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1. 发明申请

US20150329790A1 SYSTEMS AND METHODS FOR PRODUCING A CRUDE PRODUCT 审中-公开
标题翻译：用于生产原料产品的系统和方法
公开(公告)号：US20150329790A1
公开(公告)日：2015-11-19
申请号：US14279093
申请日：2014-05-15
申请人： Shuwu YANG , Julie CHABOT , Bruce Edward REYNOLDS , Bo KOU
发明人： Shuwu YANG , Julie CHABOT , Bruce Edward REYNOLDS , Bo KOU
IPC分类号： C10G65/10
CPC分类号： C10G65/10 , C10G65/12
摘要： Systems and methods for hydroprocessing heavy oil feedstocks are disclosed. The process employs a plurality of contacting zones operating under hydrocracking conditions and at least one separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. The first contacting zone consists of one or more ebullated bed reactors. Most of the metals in the heavy oil feed are converted and adsorbed on the ebullated bed catalyst and can be removed during catalyst replacement. The second contacting zone consists of one or more slurry phase reactors. The slurry phase reactor can be operated at higher temperature to achieve higher conversion.
摘要翻译：公开了用于加氢处理重油原料的系统和方法。该方法采用在加氢裂化条件下操作的多个接触区和至少一个分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。第一接触区由一个或多个沸腾床反应器组成。重油进料中的大部分金属被转化并吸附在沸腾床催化剂上，并且可以在催化剂更换期间除去。第二接触区由一个或多个淤浆相反应器组成。浆料相反应器可以在更高的温度下运行以实现更高的转化率。

2. 发明授权

US08435400B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US08435400B2
公开(公告)日：2013-05-07
申请号：US13103790
申请日：2011-05-09
申请人： Bo Kou , Shuwu Yang , Bruce Reynolds , Julie Chabot
发明人： Bo Kou , Shuwu Yang , Bruce Reynolds , Julie Chabot
IPC分类号： C10G65/10
CPC分类号： C10G47/02 , C10G47/26 , C10G47/32 , C10G65/02 , C10G65/10 , C10G65/18 , C10G2300/1044 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/4081 , C10G2300/44 , C10G2300/80 , C10G2300/805
摘要： Systems and methods for hydroprocessing heavy oil feedstock is disclosed. The process employs a plurality of contacting zones and at least a separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. In one embodiment, water and/or steam being injected into at least a contacting zone. The contacting zones operate under hydrocracking conditions, employing at least a slurry catalyst. In one embodiment, at least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to at least a contacting zone (“recycled mode”). In one embodiment, the number of separation zones is less than the number of contacting zones in the system. In the separation zones, upgraded products are removed overhead and optionally treated in an in-line hydrotreater; and the bottom stream is optionally further treated in a fractionator.
摘要翻译：公开了用于加氢处理重油原料的系统和方法。该方法采用多个接触区和至少一个分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。在一个实施方案中，将水和/或蒸汽注入至少一个接触区。接触区在加氢裂化条件下运行，至少使用浆料催化剂。在一个实施方案中，从至少一个分离区回收的至少一部分非挥发性馏分被再循环回至少一个接触区（“再循环模式”）。在一个实施例中，分离区的数量小于系统中接触区的数量。在分离区中，升级后的产品被顶部除去并任选地在直列加氢处理器中处理; 并且底部物流任选地在分馏器中进一步处理。

3. 发明授权

US09321037B2 Hydroprocessing co-catalyst compositions and methods of introduction thereof into hydroprocessing units 有权
标题翻译：加氢处理助催化剂组合物及其引入加氢处理装置的方法
公开(公告)号：US09321037B2
公开(公告)日：2016-04-26
申请号：US13715918
申请日：2012-12-14
申请人： Julie Chabot , Bo Kou , Alexander Kuperman
发明人： Julie Chabot , Bo Kou , Alexander Kuperman
IPC分类号： B01J8/20 , B01J23/78 , B01J23/28 , B01J23/30 , B01J23/75 , B01J23/755 , B01J35/00 , B01J23/85 , B01J31/02 , B01J35/02 , B01J37/00 , B01J31/04 , B01J31/06 , C10G45/08 , C10G45/16 , B01J37/04 , B01J21/02 , B01J21/06 , B01J21/10 , B01J21/12
CPC分类号： B01J23/78 , B01J21/02 , B01J21/06 , B01J21/10 , B01J21/12 , B01J23/28 , B01J23/30 , B01J23/75 , B01J23/755 , B01J23/85 , B01J31/0247 , B01J31/04 , B01J31/06 , B01J35/0006 , B01J35/023 , B01J37/0036 , B01J37/04 , C10G45/08 , C10G45/16 , C10G2300/1033 , C10G2300/202
摘要： A hydroprocessing co-catalyst composition may comprise in an embodiment a first component comprising co-catalyst particles and a liquid carrier, and a second component comprising a dispersant and a dispersant diluent. The co-catalyst particles may be in the micron size range, and the dispersant may promote dispersion of the co-catalyst particles in materials such as the liquid carrier, the dispersant diluent, and combinations thereof. Methods of introducing a hydroprocessing co-catalyst composition into a hydroprocessing system are also disclosed.
摘要翻译：加氢处理助催化剂组合物可以在一个实施方案中包括包含助催化剂颗粒和液体载体的第一组分，和包含分散剂和分散剂稀释剂的第二组分。助催化剂颗粒可以在微米尺寸范围内，并且分散剂可以促进助催化剂颗粒在诸如液体载体，分散剂稀释剂及其组合的材料中的分散。还公开了将加氢助催化剂组合物引入加氢处理系统的方法。

4. 发明授权

US08846560B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US08846560B2
公开(公告)日：2014-09-30
申请号：US13331274
申请日：2011-12-20
申请人： Shuwu Yang , Bruce Edward Reynolds , Julie Chabot , Bo Kou
发明人： Shuwu Yang , Bruce Edward Reynolds , Julie Chabot , Bo Kou
IPC分类号： B01J23/00 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/70 , B01J23/74 , B01J27/02 , B01J27/043 , B01J27/045 , B01J27/24 , B01J31/00 , B01J23/883 , B01J27/051 , B01J23/85 , B01J37/20 , B01J23/887 , C10G49/04 , B01J23/24 , B01J35/00 , B01J35/10
CPC分类号： B01J23/883 , B01J23/24 , B01J23/85 , B01J23/8872 , B01J23/8873 , B01J27/051 , B01J27/0515 , B01J35/0073 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1095 , B01J37/20 , C10G49/04 , C10G49/06 , C10G49/12 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/301 , C10G2300/701 , C10G2300/703 , C10G2300/802
摘要： A process for preparing a slurry catalyst is provided. The slurry catalyst is prepared from at least a Group VIB metal precursor and optionally at least a Promoter metal precursor selected from Group VIII, Group IIB, Group IIA, Group IVA metals and combinations thereof. The slurry catalyst comprises a plurality of dispersed particles in a hydrocarbon medium having an average particle size ranging from 1 to 300 μm. The slurry catalyst is then mixed with a hydrogen feed at a pressure from 1435 psig (10 MPa) to 3610 psig (25 MPa) and a temperature from 200-800° F. at 500 to 15,000 scf hydrogen per bbl of slurry catalyst for a minute to 20 hours, for the slurry catalyst to be saturated with hydrogen providing an increase of k-values in terms of HDS, HDN, and HDMCR of at least 15% compared to a slurry catalyst that is not saturated with hydrogen.
摘要翻译：提供了一种制备浆料催化剂的方法。浆料催化剂由至少VIB族金属前体和任选的至少一种选自VIII族，IIB族，IIA族，IVA族金属及其组合的促进剂金属前体制备。浆料催化剂在平均粒度为1〜300μm的烃介质中含有多个分散粒子。然后将浆料催化剂与氢气进料混合，压力为1435psig（10MPa）至3610psig（25MPa），温度为200-800°F，每桶浆料催化剂为500至15,000scf氢气分钟至20小时，浆液催化剂用氢饱和，与不饱和氢气的浆料催化剂相比，HDS，HDN和HDMCR的k值提高至少15％。

5. 发明申请

US20140171299A1 HYDROPROCESSING CO-CATALYST COMPOSITIONS AND METHODS OF INTRODUCTION THEREOF INTO HYDROPROCESSING UNITS 有权
标题翻译：氢化催化剂组合物及其引入方法进入水解单位
公开(公告)号：US20140171299A1
公开(公告)日：2014-06-19
申请号：US13715943
申请日：2012-12-14
申请人： Julie Chabot , Bo Kou , Alexander Kuperman
发明人： Julie Chabot , Bo Kou , Alexander Kuperman
IPC分类号： B01J23/78 , B01J23/75 , B01J23/755 , B01J23/28 , B01J23/30
CPC分类号： B01J23/78 , B01J21/02 , B01J21/06 , B01J21/10 , B01J21/12 , B01J23/28 , B01J23/30 , B01J23/75 , B01J23/755 , B01J23/85 , B01J31/0205 , B01J31/0247 , B01J35/0006 , B01J35/023 , B01J37/0036 , B01J37/04 , C10G47/26 , C10G49/02 , C10G49/12
摘要： A hydroprocessing co-catalyst composition may comprise in an embodiment a first component comprising co-catalyst particles and a liquid carrier, and a second component comprising a dispersant and a dispersant diluent. The co-catalyst particles may be in the micron size range, and the dispersant may promote dispersion of the co-catalyst particles in materials such as the liquid carrier, the dispersant diluent, and combinations thereof. Methods of introducing a hydroprocessing co-catalyst composition into a hydroprocessing system are also disclosed.
摘要翻译：加氢处理助催化剂组合物可以在一个实施方案中包括包含助催化剂颗粒和液体载体的第一组分，和包含分散剂和分散剂稀释剂的第二组分。助催化剂颗粒可以在微米尺寸范围内，并且分散剂可以促进助催化剂颗粒在诸如液体载体，分散剂稀释剂及其组合的材料中的分散。还公开了将加氢助催化剂组合物引入加氢处理系统的方法。

6. 发明申请

US20140166541A1 HYDROPROCESSING CO-CATALYST COMPOSITIONS AND METHODS OF INTRODUCTION THEREOF INTO HYDROPROCESSING UNITS 审中-公开
公开(公告)号：US20140166541A1
公开(公告)日：2014-06-19
申请号：US13715959
申请日：2012-12-14
申请人： Julie Chabot , Bo Kou , Alexander Kuperman
发明人： Julie Chabot , Bo Kou , Alexander Kuperman
IPC分类号： C10G45/04
CPC分类号： C10G45/04 , C10G45/16
摘要： A hydroprocessing co-catalyst composition may comprise in an embodiment a first component comprising co-catalyst particles and a liquid carrier, and a second component comprising a dispersant and a dispersant diluent. The co-catalyst particles may be in the micron size range, and the dispersant may promote dispersion of the co-catalyst particles in materials such as the liquid carrier, the dispersant diluent, and combinations thereof. Methods of introducing a hydroprocessing co-catalyst composition into a hydroprocessing system are also disclosed.

7. 发明申请

US20120172201A1 HYDROPROCESSING CATALYSTS AND METHODS FOR MAKING THEREOF 有权
标题翻译：氢化催化剂及其制备方法
公开(公告)号：US20120172201A1
公开(公告)日：2012-07-05
申请号：US13331274
申请日：2011-12-20
申请人： Shuwu Yang , Bruce Edward Reynolds , Julie Chabot , Bo Kou
发明人： Shuwu Yang , Bruce Edward Reynolds , Julie Chabot , Bo Kou
IPC分类号： B01J37/18 , B01J27/043 , B01J37/20 , B01J27/047
CPC分类号： B01J23/883 , B01J23/24 , B01J23/85 , B01J23/8872 , B01J23/8873 , B01J27/051 , B01J27/0515 , B01J35/0073 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1095 , B01J37/20 , C10G49/04 , C10G49/06 , C10G49/12 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/301 , C10G2300/701 , C10G2300/703 , C10G2300/802
摘要： A process for preparing a slurry catalyst is provided. The slurry catalyst is prepared from at least a Group VIB metal precursor and optionally at least a Promoter metal precursor selected from Group VIII, Group IIB, Group IIA, Group IVA metals and combinations thereof. The slurry catalyst comprises a plurality of dispersed particles in a hydrocarbon medium having an average particle size ranging from 1 to 300 nm. The slurry catalyst is then mixed with a hydrogen feed at a pressure from 1435 psig (10 MPa) to 3610 psig (25 MPa) and a temperature from 200-800° F. at 500 to 15,000 scf hydrogen per bbl of slurry catalyst for a minute to 20 hours, for the slurry catalyst to be saturated with hydrogen providing an increase of k-values in terms of HDS, HDN, and HDMCR of at least 15% compared to a slurry catalyst that is not saturated with hydrogen.
摘要翻译：提供了一种制备浆料催化剂的方法。浆料催化剂由至少VIB族金属前体和任选的至少一种选自VIII族，IIB族，IIA族，IVA族金属及其组合的促进剂金属前体制备。浆料催化剂在平均粒径为1〜300nm的烃介质中含有多个分散粒子。然后将浆料催化剂与氢气进料混合，压力为1435psig（10MPa）至3610psig（25MPa），温度为200-800°F，每桶浆料催化剂为500至15,000scf氢气分钟至20小时，浆液催化剂用氢饱和，与不饱和氢气的浆料催化剂相比，HDS，HDN和HDMCR的k值提高至少15％。

8. 发明申请

US20120004091A1 HYDROPROCESSING CATALYSTS AND METHODS FOR MAKING THEREOF 有权
标题翻译：氢化催化剂及其制备方法
公开(公告)号：US20120004091A1
公开(公告)日：2012-01-05
申请号：US13233491
申请日：2011-09-15
申请人： Bo Kou , Julie Chabot
发明人： Bo Kou , Julie Chabot
IPC分类号： B01J38/48 , B01J38/60
CPC分类号： C10G47/02 , C10G47/26 , C10G47/32 , C10G65/00 , C10G65/10 , C10G65/18 , C10G2300/205 , C10G2300/206 , C10G2300/701 , C10G2300/802
摘要： A method to prepare an improved catalyst feed to a system to upgrade heavy oil. The method comprises: providing a spent catalyst that has been used in a hydroprocessing operation has with a solid content ranging from 5 to 50 wt. % in soluble hydrocarbons and having less than 80% but more than 10% of original catalytic activity; removing at least 50% of the soluble hydrocarbons removed in a deoiling step; treating the deoiled spent catalyst with a treating solution containing at least one of plain water, a mineral acid, an oxidizing agent, and combinations thereof to reduce the concentration of at least one metal contaminant in the deoiled spent catalyst by at least 40%. After treatment, the treated deoiled spent catalyst is slurried in a hydrocarbon medium, and fed to the heavy oil upgrade system as part of the catalyst feed system with a fresh slurry catalyst.
摘要翻译：一种制备改进的催化剂进料到系统以升级重油的方法。该方法包括：提供已经在加氢操作中使用的废催化剂的固体含量范围为5-50wt。％的可溶性碳氢化合物，并且具有小于80％但大于10％的原始催化活性; 去除在脱油步骤中去除的至少50％的可溶性烃; 用含有浅水，无机酸，氧化剂及其组合中的至少一种的处理溶液处理脱油的废催化剂，以将去除的废催化剂中的至少一种金属污染物的浓度降低至少40％。处理后，经处理的脱油废催化剂在烃介质中浆化，并作为催化剂进料系统的一部分用新鲜的浆料催化剂进料至重油升级系统。

9. 发明申请

US20120000821A1 HYDROPROCESSING CATALYSTS AND METHODS FOR MAKING THEREOF 有权
标题翻译：氢化催化剂及其制备方法
公开(公告)号：US20120000821A1
公开(公告)日：2012-01-05
申请号：US13233477
申请日：2011-09-15
申请人： Shuwu Yang , Julie Chabot , Bruce Edward Reynolds , Bo Kou
发明人： Shuwu Yang , Julie Chabot , Bruce Edward Reynolds , Bo Kou
IPC分类号： C10G65/10
CPC分类号： C10G47/02 , C10G47/26 , C10G47/32 , C10G47/36 , C10G65/00 , C10G65/10 , C10G65/18 , C10G2300/205 , C10G2300/4075 , C10G2300/701 , C10G2300/802
摘要： A method to reduce metal deposit in the hydroprocessing or upgrade of heavy oil feedstock is provided. The method comprises feeding an improved catalyst feed to the system, with the improved catalyst feed comprising a fresh slurry catalyst and a deoiled spent catalyst, with the deoiled spent catalyst being present in an amount of at least 10% the catalyst feed for the heavy oil upgrade system to have at least a 5% reduction in metal contaminant build-up compared to heavy oil upgrade system without the deoiled spent catalyst in the feed.
摘要翻译：提供了一种在重油原料的加氢处理或升级中减少金属沉积的方法。该方法包括将改进的催化剂进料进料给系统，改进的催化剂进料包含新鲜的浆料催化剂和脱油的废催化剂，脱油的废催化剂的存在量为重油的催化剂进料的至少10％升级系统与重油升级系统相比，金属污染物累积量减少至少5％，而在进料中没有脱油废催化剂。

10. 发明授权

US07935243B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US07935243B2
公开(公告)日：2011-05-03
申请号：US12233393
申请日：2008-09-18
申请人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
发明人： Julie Chabot , Bo Kou , Vivion Andrew Brennan , Erin Maris , Shuwu Yang
IPC分类号： C10G45/00
CPC分类号： C10G65/12 , C10G65/10
摘要： Systems and methods for hydroprocessing a heavy oil feedstock with reduced heavy oil deposits, the system employs a plurality of contacting zones and separation zones zone under hydrocracking conditions to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products, wherein the first contacting zone is operated at a temperature of at least 10° F. lower than a next contacting zone. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and, optionally, further treated in an in-line hydrotreater. At least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to the first contacting zone in the system.
摘要翻译：用减重油沉积物加氢处理重油原料的系统和方法，该系统在加氢裂化条件下使用多个接触区和分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物，其中所述第一接触区域在比下一个接触区域低至少10°F的温度下操作。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂，形成较低沸点烃的升级产物。在分离区中，升级产品被顶部除去，并且任选地在直列加氢处理器中进一步处理。从至少一个分离区回收的至少一部分非挥发性馏分被循环回系统中的第一接触区。

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