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1. 发明申请

US20120248378A1 Substituted Triazine Compositions and Methods for Producing Same 审中-公开
标题翻译：取代三嗪组合物及其制备方法
公开(公告)号：US20120248378A1
公开(公告)日：2012-10-04
申请号：US13495061
申请日：2012-06-13
申请人： Joseph F. Stieber , Venratramanan K. Madabusi , Edward L. Wheeler
发明人： Joseph F. Stieber , Venratramanan K. Madabusi , Edward L. Wheeler
IPC分类号： C09K15/30
CPC分类号： C08K5/005 , C08K5/18 , C08K5/3492 , C08L21/00
摘要： Compositions comprising substituted phenylenediamine and substituted triazine compounds, including tris-(N-alkyl-p-phenylenediamino)-1,3,5-triazines. The compositions are liquid and do not sinter during storage or transportation. The compositions are used as antiozonants for elastomer articles, including rubber articles.
摘要翻译：包含取代的苯二胺和取代的三嗪化合物的组合物，包括三 - （N-烷基 - 对苯二胺基）-1,3,5-三嗪。组合物是液体的，并且在储存或运输过程中不会烧结。该组合物用作弹性体制品的防臭剂，包括橡胶制品。

2. 发明授权

US07390928B2 Alkylation of N′-phenyl-N-alkylphenylenediamines in ionic liquid, N′-phenyl-N-alkyl (alkylphenylene) diamines produced thereby, and lubricant compositions containing same 有权
标题翻译：在离子液体中的N-苯基-N-烷基苯二胺的烷基化，由此制备的N'-苯基-N-烷基（烷基亚苯基）二胺和含有它们的润滑剂组合物
公开(公告)号：US07390928B2
公开(公告)日：2008-06-24
申请号：US11304829
申请日：2005-12-14
申请人： Steven J. Hobbs , Joseph F. Stieber
发明人： Steven J. Hobbs , Joseph F. Stieber
IPC分类号： C07C209/68 , C07C211/43 , C10M169/04
CPC分类号： C07C211/55 , C07C209/68 , C10M133/12 , C10M169/04 , C10M177/00 , C10M2215/064 , C10N2270/00
摘要： A process for alkylation of a N′-phenyl-N-alkyl-p-phenylenediamine of specified formula in an ionic liquid unexpectedly produces a N′-phenyl-N-alkyl(alkylphenylene)diamine of a second specified formula. The use of an inorganic liquid permits convenient separation of the alkylated reaction product from the reaction mixture.
摘要翻译：在离子液体中烷基化具有规定式的N'-苯基-N-烷基 - 对苯二胺的方法意外地产生第二规定的式N' - 苯基-N-烷基（烷基亚苯基）二胺。使用无机液体可方便地将烷基化反应产物与反应混合物分离。

3. 发明授权

US07361788B2 Direct alkylation of N-alkyl-N′-phenyl-p-phenylenediamine 有权
标题翻译：直接烷基化N-烷基-N'-苯基对苯二胺
公开(公告)号：US07361788B2
公开(公告)日：2008-04-22
申请号：US11339231
申请日：2006-01-24
申请人： Jin-Yun Wang , Huiling Ding , Joseph F. Stieber
发明人： Jin-Yun Wang , Huiling Ding , Joseph F. Stieber
IPC分类号： C07C211/00
CPC分类号： C07C209/68 , C07C2601/14 , C07C2601/18 , C07C211/51
摘要： A single-step process is disclosed for the ring alkylation of at least one N-alkyl-N′-phenyl-phenylenediamine with at least one olefin wherein the process comprises heating a mixture of the N-alkyl-N′-phenyl-phenylenediamine(s) and olefin(s) in the presence of a catalytic amount of at least one alkyl aluminum halide at a temperature of from about 50 to about 350° C. in a sealed vessel for from about one to about 30 hours.
摘要翻译：公开了至少一种N-烷基-N'-苯基 - 苯二胺与至少一种烯烃的环烷基化的单步方法，其中该方法包括加热N-烷基-N'-苯基 - 苯二胺（ s）和烯烃在催化量的至少一种烷基铝卤化物存在下，在约50至约350℃的温度下在密封容器中约1至约30小时。

4. 发明授权

US06245912B1 Process for making N-alkyl bis(2-pyridyl) sulfenimides 失效
标题翻译：制备N-烷基双（2-吡啶基）亚磺酰亚胺的方法
公开(公告)号：US06245912B1
公开(公告)日：2001-06-12
申请号：US09686095
申请日：2000-10-12
申请人： Joseph F. Stieber , Franklin H. Barrows
发明人： Joseph F. Stieber , Franklin H. Barrows
IPC分类号： C07D40112
CPC分类号： C07D213/70 , C07D239/38 , C07D277/36 , C07D277/80
摘要： There is disclosed a process for the preparation of sulfenimides comprising: mixing, in a hydrocarbon solvent, a sulfenamide of the formula with an aldehyde of the formula R4CHO where X is a sulfur atom, a —C═N— group, or a —C═C— group, R1 and R2 are independently selected from the group consisting of hydrogen, alkyl, and aryl or may be joined to form a saturated or unsaturated ring or aromatic ring, R3 is alkyl or cycloalkyl, and R4 is a hydrocarbon radical wherein the carbon bearing the aldehyde function is bonded only to other carbon atoms, a substituted or unsubstituted aryl ring, or a heteroaromatic ring; and heating the mixture at a temperature and for a period of time sufficient to convert the sulfenamide to the sulfenimide.
摘要翻译：公开了一种制备亚磺酰亚胺的方法，包括：在烃溶剂中混合制得的醛的亚磺酰胺，其中X是硫原子，-C = N-基或-C = C- 基团，R 1和R 2独立地选自氢，烷基和芳基，或可以连接形成饱和或不饱和的环或芳环，R 3是烷基或环烷基，R 4是烃基，其中碳醛官能团仅与其它碳原子结合，取代或未取代的芳基环或杂芳环; 并在足以将亚磺酰胺转化为亚磺酰亚胺的温度和时间内加热混合物。

5. 发明授权

US06180795B2 Process for making N-alkyl bis(thiazolyl)sulfenimides 有权
标题翻译：制备N-烷基双（噻唑基）亚磺酰亚胺的方法
公开(公告)号：US06180795B2
公开(公告)日：2001-01-30
申请号：US09365295
申请日：1999-07-30
申请人： Joseph F. Stieber , Franklin H. Barrows
发明人： Joseph F. Stieber , Franklin H. Barrows
IPC分类号： C07D41712
CPC分类号： C07D213/70 , C07D239/38 , C07D277/36 , C07D277/80
摘要： There is disclosed a process for the preparation of sulfenimides comprising: mixing, in a hydrocarbon solvent, a sulfenamide of the formula with an aldehyde of the formula R4CHO where X is a sulfur atom, a —C═N— group, or a —C═C— group, R1 and R2 are independently selected from the group consisting of hydrogen, alkyl, and aryl or may be joined to form a saturated or unsaturated ring or aromatic ring, R3 is alkyl or cycloalkyl, and R4 is a hydrocarbon radical wherein the carbon bearing the aldehyde function is bonded only to other carbon atoms, a substituted or unsubstituted aryl ring, or a heteroaromatic ring; and heating the mixture at a temperature and for a period of time sufficient to convert the sulfenamide to the sulfenimide.
摘要翻译：公开了一种制备亚磺酰亚胺的方法，包括：在烃溶剂中混合制得的醛的亚磺酰胺，其中X是硫原子，-C = N-基或-C = C- 基团，R 1和R 2独立地选自氢，烷基和芳基，或可以连接形成饱和或不饱和的环或芳环，R 3是烷基或环烷基，R 4是烃基，其中碳醛官能团仅与其它碳原子结合，取代或未取代的芳基环或杂芳环; 并在足以将亚磺酰胺转化为亚磺酰亚胺的温度和时间内加热混合物。

6. 发明申请

US20090156449A1 ALKYLATED 1,3-BENZENEDIAMINE COMPOUNDS AND METHODS FOR PRODUCING SAME 有权
标题翻译：烷基-1,3-苯二胺化合物及其生产方法
公开(公告)号：US20090156449A1
公开(公告)日：2009-06-18
申请号：US12212131
申请日：2008-09-17
申请人： Robert G. Rowland , Joseph F. Stieber , Clifford M. Pratt , Ronald D. Abbott
发明人： Robert G. Rowland , Joseph F. Stieber , Clifford M. Pratt , Ronald D. Abbott
IPC分类号： C10M133/12 , C07C211/44 , C07C209/24
CPC分类号： C10L1/223 , C07C209/24 , C07C211/51 , C09K15/18 , C09K15/30 , C10L10/00 , C10L10/04 , C10M133/12 , C10M133/40 , C10M177/00 , C10M2215/066 , C10M2215/221 , C10N2230/10 , C10N2240/04 , C10N2240/08 , C10N2240/10 , C10N2240/30 , C10N2270/00
摘要： An alkylated 1,3-benzenediamine compound used as a deposit-control lubricant additives for organic materials including lubricating oil, gasoline, and diesel fuels. The invention improves the oxidative stability of the lubricants and fuels by adding the alkylated 1,3-benzenediamine compound. The alkylated 1,3-benzenediamine compound is formed using a catalytic hydrogenation that alkylates the 4 and/or 6 position of the central aromatic ring.
摘要翻译：用作有机材料（包括润滑油，汽油和柴油）的沉积物控制润滑剂添加剂的烷基化1,3-苯二胺化合物。本发明通过加入烷基化1,3-苯二胺化合物来改善润滑剂和燃料的氧化稳定性。烷基化1,3-苯二胺化合物是通过使中心芳环的4位和/或6位烷基化的催化氢化形成的。

7. 发明授权

US07205348B2 Rubber composition and method of making same 失效
标题翻译：橡胶组合物及其制备方法
公开(公告)号：US07205348B2
公开(公告)日：2007-04-17
申请号：US10819691
申请日：2004-04-07
申请人： Joseph F. Stieber , Martin J. Hannon , L. P. Felipe Chibante , James R. Korte , Frank E. Welsh
发明人： Joseph F. Stieber , Martin J. Hannon , L. P. Felipe Chibante , James R. Korte , Frank E. Welsh
IPC分类号： A61K8/81
CPC分类号： C08K5/38 , C08K9/04 , C08L21/00
摘要： Process of producing unvulcanized rubber useful for producing vulcanized rubber with improved hysteresis, which comprises mixing a composition comprising unvulcanized rubber, carbon black and xanthogen polysulfide at an elevated temperature in a non-productive stage and composition suitable for producing unvulcanized rubber useful for producing vulcanized rubber with improved hysteresis, which comprises unvulcanized rubber, a filler comprising carbon black and xanthogen polysulfide.
摘要翻译：生产具有改善滞后性的硫化橡胶的未硫化橡胶的生产方法，其包括将非硫化橡胶，炭黑和黄原子多硫化物的组合物在非生产阶段和升高的温度下混合并适用于制备用于生产硫化橡胶的未硫化橡胶的组合物具有改善的滞后，其包括未硫化橡胶，包含炭黑和黄原酸多硫化物的填料。

8. 发明授权

US06906121B2 4-nitrosodiphenylamine derivatives and their use as coupling agents for filled rubber compounds 失效
标题翻译： 4-亚硝基二苯胺衍生物及其作为填充橡胶化合物的偶联剂的用途
公开(公告)号：US06906121B2
公开(公告)日：2005-06-14
申请号：US10395591
申请日：2003-03-24
申请人： Joseph F. Stieber , Franklin H. Barrows
发明人： Joseph F. Stieber , Franklin H. Barrows
IPC分类号： B60C1/00 , C07D251/34 , C08K5/33 , C08K5/34 , C08K5/32
CPC分类号： C07C251/68 , B60C1/0016 , C07C251/66 , C07C2601/16 , C07D251/34 , C08K5/33 , C08L21/00
摘要： A composition of matter is disclosed that comprises a compound of the formula AnR, wherein: A is R1 is hydrocarbyl; m is 0 or 1; n is 1, 2, or 3; R is selected from the group consisting of: mono-, di-, and trivalent aliphatic groups; mono-, di-, and trivalent aromatic groups; five- and six-membered heterocyclic rings comprising n carbon atoms bonded to A, at least one nitrogen atom, and, optionally, at least one sulfur atom; and wherein R2 and R3 are independently selected from the group consisting of hydrogen and hydrocarbyl. These compounds are useful as coupling agents in filled elastomer compositions.
摘要翻译：公开了一种物质组合物，其包含式A N n R的化合物，其中：A为R 1为烃基; m为0或1; n为1,2或3; R选自：单 - ，二 - 和三价脂族基团; 单，二和三价芳基; 包含与A键合的n个碳原子，至少一个氮原子和任选地至少一个硫原子的五元和六元杂环; 并且其中R 2和R 3独立地选自氢和烃基。这些化合物可用作填充弹性体组合物中的偶联剂。

9. 发明授权

US08563489B2 Alkylated 1,3-benzenediamine compounds and methods for producing same 有权
标题翻译：烷基化1,3-苯二胺化合物及其制备方法
公开(公告)号：US08563489B2
公开(公告)日：2013-10-22
申请号：US12212131
申请日：2008-09-17
申请人： Robert G. Rowland , Joseph F. Stieber , Clifford M. Pratt , Ronald D. Abbott
发明人： Robert G. Rowland , Joseph F. Stieber , Clifford M. Pratt , Ronald D. Abbott
IPC分类号： C10M133/12
CPC分类号： C10L1/223 , C07C209/24 , C07C211/51 , C09K15/18 , C09K15/30 , C10L10/00 , C10L10/04 , C10M133/12 , C10M133/40 , C10M177/00 , C10M2215/066 , C10M2215/221 , C10N2230/10 , C10N2240/04 , C10N2240/08 , C10N2240/10 , C10N2240/30 , C10N2270/00
摘要： An alkylated 1,3-benzenediamine compound used as a deposit-control lubricant additives for organic materials including lubricating oil, gasoline, and diesel fuels. The invention improves the oxidative stability of the lubricants and fuels by adding the alkylated 1,3-benzenediamine compound. The alkylated 1,3-benzenediamine compound is formed using a catalytic hydrogenation that alkylates the 4 and/or 6 position of the central aromatic ring.
摘要翻译：用作有机材料（包括润滑油，汽油和柴油）的沉积物控制润滑剂添加剂的烷基化1,3-苯二胺化合物。本发明通过加入烷基化1,3-苯二胺化合物来改善润滑剂和燃料的氧化稳定性。烷基化1,3-苯二胺化合物是通过使中心芳环的4位和/或6位烷基化的催化氢化形成的。

10. 发明授权

US07563929B2 Alkylation of N′-phenyl-N-alkylphenylenediamines in ionic liquid and N′-phenyl-N-alkyl(alkylphenylene) diamines produced thereby 有权
标题翻译：由此产生的N-苯基-N-烷基苯二胺在离子液体中的烷基化和由此产生的N'-苯基-N-烷基（烷基亚苯基）二胺
公开(公告)号：US07563929B2
公开(公告)日：2009-07-21
申请号：US12103835
申请日：2008-04-16
申请人： Steven J. Hobbs , Joseph F. Stieber
发明人： Steven J. Hobbs , Joseph F. Stieber
IPC分类号： C07C209/68
CPC分类号： C07C211/55 , C07C209/68 , C10M133/12 , C10M169/04 , C10M177/00 , C10M2215/064 , C10N2270/00
摘要： A process for alkylation of a N′-phenyl-N-alkyl-p-phenylenediamine of specified formula in an ionic liquid unexpectedly produces a N′-phenyl-N-alkyl(alkylphenylene)diamine of a second specified formula. The use of an inorganic liquid permits convenient separation of the alkylated reaction product from the reaction mixture.
摘要翻译：在离子液体中烷基化具有规定式的N'-苯基-N-烷基 - 对苯二胺的方法意外地产生具有第二规定式的N'-苯基-N-烷基（烷基亚苯基）二胺。使用无机液体可方便地将烷基化反应产物与反应混合物分离。

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