalyst having a particle size of greater than 0.65 mm; and a slurry catalyst having an average particle size ranging from 1 to 300 μm. The slurry catalyst is provided to the ebullated bed system containing the heavy oil feedstock, and entrained in the upflowing hydrocarbon liquid passing through the ebullated bed reaction zone. The slurry catalyst reduces the formation of sediment and coke precursors in the ebullating bed reactor system. The slurry catalyst is prepared from rework materials, which form a slurry catalyst in-situ upon mixing with the heavy oil feedstock.
摘要翻译：提供了一种使用沸腾床反应器和新型催化剂体系升级重油原料的方法。沸腾床反应器系统包括具有不同特性的两种不同的催化剂：包含粒度大于0.65mm的颗粒催化剂的膨胀催化剂区; 和平均粒度为1〜300μm的浆料催化剂。将浆料催化剂提供给含有重油原料的沸腾床系统，并夹带在通过沸腾床反应区的向上流动的烃液中。浆料催化剂减少沸腾床反应器系统中沉淀物和焦炭前体的形成。浆料催化剂由返工材料制备，其在与重油原料混合时原位形成浆料催化剂。

3. 发明申请

US20100065473A1 Systems and Methods for Producing a Crude Product 有权
标题翻译：生产原油产品的系统和方法
公开(公告)号：US20100065473A1
公开(公告)日：2010-03-18
申请号：US12233327
申请日：2008-09-18
申请人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
发明人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
IPC分类号： C10G35/00
CPC分类号： C10G65/12 , C10G65/10
摘要： Systems and methods for hydroprocessing a heavy oil feedstock with reduced heavy oil deposits, the system employs a plurality of contacting zones and separation zones zone under hydrocracking conditions to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products, wherein water and/or steam being injected into first contacting zone in an amount of 1 to 25 weight % on the weight of the heavy oil feedstock. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and optionally, further treated in an in-line hydrotreater. At least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to the first contacting zone in the system.
摘要翻译：用减重油沉积物加氢处理重油原料的系统和方法，该系统在加氢裂化条件下使用多个接触区和分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物，其中将水和/或蒸汽以重油原料的重量计为1至25重量％的量注入第一接触区。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂，形成较低沸点烃的升级产物。在分离区中，升级产物在顶部除去，任选地，在直列加氢处理机中进一步处理。从至少一个分离区回收的至少一部分非挥发性馏分被循环回系统中的第一接触区。

4. 发明授权

US07938954B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US07938954B2
公开(公告)日：2011-05-10
申请号：US12233439
申请日：2008-09-18
申请人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang , Bruce Reynolds
发明人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang , Bruce Reynolds
IPC分类号： C10G45/22
CPC分类号： C10G67/049 , C10G65/10
摘要： Systems and methods for hydroprocessing a heavy oil feedstock with reduced heavy oil deposits, the system employs a plurality of contacting zones and separation zones zone under hydrocracking conditions to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and optionally, further treated in an in-line hydrotreater. At least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to the first contacting zone in the system, in an amount ranging between 3 to 50 wt. % of the heavy oil feedstock.
摘要翻译：用减重油沉积物加氢处理重油原料的系统和方法，该系统在加氢裂化条件下采用多个接触区和分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。接触区在加氢裂化条件下运行，使用浆料催化剂来提升重油原料，形成较低沸点烃的升级产物。在分离区中，升级产物在顶部除去，任选地，在直列加氢处理机中进一步处理。从至少一个分离区回收的至少一部分非挥发性级分循环回系统中的第一接触区，其量为3至50wt。％的重油原料。

5. 发明授权

US07897036B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US07897036B2
公开(公告)日：2011-03-01
申请号：US12233327
申请日：2008-09-18
申请人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
发明人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
IPC分类号： C10G45/00
CPC分类号： C10G65/12 , C10G65/10
摘要： Systems and methods for hydroprocessing a heavy oil feedstock with reduced heavy oil deposits, the system employs a plurality of contacting zones and separation zones zone under hydrocracking conditions to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products, wherein water and/or steam being injected into first contacting zone in an amount of 1 to 25 weight % on the weight of the heavy oil feedstock. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and optionally, further treated in an in-line hydrotreater. At least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to the first contacting zone in the system.
摘要翻译：用减重油沉积物加氢处理重油原料的系统和方法，该系统在加氢裂化条件下使用多个接触区和分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物，其中将水和/或蒸汽以重油原料的重量计为1至25重量％的量注入第一接触区。接触区在加氢裂化条件下运行，使用浆料催化剂来提升重油原料，形成较低沸点烃的升级产物。在分离区中，升级产物在顶部除去，任选地，在直列加氢处理机中进一步处理。从至少一个分离区回收的至少一部分非挥发性馏分被循环回系统中的第一接触区。

6. 发明授权

US07935243B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US07935243B2
公开(公告)日：2011-05-03
申请号：US12233393
申请日：2008-09-18
申请人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
发明人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
IPC分类号： C10G45/00
CPC分类号： C10G65/12 , C10G65/10
摘要： Systems and methods for hydroprocessing a heavy oil feedstock with reduced heavy oil deposits, the system employs a plurality of contacting zones and separation zones zone under hydrocracking conditions to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products, wherein the first contacting zone is operated at a temperature of at least 10° F. lower than a next contacting zone. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and, optionally, further treated in an in-line hydrotreater. At least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to the first contacting zone in the system.
摘要翻译：用减重油沉积物加氢处理重油原料的系统和方法，该系统在加氢裂化条件下使用多个接触区和分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物，其中所述第一接触区域在比下一个接触区域低至少10°F的温度下操作。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂，形成较低沸点烃的升级产物。在分离区中，升级产品被顶部除去，并且任选地在直列加氢处理器中进一步处理。从至少一个分离区回收的至少一部分非挥发性馏分被循环回系统中的第一接触区。

7. 发明申请

US20100065474A1 Systems and Methods for Producing a Crude Product 有权
标题翻译：生产原油产品的系统和方法
公开(公告)号：US20100065474A1
公开(公告)日：2010-03-18
申请号：US12233393
申请日：2008-09-18
申请人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
发明人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
IPC分类号： C10G45/00
CPC分类号： C10G65/12 , C10G65/10
摘要： Systems and methods for hydroprocessing a heavy oil feedstock with reduced heavy oil deposits, the system employs a plurality of contacting zones and separation zones zone under hydrocracking conditions to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products, wherein the first contacting zone is operated at a temperature of at least 10° F. lower than a next contacting zone. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and optionally, further treated in an in-line hydrotreater. At least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to the first contacting zone in the system.
摘要翻译：用减重油沉积物加氢处理重油原料的系统和方法，该系统在加氢裂化条件下使用多个接触区和分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物，其中所述第一接触区域在比下一个接触区域低至少10°F的温度下操作。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂，形成较低沸点烃的升级产物。在分离区中，升级产物在顶部除去，任选地，在直列加氢处理机中进一步处理。从至少一个分离区回收的至少一部分非挥发性馏分被循环回系统中的第一接触区。

8. 发明申请

US20090008291A1 Systems and Methods for Producing a Crude Product 有权
标题翻译：生产原油产品的系统和方法
公开(公告)号：US20090008291A1
公开(公告)日：2009-01-08
申请号：US12233439
申请日：2008-09-18
申请人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang , Bruce Reynolds
发明人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang , Bruce Reynolds
IPC分类号： C10G45/22
CPC分类号： C10G67/049 , C10G65/10
摘要： Systems and methods for hydroprocessing a heavy oil feedstock with reduced heavy oil deposits, the system employs a plurality of contacting zones and separation zones zone under hydrocracking conditions to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and optionally, further treated in an in-line hydrotreater. At least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to the first contacting zone in the system, in an amount ranging between 3 to 50 wt. % of the heavy oil feedstock.
摘要翻译：用减重油沉积物加氢处理重油原料的系统和方法，该系统在加氢裂化条件下采用多个接触区和分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂，形成较低沸点烃的升级产物。在分离区中，升级产物在顶部除去，任选地，在直列加氢处理机中进一步处理。从至少一个分离区回收的至少一部分非挥发性级分循环回系统中的第一接触区，其量为3至50wt。％的重油原料。

9. 发明授权

US09169449B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US09169449B2
公开(公告)日：2015-10-27
申请号：US13330925
申请日：2011-12-20
申请人： Bruce E. Reynolds , Julie Chabot , Erin Maris , Sean Solberg , Kaidong Chen
发明人： Bruce E. Reynolds , Julie Chabot , Erin Maris , Sean Solberg , Kaidong Chen
IPC分类号： C10G47/26 , C10G49/00 , C10G49/02 , B01J37/20 , B01J35/00 , B01J23/883 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/02 , C10G49/12
CPC分类号： C10G49/02 , B01J23/883 , B01J35/0006 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1052 , B01J35/1066 , B01J35/1076 , B01J37/0036 , B01J37/0201 , B01J37/20 , C10G49/12 , C10G2300/208 , C10G2300/4056 , C10G2300/70 , C10G2300/708 , C10G2300/802
摘要： A method to upgrade heavy oil feedstock using an ebullated bed reactor and a novel catalyst system is provided. The ebullated bed reactor system includes two different catalyst with different characteristics: an expanded catalyst zone containing particulate catalyst having a particle size of greater than 0.65 mm; and a slurry catalyst having an average particle size ranging from 1 to 300 μm. The slurry catalyst is introduced to the ebullated bed system with the heavy oil feedstock, and entrained in the upflowing hydrocarbon liquid passing through the ebullated bed reaction zone. The slurry catalyst reduces the formation of sediment and coke precursors in the ebullating bed reactor system. The slurry catalyst is prepared from at least a water-soluble metal precursor and pre-sulfided prior to being introduced with the heavy oil feedstock to the reactor system, or sulfided in-situ in the ebullated bed reactor in another embodiment.
摘要翻译：提供了一种使用沸腾床反应器和新型催化剂体系升级重油原料的方法。沸腾床反应器系统包括具有不同特性的两种不同的催化剂：包含粒度大于0.65mm的颗粒催化剂的膨胀催化剂区; 和平均粒度为1〜300μm的浆料催化剂。将浆料催化剂与重油原料引入沸腾床系统，并夹带在通过沸腾床反应区的向上流动的烃液中。浆料催化剂减少沸腾床反应器系统中沉淀物和焦炭前体的形成。浆料催化剂由至少一种水溶性金属前体制备，并在将重油原料引入反应器系统之前进行预硫化，或在另一个实施方案中在沸腾床反应器中原位硫化。

10. 发明申请

US20120152806A1 Hydroprocessing Catalysts and Methods for Making Thereof 有权
标题翻译：加氢催化剂及其制备方法
公开(公告)号：US20120152806A1
公开(公告)日：2012-06-21
申请号：US13330925
申请日：2011-12-20
申请人： Bruce E. Reynolds , Julie Chabot , Erin Maris , Sean Solberg , Kaidong Chen
发明人： Bruce E. Reynolds , Julie Chabot , Erin Maris , Sean Solberg , Kaidong Chen
IPC分类号： C10G47/06 , C10G45/00 , C10G35/085 , B01J31/28 , B01J27/043 , B01J27/24 , B01J27/053 , B01J31/34 , C10G35/06 , B01J27/047
CPC分类号： C10G49/02 , B01J23/883 , B01J35/0006 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1052 , B01J35/1066 , B01J35/1076 , B01J37/0036 , B01J37/0201 , B01J37/20 , C10G49/12 , C10G2300/208 , C10G2300/4056 , C10G2300/70 , C10G2300/708 , C10G2300/802
摘要： A method to upgrade heavy oil feedstock using an ebullated bed reactor and a novel catalyst system is provided. The ebullated bed reactor system includes two different catalyst with different characteristics: an expanded catalyst zone containing particulate catalyst having a particle size of greater than 0.65 mm; and a slurry catalyst having an average particle size ranging from 1 to 300 μm. The slurry catalyst is introduced to the ebullated bed system with the heavy oil feedstock, and entrained in the upflowing hydrocarbon liquid passing through the ebullated bed reaction zone. The slurry catalyst reduces the formation of sediment and coke precursors in the ebullating bed reactor system. The slurry catalyst is prepared from at least a water-soluble metal precursor and pre-sulfided prior to being introduced with the heavy oil feedstock to the reactor system, or sulfided in-situ in the ebullated bed reactor in another embodiment.
摘要翻译：提供了一种使用沸腾床反应器和新型催化剂体系升级重油原料的方法。沸腾床反应器系统包括具有不同特性的两种不同的催化剂：包含粒度大于0.65mm的颗粒催化剂的膨胀催化剂区; 和平均粒度为1〜300μm的浆料催化剂。将浆料催化剂与重油原料引入沸腾床系统，并夹带在通过沸腾床反应区的向上流动的烃液中。浆料催化剂减少沸腾床反应器系统中沉淀物和焦炭前体的形成。浆料催化剂由至少一种水溶性金属前体制备，并在将重油原料引入反应器系统之前进行预硫化，或在另一个实施方案中在沸腾床反应器中原位硫化。

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