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1. 发明授权

US07858154B2 Paper coating slip based on pigment-polymer hybrids 有权
标题翻译：基于颜料 - 聚合物杂化物的纸涂层滑移
公开(公告)号：US07858154B2
公开(公告)日：2010-12-28
申请号：US11719219
申请日：2005-11-05
申请人： Juergen Schmidt-Thuemmes , Hubertus Kroener
发明人： Juergen Schmidt-Thuemmes , Hubertus Kroener
IPC分类号： B05D1/04 , C09D4/00
CPC分类号： D21H19/58 , D21H19/42 , Y10T428/31895
摘要： A paper coating slip comprising at least one inorganic pigment and, based on 100 parts by weight of the inorganic pigments, less than 40 parts by weight of organic polymers, and less than 25 parts by weight of water or other solvents having a boiling point below 150° C. at 1 bar.
摘要翻译：包含至少一种无机颜料的纸涂层滑爽剂，基于100重量份的无机颜料，少于40重量份的有机聚合物和小于25重量份的沸点低于25重量份的水或其它溶剂 150℃，1巴。

2. 发明申请

US20110229731A1 PROCESS FOR THE PREPARATION OF AQUEOUS POLYMER DISPERSIONS FROM A AROMATIC COMPOUND, A CONJUGATED ALIPHATIC DIENE AND AN ETHYLENICALLY UNSATURATED CARBONITRILE 有权
标题翻译：用于制备芳族聚合物分散体的方法，由芳族化合物，共轭二醇和乙烯基不饱和碳原子
公开(公告)号：US20110229731A1
公开(公告)日：2011-09-22
申请号：US13129327
申请日：2009-11-20
申请人： Elitsa Evstatieva , Juergen Schmidt-Thuemmes , Dirk Lawrenz
发明人： Elitsa Evstatieva , Juergen Schmidt-Thuemmes , Dirk Lawrenz
IPC分类号： B32B27/10 , C08L3/00 , C09J103/00 , C09D103/00
CPC分类号： C08F251/00 , C08F251/02 , C08F279/02 , C08F279/04 , C08L51/02 , C08L55/02 , C09D151/02 , C09D155/02 , Y10T428/31906 , C08L2666/02
摘要： A process for the preparation of aqueous polymer dispersions is described, a vinylaromatic compound, such as, for example, styrene, a conjugated aliphatic diene, such as, for example, butadiene, and an ethylenically unsaturated carbonitrile, such as, for example, acrylonitrile, being copolymerized in an aqueous medium. The copolymerization is effected in the presence of a degraded starch and of free radical initiators. At least part of the monomers differing from ethylenically unsaturated carbonitriles are polymerized before the ethylenically unsaturated carbonitriles are added to the polymerization mixture.
摘要翻译：描述了制备聚合物水分散体的方法，乙烯基芳族化合物，例如苯乙烯，共轭脂族二烯，例如丁二烯和烯键式不饱和腈，例如丙烯腈，在水性介质中共聚。共聚反应在降解淀粉和自由基引发剂存在下进行。不同于烯属不饱和碳原子的单体的至少一部分在将烯属不饱和碳原子加入聚合混合物之前聚合。

3. 发明授权

US5324772A Aqueous polymer dispersion 失效
标题翻译：聚合物水分散体
公开(公告)号：US5324772A
公开(公告)日：1994-06-28
申请号：US983405
申请日：1992-11-30
申请人： Juergen Schmidt-Thuemmes , Guenter Eckert
发明人： Juergen Schmidt-Thuemmes , Guenter Eckert
IPC分类号： C08F2/22 , C08F4/30 , C08F4/40 , C08F220/12 , C08L33/00 , C14C11/00
CPC分类号： C08F220/12
摘要： An aqueous polymer dispersion gives a film having high resilience in conjunction with reduced surface tack and good aging resistance under the action of light, heat and oxygen and is used for coating leather.
摘要翻译：水性聚合物分散体在光，热和氧的作用下，提供具有高回弹性的薄膜，结合降低的表面粘着性和良好的耐老化性，并用于涂布皮革。

4. 发明授权

US4814308A Preparation of homopolymers and copolymers of ethene by Phillips catalysis 失效
标题翻译：通过菲利普斯催化制备乙烯的均聚物和共聚物
公开(公告)号：US4814308A
公开(公告)日：1989-03-21
申请号：US110872
申请日：1987-10-21
申请人： Rainer Konrad , Guido Funk , Juergen Schmidt-Thuemmes , Rudolf Mueller-Mall , Guenther Schweier
发明人： Rainer Konrad , Guido Funk , Juergen Schmidt-Thuemmes , Rudolf Mueller-Mall , Guenther Schweier
IPC分类号： C08F4/02 , C08F4/24 , C08F4/48 , C08F4/62 , C08F10/02
CPC分类号： C08F10/02
摘要： Ethene polymerization by Phillips catalysis is carried out using (1) a supported catalyst, which is laden with chromium, phosphorus and aluminum, and (2) a cocatalyst, (1) being obtained by a method in which (1.1) a catalyst intermediate laden with chromium, phosphorus and aluminum is prepared from a silicate carrier, a selected chromium compound, a selected phosphorus compound and a selected aluminum compound, and then (1.2) the catalyst intermediate is heated in an oxygen-containing gas stream. In this process, the component (1) used is one which is obtained by a method in which, in each case in a specific manner, (1.1) in a first stage, (1.1.1) first a suspension is prepared from (1.1.1.1) a finely divided silicate carrier and (1.1.1.2) an inert organic solvent, (1.1.2) then, (1.1.2.1) in an inert organic solvent, (1.1.2.2) an organic chromium compound is combined with (1.1.2.3) an aluminum trialkyl, (1.1.3) then (1.1.3.1) the suspension resulting from (1.1.1) is combined with (1.1.3.2) a phosphoric acid or phosphite and (1.1.3.3) the product obtained from (1.1.2), (1.1.4) finally, the suspension obtained in (1.1.3) is evaporated to dryness, and then (1.2) in a second stage, first (1.2.1) the intermediate obtained from (1.1) is treated with a stream of nitrogen, then (1.2.2) the intermediate obtained from (1.2.1) is heated in an oxygen-containing gas stream, and finally (1.2.3) the intermediate obtained from (1.2.2) is treated with a stream of nitrogen, and both a lithiumalkyl and a boronalkyl are used as (2).
摘要翻译：通过菲利普斯催化进行的乙烯聚合使用（1）负载催化剂，其载有铬，磷和铝，和（2）助催化剂，（1）通过以下方法获得：（1）将载体催化剂中间体由硅酸盐载体，选择的铬化合物，选择的磷化合物和选择的铝化合物制备铬，磷和铝，然后（1.2）在含氧气流中加热催化剂中间体。在该方法中，所使用的组分（1）是通过在每种情况下以具体方式（1.1）在第一阶段（1.1.1）中首先从（1.1）制备悬浮液的方法获得的组分 .1.1）精细分散的硅酸盐载体和（1.1.1.2）惰性有机溶剂（1.1.2）然后，（1.1.2.1）在惰性有机溶剂（1.1.2.2）中将有机铬化合物与（ 1.1.2.3）三烷基铝（1.1.3）然后（1.1.3.1）将由（1.1.1）得到的悬浮液与（1.1.3.2）磷酸或亚磷酸酯和（1.1.3.3）得到的产物从（1.1.2），（1.1.4）最终得到的（1.1.3）中得到的悬浮液蒸发至干，然后在第二阶段（1.2）中，首先（1.2.1）从（1.1 ）用氮气流处理，然后（1.2.2）从（1.2.1）获得的中间体在含氧气流中加热，最后（1.2.3）从（1.2.2）得到的中间体用氮气流和二氧化钛处理和硼烷基用作（2）。

5. 发明授权

US08449721B2 Aqueous suspensions of fine-particulate fillers, method for the manufacture thereof and use thereof for the manufacture of fluid-containing papers 失效
标题翻译：微粒填料的水性悬浮液，其制造方法及其制造含流体纸的用途
公开(公告)号：US08449721B2
公开(公告)日：2013-05-28
申请号：US13002351
申请日：2009-06-30
申请人： Juergen Schmidt-Thuemmes , Anton Esser , Joerg Nieberle
发明人： Juergen Schmidt-Thuemmes , Anton Esser , Joerg Nieberle
IPC分类号： D21H17/46 , D21H17/63 , C08L43/02
CPC分类号： D21H17/69 , C01P2004/62 , C09C1/021 , C09C1/42 , C09C3/10 , D21H17/10 , D21H17/36 , D21H17/37 , D21H17/55 , D21H21/10 , Y10T428/2982
摘要： Aqueous slurries of finely divided fillers which are at least partly covered by anionic latices, the slurries being obtainable by treating aqueous slurries of finely divided fillers with at least one anionic latex which comprises, incorporated in the form of polymerized units, at least one monomer comprising phosphonic and/or phosphoric acid groups, preparation of the aqueous slurries and their use as an additive to the paper stock in the production of filler-containing paper, filler-containing cardboard or filler-containing board by draining the paper stock.
摘要翻译：至少部分地由阴离子胶乳覆盖的细分散填料的水性浆料，浆料可通过用至少一种阴离子胶乳处理细分散填料的水性浆料而获得，所述阴离子胶乳包含以聚合单元形式结合的至少一种单体，所述单体包含膦酸和/或磷酸基团，水性浆料的制备以及它们在通过排出纸料而生产含填料的纸，含填料的纸板或含填料的板中作为纸料添加剂的用途。

6. 发明授权

US08034885B2 Free-radical polymerization process producing aqueous polymer dispersion with low residual monomer content utilizing oil and water soluble initiators 有权
标题翻译：使用油和水溶性引发剂制备具有低残留单体含量的聚合物水分散体的自由基聚合方法
公开(公告)号：US08034885B2
公开(公告)日：2011-10-11
申请号：US10566248
申请日：2004-07-08
申请人： Jun Gao , Xiang-Ming Kong , Klaus-Dieter Hungenberg , Juergen Schmidt-Thuemmes
发明人： Jun Gao , Xiang-Ming Kong , Klaus-Dieter Hungenberg , Juergen Schmidt-Thuemmes
IPC分类号： C08F2/00 , C08F2/16 , C08G85/00
CPC分类号： C08F2/22
摘要： The present invention provides a novel one-step process for preparing an aqueous polymer dispersion by the free radical aqueous emulsion polymerization comprising mixing at least water, a dispersant, and an oil-soluble initiator; raising a temperature from the starting to the end reaction temperature while metering at least ethylenically unsaturated monomers and a water-soluble initiator into a reaction vessel, conducting polymerization of the monomers in the presence of the water-soluble initiator at a temperature up to the end reaction temperature, and when the temperature has reached the end reaction temperature, conducting polymerization by the oil-soluble initiator. The oil-soluble initiator is inactive at the starting reaction temperature and becomes more active as a temperature approaches the end reaction temperature at which the oil-soluble initiator is fully active.
摘要翻译：本发明提供一种通过自由基水乳液聚合制备含水聚合物分散体的新型一步法，包括至少混合水，分散剂和油溶性引发剂; 从开始到结束的反应温度升高温度，同时至少将烯属不饱和单体和水溶性引发剂计量到反应容器中，在水溶性引发剂的存在下在最终达到最终温度下进行单体聚合反应温度，当温度达到最终反应温度时，通过油溶性引发剂进行聚合。油溶性引发剂在起始反应温度下无活性，随着温度接近油溶性引发剂完全活化的最终反应温度，其变得更有活性。

7. 发明申请

US20110100575A1 AQUEOUS SUSPENSIONS OF FINE-PARTICULATE FILLERS, METHOD FOR THE MANUFACTURE THEREOF AND USE THEREOF FOR THE MANUFACTURE OF FLUID-CONTAINING PAPERS 失效
标题翻译：细颗粒填料的水性悬浮液，其制造方法及其制造含流体纸的用途
公开(公告)号：US20110100575A1
公开(公告)日：2011-05-05
申请号：US13002351
申请日：2009-06-30
申请人： Juergen Schmidt-Thuemmes , Anton Esser , Joerg Nieberle
发明人： Juergen Schmidt-Thuemmes , Anton Esser , Joerg Nieberle
IPC分类号： D21H17/34 , C08L43/02
CPC分类号： D21H17/69 , C01P2004/62 , C09C1/021 , C09C1/42 , C09C3/10 , D21H17/10 , D21H17/36 , D21H17/37 , D21H17/55 , D21H21/10 , Y10T428/2982
摘要： Aqueous slurries of finely divided fillers which are at least partly covered by anionic latices, the slurries being obtainable by treating aqueous slurries of finely divided fillers with at least one anionic latex which comprises, incorporated in the form of polymerized units, at least one monomer comprising phosphonic and/or phosphoric acid groups, preparation of the aqueous slurries and their use as an additive to the paper stock in the production of filler-containing paper, filler-containing cardboard or filler-containing board by draining the paper stock.
摘要翻译：至少部分地由阴离子胶乳覆盖的细分散填料的水性浆料，浆料可通过用至少一种阴离子胶乳处理细分散填料的水性浆料而获得，所述阴离子胶乳包含以聚合单元形式结合的至少一种单体，所述单体包含膦酸和/或磷酸基团，水性浆料的制备以及它们在通过排出纸料而生产含填料的纸，含填料的纸板或含填料的板中作为纸料添加剂的用途。

8. 发明授权

US08637160B2 Polymer dispersions of vinylaromatic compounds and acrylate monomers prepared in the presence of seed latex and carbohydrate compounds 有权
标题翻译：在种子胶乳和碳水化合物化合物存在下制备的乙烯基芳族化合物和丙烯酸酯单体的聚合物分散体
公开(公告)号：US08637160B2
公开(公告)日：2014-01-28
申请号：US13157779
申请日：2011-06-10
申请人： Juergen Schmidt-Thuemmes , Elitsa Evstatieva , Aurelie Morel , Dirk Lawrenz , Hermann Seyffer
发明人： Juergen Schmidt-Thuemmes , Elitsa Evstatieva , Aurelie Morel , Dirk Lawrenz , Hermann Seyffer
IPC分类号： B32B23/04
CPC分类号： C08L3/02 , C09D103/02 , D21H17/28 , D21H19/54 , D21H21/52 , Y10T428/2982 , Y10T428/31906 , Y10T428/31971 , Y10T428/31993
摘要： Described are aqueous polymer dispersions and methods of making them. The polymer dispersions are obtainable by free-radically initiated emulsion polymerization of 19.9 to 80 parts by weight of vinylaromatic compounds, 19.9 to 80 parts by weight of acrylate monomers selected from C1-C10 alkyl acrylates and C1-C10 alkyl methacrylates, 0.1 to 10 parts by weight of ethylenically unsaturated acids, and 0 to 20 parts by weight of other ethylenically unsaturated monomers, wherein the emulsion polymerization is effected in an aqueous medium in the presence of free-radical initiators, seed latex and also at least one carbohydrate compound in the form of a degraded starch. The polymer dispersions are particularly useful in the manufacture of paper coating slips.
摘要翻译：描述了水性聚合物分散体及其制备方法。聚合物分散体可通过自由基引发的19.9-80重量份乙烯基芳族化合物的乳液聚合获得，19.9-80重量份选自丙烯酸C1-C10烷基酯和甲基丙烯酸C1-C10烷基酯的丙烯酸酯单体，0.1-10重量份的烯键式不饱和酸和0至20重量份的其它烯键式不饱和单体，其中乳液聚合在水性介质中在自由基引发剂，种子胶乳和至少一种碳水化合物的存在下进行，降解淀粉的形式。聚合物分散体特别可用于制造纸张涂布纸。

9. 发明授权

US08530563B2 Process for the preparation of aqueous polymer dispersions from a aromatic compound, a conjugated aliphatic diene and an ethylenically unsaturated carbonitrile 有权
标题翻译：用于由芳族化合物，共轭脂族二烯和烯属不饱和腈制备聚合物水分散体的方法
公开(公告)号：US08530563B2
公开(公告)日：2013-09-10
申请号：US13532062
申请日：2012-06-25
申请人： Elitsa Evstatieva , Juergen Schmidt-Thuemmes , Dirk Lawrenz
发明人： Elitsa Evstatieva , Juergen Schmidt-Thuemmes , Dirk Lawrenz
IPC分类号： C08K3/22 , B32B27/10
CPC分类号： C08F251/00 , C08F251/02 , C08F279/02 , C08F279/04 , C08L51/02 , C08L55/02 , C09D151/02 , C09D155/02 , Y10T428/31906 , C08L2666/02
摘要： A process for the preparation of aqueous polymer dispersions is described, a vinylaromatic compound, such as, for example, styrene, a conjugated aliphatic diene, such as, for example, butadiene, and an ethylenically unsaturated carbonitrile, such as, for example, acrylonitrile, being copolymerized in an aqueous medium. The copolymerization is effected in the presence of a degraded starch and of free radical initiators. At least part of the monomers differing from ethylenically unsaturated carbonitriles are polymerized before the ethylenically unsaturated carbonitriles are added to the polymerization mixture.
摘要翻译：描述了制备聚合物水分散体的方法，乙烯基芳族化合物，例如苯乙烯，共轭脂族二烯，例如丁二烯和烯键式不饱和腈，例如丙烯腈，在水性介质中共聚。共聚反应在降解淀粉和自由基引发剂存在下进行。不同于烯属不饱和碳原子的单体的至少一部分在将烯属不饱和碳原子加入聚合混合物之前聚合。

10. 发明授权

US08003716B2 Aqueous polymer dispersions based on copolymers formed from vinylaromatics and conjugated aliphatic dienes, processes for preparation thereof and use thereof 有权
标题翻译：基于由乙烯基芳烃和共轭脂族二烯形成的共聚物的聚合物水分散体，其制备方法和用途
公开(公告)号：US08003716B2
公开(公告)日：2011-08-23
申请号：US12679678
申请日：2008-10-06
申请人： Elitsa Evstatieva , Juergen Schmidt-Thuemmes , Dirk Lawrenz , Johannes Jan-Bessel Minderhoud , Guillermo Arens
发明人： Elitsa Evstatieva , Juergen Schmidt-Thuemmes , Dirk Lawrenz , Johannes Jan-Bessel Minderhoud , Guillermo Arens
IPC分类号： C08F251/02 , C08F2/22 , C08L51/02
CPC分类号： C08F251/02 , C08F2/24 , C08F212/08 , C08F220/06 , C08F222/02 , C08F236/10 , C08L3/02 , C08L51/02 , C09D125/14 , C09D151/02 , C09J125/14 , D21H19/44 , D21H19/54 , D21H19/56 , D21H19/60 , C08L2666/02
摘要： Aqueous polymer dispersions based on copolymers of vinyl aromatics and conjugated aliphatic dienes having a mean particle size of from 80 to 150 nm, obtained by free radical emulsion copolymerization of (a) from 19.9 to 80 parts by weight of at least one vinyl aromatic compound, (b) from 19.9 to 80 parts by weight of at least one conjugated aliphatic diene, (c) from 0.1 to 10 parts by weight of at least one ethylenically unsaturated acid, and (d) from 0 to 20 parts by weight of at least one other monoethylenically Unsaturated monomer, the sum of the parts by weight of the monomers (a), (b), (c) and (d) always being 100, in an aqueous medium in the presence of at least one degraded starch having an intrinsic viscosity ηi of less than 0.07 dl/g with the use of at least 0.9% by weight, based on the monomers used altogether, of initiators selected from peroxodisulfates, peroxosulfates, azo initiators, organic peroxides, organic hydroperoxides and hydrogen peroxide, at least 30% by weight of the initiators being initially taken together with the degraded starch in the aqueous medium and the monomers and the remaining initiators being metered into this initially taken mixture under polymerization conditions.
摘要翻译：基于乙烯基芳族化合物和平均粒径为80-150nm的共轭脂族二烯的共聚物的水性聚合物分散体，其通过（a）从19.9至80重量份的至少一种乙烯基芳族化合物的自由基乳液共聚获得，（b）19.9至80重量份的至少一种共轭脂族二烯，（c）0.1至10重量份的至少一种烯属不饱和酸，和（d）0至20重量份至少一种其它单烯属不饱和单体，在含有至少一种降解淀粉的水性介质中，单体（a），（b），（c）和（d）的重量份数总和为100，总共为100 基于所使用的单体，选自过氧二硫酸盐，过氧化硫酸盐，偶氮引发剂，有机过氧化物，有机氢过氧化物和过氧化氢的引发剂，使用至少0.9重量％的特性粘度＆e小于0.07dl / g，至少30％以上这些引发剂最初与水性介质中的降解淀粉一起并入，并且在聚合条件下将单体和剩余的引发剂计量加入到该初始混合物中。

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