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1. 发明授权

US6036733A Process for the preparation of crystalline sodium silicates 失效
标题翻译：制备结晶硅酸钠的方法
公开(公告)号：US6036733A
公开(公告)日：2000-03-14
申请号：US027531
申请日：1998-02-23
申请人： Josef Holz , Gunther Schimmel , Alexander Tapper , Volker Thewes
发明人： Josef Holz , Gunther Schimmel , Alexander Tapper , Volker Thewes
IPC分类号： C01B33/32 , C01B33/38 , C11D3/08 , C11D3/12 , B01D9/00 , C01B33/00 , C01B33/20 , C01D1/30
CPC分类号： C11D3/1273 , C01B33/38
摘要： The invention relates to a process for the preparation of crystalline sodium silicates having a sheet structure and high .delta. phase content from water glass, which has been prepared predominantly hydrothermally, by dehydration of the water glass and subsequent crystallization at elevated temperature, wherein the water glass is a mixture of water glass prepared hydrothermally and tank furnace water glass, and also to its use.
摘要翻译：本发明涉及通过水玻璃的脱水和随后的高温结晶，制备具有主要水热制备的片状结构和高δ相含量的结晶硅酸钠的方法，其中水玻璃是水热玻璃和水箱玻璃水玻璃的混合物，也是它的用途。

2. 发明授权

US6099595A Process for the preparation of crystalline sodium silicates 失效
标题翻译：制备结晶硅酸钠的方法
公开(公告)号：US6099595A
公开(公告)日：2000-08-08
申请号：US27891
申请日：1998-02-23
申请人： Josef Holz , Gunther Schimmel , Alexander Tapper , Volker Thewes
发明人： Josef Holz , Gunther Schimmel , Alexander Tapper , Volker Thewes
IPC分类号： C01B33/32 , C01B33/38 , C11D3/08 , C11D3/12 , B01D9/00 , C01D1/30 , C01D33/00 , C01D33/20 , C01D33/32
CPC分类号： C01B33/38 , C11D3/1273
摘要： The invention relates to a process for the preparation of crystalline sodium silicates having a sheet structure and high .delta. phase content from water glass, which has been prepared hydrothermally, by dehydration of the water glass and subsequent crystallization at elevated temperature, which comprises treating the water glass at temperatures of from 50 to 140.degree. C. prior to dehydration.
摘要翻译：本发明涉及一种通过水玻璃脱水并随后在升高的温度下结晶而制备具有水玻璃的片状结构和高δ相含量的结晶硅酸钠的方法，该方法包括处理水在脱水之前的温度为50至140℃的玻璃。

3. 发明授权

US07256169B2 Pulverulent laundry and cleaning detergent ingredient consisting of polycarbosylate and silicate 失效
标题翻译：由多碳酸盐和硅酸盐组成的粉状衣物和清洁剂
公开(公告)号：US07256169B2
公开(公告)日：2007-08-14
申请号：US08994479
申请日：2001-01-30
申请人： Günther Schimmel , Harald Bauer , Josef Holz , Volker Thewes , Richard Mertens , Peter Hardt , Matthias Berghahn , Thomas Müller
发明人： Günther Schimmel , Harald Bauer , Josef Holz , Volker Thewes , Richard Mertens , Peter Hardt , Matthias Berghahn , Thomas Müller
IPC分类号： C11D3/08 , C11D3/37
CPC分类号： C11D3/3761 , C11D3/08 , C11D3/1273 , C11D3/3788 , C11D11/0088
摘要： The invention relates to a pulverulent laundry and cleaning detergents ingredient, to a process for its preparation and to its use.
摘要翻译：本发明涉及一种粉状衣物和清洁洗涤剂成分，涉及其制备方法及其用途。

4. 发明授权

US06387869B2 Granular surfactant composition of improved flowability compromising sodium silicate and linear alkylbenzenesulfonates 失效
标题翻译：颗粒表面活性剂组合物改善流动性，从而影响硅酸钠和直链烷基苯磺酸盐
公开(公告)号：US06387869B2
公开(公告)日：2002-05-14
申请号：US09822977
申请日：2001-03-30
申请人： Harald Bauer , Josef Holz , Gunther Schimmel
发明人： Harald Bauer , Josef Holz , Gunther Schimmel
IPC分类号： C11D1310
CPC分类号： C11D3/08 , C11D1/22 , C11D3/126
摘要： A granular surfactant composition comprising sodium silicate and linear alkylbenzenesulfonates, wherein the granular surfactant composition has a mean particle diameter of ≧50 &mgr;m and an ffc value of ≧7; a process for the preparation of this granular surfactant composition, its use, and detergents and cleaners which comprise such granular surfactant composition and a process for the making of the same; and, where appropriate, the granular surfactant composition comprises other active ingredients and auxiliaries.
摘要翻译：一种包含硅酸钠和直链烷基苯磺酸盐的颗粒状表面活性剂组合物，其中颗粒状表面活性剂组合物的平均粒径>50μm，ffc值> 7。制备这种颗粒状表面活性剂组合物的方法，其用途和包含这种颗粒状表面活性剂组合物的洗涤剂和清洁剂及其制备方法; 并且在适当的情况下，颗粒表面活性剂组合物包含其它活性成分和助剂。

5. 发明授权

US06743766B1 Sparingly soluble alkali metal silicate 失效
标题翻译：微溶性碱金属硅酸盐
公开(公告)号：US06743766B1
公开(公告)日：2004-06-01
申请号：US09659394
申请日：2000-09-11
申请人： Harald Bauer , Josef Holz , Guenther Schimmel , Alexander Tapper
发明人： Harald Bauer , Josef Holz , Guenther Schimmel , Alexander Tapper
IPC分类号： C11D308
CPC分类号： C01B33/32 , C11D3/1273
摘要： The invention relates to a sparingly soluble alkali metal silicate which comprises alkali metal phyllosilicate in finely divided form in a non-phyllosilicatic alkali metal silicate environment of the formula x MI2O.y SiO2, in which MI is an alkali metal and y/x (1.9 to 500): 1; a process for its preparation and its use in detergents and cleaners.
摘要翻译：本发明涉及一种微溶的碱金属硅酸盐，其在细粉状形式的碱金属页硅酸盐在式（M 2）SiO 2的非页硅酸碱金属硅酸盐环境中，其中M是碱金属和y / x（1.9〜500）：1; 其制备方法及其在洗涤剂和清洁剂中的应用。

6. 发明授权

US5147625A Process for the preparation of phosphorous acid 失效
标题翻译：制备磷酸的方法
公开(公告)号：US5147625A
公开(公告)日：1992-09-15
申请号：US739873
申请日：1991-08-02
申请人： Alexander Tapper , Horst Buhl , Josef Holz
发明人： Alexander Tapper , Horst Buhl , Josef Holz
IPC分类号： C01B7/03 , C01B25/163
CPC分类号： C01B7/035 , C01B25/163
摘要： In a continuous process for the preparation of phosphorous acid with simultaneous production of hydrochloric acid, a reaction zone is provided which is in open communication with a first scrubbing zone. A portion of the reaction product is recycled from the bottom of the reaction zone into the top of the scrubbing zone and phosphorous acid is removed from the circulation. Hydrogen chloride gas escaping from the top of the first scrubbing zone is brought into contact, in a cooled, second scrubbing zone, with an overstoichiometric amount of water. Hydrochloric acid is obtained which is passed as starting material into the reaction zone or into the top of the first scrubbing zone. The external cooling of the second scrubbing zone is controlled such that the temperature in the reaction zone is kept constant at a desired value between 90.degree. and 130.degree. C. without adding any external cooling or heating energy. Pure hydrochloric acid is recovered in an absorption zone.
摘要翻译：在以同时生产盐酸制备亚磷酸的连续方法中，提供了与第一洗涤区开放连通的反应区。反应产物的一部分从反应区的底部再循环到洗涤区的顶部，并且从循环中除去亚磷酸。从第一洗涤区的顶部排出的氯化氢气体在冷却的第二洗涤区中与化学计量的水接触。得到的盐酸作为原料进入反应区或进入第一洗涤区的顶部。控制第二洗涤区的外部冷却，使得反应区中的温度保持恒定在90℃至130℃之间的期望值，而不增加任何外部冷却或加热能量。在吸收区中回收纯盐酸。

7. 发明授权

US06908896B2 Builder composition prepared by heat-treating a crystalline layered Na silicate 失效
标题翻译：通过热处理结晶层状硅酸钠制备的生成器组合物
公开(公告)号：US06908896B2
公开(公告)日：2005-06-21
申请号：US10123796
申请日：2002-04-16
申请人： Harald Bauer , Josef Holz , Günther Schimmel
发明人： Harald Bauer , Josef Holz , Günther Schimmel
IPC分类号： C11D3/08 , C11D3/12
CPC分类号： C11D3/1273
摘要： The invention relates to builder compositions with improved dissolution residue behavior, obtained by bringing a) crystalline layered sodium silicate of the formula NaMSixO2x+1*yH2O, where M is sodium or hydrogen, x is a number from 1.9 to 4 and y is a number from 0 to 20, and b) water or an aqueous solution or dispersion of at least one detergent ingredient, c) where the molar ratio of component a) to the water from component b) is 0.5:1 to 20:1, into contact with one another and subsequently heat-treating the resulting builder composition at 30 to 400° C. for 0.5 to 1000 min.
摘要翻译：本发明涉及具有改进的溶解残留行为的助洗剂组合物，其通过使a）结晶层状硅酸钠由式NaMSi x O 2 x + 1 * y H 2 其中M为钠或氢，x为1.9至4的数，y为0至20的数，b）水或至少一种洗涤剂成分的水溶液或分散体，c）其中组分a）与组分b）的水的摩尔比为0.5:1至20:1，彼此接触，随后在30至400℃下热处理所得助洗剂组合物0.5至1000分钟。

8. 发明授权

US06506722B1 Cogranulates comprising alkali metal phyllosilicates and disintegrants 失效
标题翻译：包含碱金属页硅酸盐和崩解剂的Cogranulates
公开(公告)号：US06506722B1
公开(公告)日：2003-01-14
申请号：US09659386
申请日：2000-09-11
申请人： Harald Bauer , Josef Holz , Guenther Schimmel , Armelle Pelissou
发明人： Harald Bauer , Josef Holz , Guenther Schimmel , Armelle Pelissou
IPC分类号： C11D308
CPC分类号： C11D3/1273 , C11D3/222 , C11D17/0073 , C11D17/06
摘要： The invention relates to cogranulates comprising phyllosilicates and disintegrants, in particular cellulose, and to detergents and cleaners which comprise these cogranulates, preferably in tablet form.
摘要翻译：本发明涉及包含页硅酸盐和崩解剂，特别是纤维素的组合物，以及包含这些cogranulates，优选片剂形式的洗涤剂和清洁剂。

9. 发明授权

US4483837A Process for making calciummonohydrogen phosphate dihydrate 失效
标题翻译：磷酸二氢钙二水合物的制备方法
公开(公告)号：US4483837A
公开(公告)日：1984-11-20
申请号：US507784
申请日：1983-06-24
申请人： Josef Cremer , Josef Holz , Hans Haas , Friedrich Schulte
发明人： Josef Cremer , Josef Holz , Hans Haas , Friedrich Schulte
IPC分类号： C01B25/32 , C01B15/16 , C01B25/26
CPC分类号： C01B25/322
摘要： The disclosure relates to a process for making calciummonohydrogen phosphate dihydrate with a high degree of whiteness from pure phosphoric acid and naturally occurring calcium carbonates. More particularly, a fine-particulate calcium carbonate is suspended in water and the suspension is mixed at temperatures between 0.degree. and 60.degree. C. with phosphoric acid so as to establish a Ca/P-ratio of 0.20 up to 0.57. The phosphoric acid is added in quantities per unit time preventing the resulting mixture from foaming over. Next, solid matter constituents are separated from the mixture, after CO.sub.2 has ceased to evolve, with the resultant formation of a clear colorless acid solution. This solution and an aqueous suspension or solution of pure alkali metal and/or alkaline earth metal carbonates and/or hydroxides, are jointly introduced into a reaction zone at a reaction temperature of 20.degree. to 45.degree. C. so as to establish a pH-value initially of 2.0 to 5.0 and then, towards the end of the reaction of 6.0 to 8.0. Finally, the reaction product is filtered off, washed out, and dried in known fashion.
摘要翻译：本公开涉及一种从纯磷酸和天然存在的碳酸钙制备具有高白度的磷酸氢钙二水合物的方法。更具体地，将细颗粒碳酸钙悬浮在水中，并将悬浮液在0℃至60℃的温度下与磷酸混合，以便确定0.20至0.57的Ca / P比。每单位时间内加入磷酸，防止所得混合物发泡。接下来，在CO 2停止放出之后，固体成分与混合物分离，形成澄清的无色酸溶液。将该溶液和纯碱金属和/或碱土金属碳酸盐和/或氢氧化物的水性悬浮液或溶液在20〜45℃的反应温度下共同引入反应区，以建立pH- 值最初为2.0〜5.0，然后在6.0〜8.0的反应结束。最后，将反应产物滤出，洗涤并以已知方式干燥。

10. 发明授权

US06844310B2 Process of preparing a crystalline sodium silicate builder composition 失效
标题翻译：制备结晶硅酸钠助洗剂组合物的方法
公开(公告)号：US06844310B2
公开(公告)日：2005-01-18
申请号：US10039480
申请日：2001-11-09
申请人： Harald Bauer , Josef Holz , Günther Schimmel
发明人： Harald Bauer , Josef Holz , Günther Schimmel
IPC分类号： C11D3/08 , C11D3/02 , C11D3/12 , C11D3/20 , C11D3/36 , C11D3/37 , C11D3/395 , C11D3/40 , C11D7/08 , C11D17/00 , C11D17/06 , C11D7/14
CPC分类号： C11D17/0073 , C11D3/042 , C11D3/1273 , C11D3/2075 , C11D3/361 , C11D3/364 , C11D3/3761 , C11D3/378
摘要： The invention relates to builder compositions obtainable by bringing a) crystalline sheetlike sodium silicate of the formula NaMSixO2x+1.yH2O, where M is sodium or hydrogen, x is a number from 1.9 to 4 and y is a number from 0 to 20. b) water and c) an acidic, H+-releasing component, where the d) molar ratio of the crystalline sheetlike sodium silicate a) to the total amount of the releasable H+ of the acid component c) is 4:1 to 1000:1 and the e) molar ratio of the water b) to the total amount of the releasable H+ of the acidic component c) is 3:1 to 1000:1. into contact with one another. The invention also relates to laundry detergents, cleaners, compounds and water softeners comprising the builder compositions according to the invention.
摘要翻译：本发明涉及通过使式NaMSixO 2 x + 1·yH 2 O的结晶片状硅酸钠得到的助洗剂组合物，其中M为钠或氢，x为数为1.9至4，y为0至20.b的数）水和c）酸性H +释放组分，其中结晶片状硅酸钠a）的d）摩尔比与酸组分c）的可释放H +的总量为4:1至1000 ：1和ee）水分b）与酸性组分c）的可释放H +的总量的摩尔比为3:1-1000:1，彼此接触。本发明还涉及洗衣洗涤剂，清洁剂，化合物和软水剂，其包含根据本发明的助洗剂组合物。

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