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1. 发明授权

US06908896B2 Builder composition prepared by heat-treating a crystalline layered Na silicate 失效
标题翻译：通过热处理结晶层状硅酸钠制备的生成器组合物
公开(公告)号：US06908896B2
公开(公告)日：2005-06-21
申请号：US10123796
申请日：2002-04-16
申请人： Harald Bauer , Josef Holz , Günther Schimmel
发明人： Harald Bauer , Josef Holz , Günther Schimmel
IPC分类号： C11D3/08 , C11D3/12
CPC分类号： C11D3/1273
摘要： The invention relates to builder compositions with improved dissolution residue behavior, obtained by bringing a) crystalline layered sodium silicate of the formula NaMSixO2x+1*yH2O, where M is sodium or hydrogen, x is a number from 1.9 to 4 and y is a number from 0 to 20, and b) water or an aqueous solution or dispersion of at least one detergent ingredient, c) where the molar ratio of component a) to the water from component b) is 0.5:1 to 20:1, into contact with one another and subsequently heat-treating the resulting builder composition at 30 to 400° C. for 0.5 to 1000 min.
摘要翻译：本发明涉及具有改进的溶解残留行为的助洗剂组合物，其通过使a）结晶层状硅酸钠由式NaMSi x O 2 x + 1 * y H 2 其中M为钠或氢，x为1.9至4的数，y为0至20的数，b）水或至少一种洗涤剂成分的水溶液或分散体，c）其中组分a）与组分b）的水的摩尔比为0.5:1至20:1，彼此接触，随后在30至400℃下热处理所得助洗剂组合物0.5至1000分钟。

2. 发明授权

US06506722B1 Cogranulates comprising alkali metal phyllosilicates and disintegrants 失效
标题翻译：包含碱金属页硅酸盐和崩解剂的Cogranulates
公开(公告)号：US06506722B1
公开(公告)日：2003-01-14
申请号：US09659386
申请日：2000-09-11
申请人： Harald Bauer , Josef Holz , Guenther Schimmel , Armelle Pelissou
发明人： Harald Bauer , Josef Holz , Guenther Schimmel , Armelle Pelissou
IPC分类号： C11D308
CPC分类号： C11D3/1273 , C11D3/222 , C11D17/0073 , C11D17/06
摘要： The invention relates to cogranulates comprising phyllosilicates and disintegrants, in particular cellulose, and to detergents and cleaners which comprise these cogranulates, preferably in tablet form.
摘要翻译：本发明涉及包含页硅酸盐和崩解剂，特别是纤维素的组合物，以及包含这些cogranulates，优选片剂形式的洗涤剂和清洁剂。

3. 发明授权

US4483837A Process for making calciummonohydrogen phosphate dihydrate 失效
标题翻译：磷酸二氢钙二水合物的制备方法
公开(公告)号：US4483837A
公开(公告)日：1984-11-20
申请号：US507784
申请日：1983-06-24
申请人： Josef Cremer , Josef Holz , Hans Haas , Friedrich Schulte
发明人： Josef Cremer , Josef Holz , Hans Haas , Friedrich Schulte
IPC分类号： C01B25/32 , C01B15/16 , C01B25/26
CPC分类号： C01B25/322
摘要： The disclosure relates to a process for making calciummonohydrogen phosphate dihydrate with a high degree of whiteness from pure phosphoric acid and naturally occurring calcium carbonates. More particularly, a fine-particulate calcium carbonate is suspended in water and the suspension is mixed at temperatures between 0.degree. and 60.degree. C. with phosphoric acid so as to establish a Ca/P-ratio of 0.20 up to 0.57. The phosphoric acid is added in quantities per unit time preventing the resulting mixture from foaming over. Next, solid matter constituents are separated from the mixture, after CO.sub.2 has ceased to evolve, with the resultant formation of a clear colorless acid solution. This solution and an aqueous suspension or solution of pure alkali metal and/or alkaline earth metal carbonates and/or hydroxides, are jointly introduced into a reaction zone at a reaction temperature of 20.degree. to 45.degree. C. so as to establish a pH-value initially of 2.0 to 5.0 and then, towards the end of the reaction of 6.0 to 8.0. Finally, the reaction product is filtered off, washed out, and dried in known fashion.
摘要翻译：本公开涉及一种从纯磷酸和天然存在的碳酸钙制备具有高白度的磷酸氢钙二水合物的方法。更具体地，将细颗粒碳酸钙悬浮在水中，并将悬浮液在0℃至60℃的温度下与磷酸混合，以便确定0.20至0.57的Ca / P比。每单位时间内加入磷酸，防止所得混合物发泡。接下来，在CO 2停止放出之后，固体成分与混合物分离，形成澄清的无色酸溶液。将该溶液和纯碱金属和/或碱土金属碳酸盐和/或氢氧化物的水性悬浮液或溶液在20〜45℃的反应温度下共同引入反应区，以建立pH- 值最初为2.0〜5.0，然后在6.0〜8.0的反应结束。最后，将反应产物滤出，洗涤并以已知方式干燥。

4. 发明授权

US06462006B1 Solid machine dishwashing detergent with phosphate and crystalline lamellar silicates 有权
标题翻译：具有磷酸盐和晶体层状硅酸盐的固体洗碗碟洗涤剂
公开(公告)号：US06462006B1
公开(公告)日：2002-10-08
申请号：US09674154
申请日：2000-12-22
申请人： Rainer Sorg , Christian Nitsch , Juergen Haerer , Harald Volk , Thomas Mueller-Kirschbaum , Peter Krings , Harald Bauer , Josef Holz , Guenther Schimmel , Lothar Westermann
发明人： Rainer Sorg , Christian Nitsch , Juergen Haerer , Harald Volk , Thomas Mueller-Kirschbaum , Peter Krings , Harald Bauer , Josef Holz , Guenther Schimmel , Lothar Westermann
IPC分类号： C11D306
CPC分类号： C11D7/265 , C11D3/06 , C11D3/1273 , C11D3/2082 , C11D7/14 , C11D7/16 , C11D17/0073
摘要： A solid-form dishwasher detergent that contains a builder combination of conventional phosphates and crystalline layer silicates. Despite its phosphate content, the detergent provides improved protection to sensitive tableware, more particularly glasses and decorated tableware, and improved cleaning performance.
摘要翻译：一种固体形式的洗碗机洗涤剂，其包含常规磷酸盐和结晶层硅酸盐的助洗剂组合。尽管它的磷酸盐含量，洗涤剂提供了更好的保护敏感的餐具，更特别是眼镜和装饰的餐具，以及改进的清洁性能。

5. 发明授权

US06387869B2 Granular surfactant composition of improved flowability compromising sodium silicate and linear alkylbenzenesulfonates 失效
标题翻译：颗粒表面活性剂组合物改善流动性，从而影响硅酸钠和直链烷基苯磺酸盐
公开(公告)号：US06387869B2
公开(公告)日：2002-05-14
申请号：US09822977
申请日：2001-03-30
申请人： Harald Bauer , Josef Holz , Gunther Schimmel
发明人： Harald Bauer , Josef Holz , Gunther Schimmel
IPC分类号： C11D1310
CPC分类号： C11D3/08 , C11D1/22 , C11D3/126
摘要： A granular surfactant composition comprising sodium silicate and linear alkylbenzenesulfonates, wherein the granular surfactant composition has a mean particle diameter of ≧50 &mgr;m and an ffc value of ≧7; a process for the preparation of this granular surfactant composition, its use, and detergents and cleaners which comprise such granular surfactant composition and a process for the making of the same; and, where appropriate, the granular surfactant composition comprises other active ingredients and auxiliaries.
摘要翻译：一种包含硅酸钠和直链烷基苯磺酸盐的颗粒状表面活性剂组合物，其中颗粒状表面活性剂组合物的平均粒径>50μm，ffc值> 7。制备这种颗粒状表面活性剂组合物的方法，其用途和包含这种颗粒状表面活性剂组合物的洗涤剂和清洁剂及其制备方法; 并且在适当的情况下，颗粒表面活性剂组合物包含其它活性成分和助剂。

6. 发明授权

US06372709B1 Finely divided crystalline sodium disilicate 失效
标题翻译：细分二晶硅酸钠
公开(公告)号：US06372709B1
公开(公告)日：2002-04-16
申请号：US09346427
申请日：1999-07-01
申请人： Harald Bauer , Josef Holz , Günther Schimmel
发明人： Harald Bauer , Josef Holz , Günther Schimmel
IPC分类号： C11D714
CPC分类号： C11D3/2086 , C01B33/38 , C11D3/1273 , C11D3/128 , C11D3/225
摘要： The invention relates to a finely divided crystalline layered sodium disilicate of the formula NaMSixO2x+1.yH2O, where M is sodium or hydrogen, x is a number from 1.9 to 4, and y is a number from 0 to 20, which comprises from 0 to 40% by weight of alpha-disodium disilicate from 0 to 40% by weight of beta-disodium disilicate from 40 to 100% by weight of delta-disodium disilicate from 0 to 40% by weight of amorphous components, to a process for its preparation and to its use.
摘要翻译：本发明涉及式NaMSixO2x + 1.yH2O的细碎结晶层状二硅酸钠，其中M为钠或氢，x为数为1.9至4，y为0至20的数，其包含0至 40重量％的二硅酸二钠二钠从0至40重量％的二硅酸β-二钠从40至100重量％的二硅酸三钠 - 二钠，0至40重量％的无定形组分，其制备方法及其制备方法使用。

7. 发明授权

US5024825A Process for the preparation of dicalcium phosphate 失效
标题翻译：磷酸二钙的制备方法
公开(公告)号：US5024825A
公开(公告)日：1991-06-18
申请号：US521737
申请日：1990-05-10
申请人： Horst Buhl , Josef Holz , Franz-Josef Dany
发明人： Horst Buhl , Josef Holz , Franz-Josef Dany
IPC分类号： C01B25/32
CPC分类号： C01B25/322
摘要： For the preparation of dicalcium phosphate dihydrate stabilized with dimagnesium phosphate trihydrate and sodium pyrophosphate, an aqueous suspension of calcium carbonate is introduced into a reactor and recirculated by pumping through a high-speed mixer at 3,500 to 8,000 rpm which is in flow connection with the lower and upper portion of the reactor. Into the mixer an amount of phosphoric acid is introduced which is at least sufficient for the quantitative formation of dicalcium phosphate dihydrate and then an oxygen-containing magnesium compound is introduced into the reactor. Finally, lime milk is metered into the reactor up to a maximum pH of 6.9, before the sodium pyrophosphate is added to the reactor. The resulting suspension which has a stabilized dicalcium phosphate dihydrate content of 20 to 33% by weight is spray-dried.An apparatus for carrying out the process comprises besides a stirred reactor 1 two stirrer-equipped slurry containers (6, 7) and an intermediate container 16 from which a line 17 leads into a spray tower 18 where it ends above an atomizer wheel 19. The spray tower 18 is also the end point for hot air lines 20 and is in flow connection with a filter 22. The bottom of filter 22 is the starting point for a product line 24 via which highly adsorbent dicalcium phosphate dihydrate can be withdrawn.
摘要翻译：为了制备用磷酸三氢镁和焦磷酸钠稳定的磷酸二钙二水合物，将碳酸钙的水性悬浮液引入反应器中，并通过泵送通过高速混合器以3,500至8,000rpm再循环，该高速混合器与下部流动相连和反应器的上部。向混合器中加入一定量的磷酸，其至少足以定量形成磷酸二钙二水合物，然后将含氧的镁化合物引入反应器中。最后，在将焦磷酸钠加入到反应器中之前，将石灰乳计量加入反应器直至最高pH为6.9。所得到的具有稳定的磷酸二钙二水合物含量为20至33重量％的悬浮液被喷雾干燥。用于进行该方法的装置除了具有搅拌反应器1的两个装有搅拌器的浆料容器（6,7）和中间容器16之外，其中管线17从该搅拌反应器引入喷雾塔18，在该喷雾塔18中它结束在雾化器轮19的上方。喷雾塔18也是热空气管线20的终点，并且与过滤器22流动连接。过滤器22的底部是产物线24的起始点，通过该产物线24可以抽出高吸附性磷酸二钙二水合物。

8. 发明授权

US1869197A Instrument for removing corns and callosities without danger 失效
标题翻译：无危险的玉米和cal的仪器
公开(公告)号：US1869197A
公开(公告)日：1932-07-26
申请号：US41047629
申请日：1929-11-29
申请人： JOSEF HOLZ
发明人： JOSEF HOLZ
IPC分类号： A61B17/54
CPC分类号： A61B17/54 , Y10T407/1956 , Y10T407/1964

9. 发明授权

US06844310B2 Process of preparing a crystalline sodium silicate builder composition 失效
标题翻译：制备结晶硅酸钠助洗剂组合物的方法
公开(公告)号：US06844310B2
公开(公告)日：2005-01-18
申请号：US10039480
申请日：2001-11-09
申请人： Harald Bauer , Josef Holz , Günther Schimmel
发明人： Harald Bauer , Josef Holz , Günther Schimmel
IPC分类号： C11D3/08 , C11D3/02 , C11D3/12 , C11D3/20 , C11D3/36 , C11D3/37 , C11D3/395 , C11D3/40 , C11D7/08 , C11D17/00 , C11D17/06 , C11D7/14
CPC分类号： C11D17/0073 , C11D3/042 , C11D3/1273 , C11D3/2075 , C11D3/361 , C11D3/364 , C11D3/3761 , C11D3/378
摘要： The invention relates to builder compositions obtainable by bringing a) crystalline sheetlike sodium silicate of the formula NaMSixO2x+1.yH2O, where M is sodium or hydrogen, x is a number from 1.9 to 4 and y is a number from 0 to 20. b) water and c) an acidic, H+-releasing component, where the d) molar ratio of the crystalline sheetlike sodium silicate a) to the total amount of the releasable H+ of the acid component c) is 4:1 to 1000:1 and the e) molar ratio of the water b) to the total amount of the releasable H+ of the acidic component c) is 3:1 to 1000:1. into contact with one another. The invention also relates to laundry detergents, cleaners, compounds and water softeners comprising the builder compositions according to the invention.
摘要翻译：本发明涉及通过使式NaMSixO 2 x + 1·yH 2 O的结晶片状硅酸钠得到的助洗剂组合物，其中M为钠或氢，x为数为1.9至4，y为0至20.b的数）水和c）酸性H +释放组分，其中结晶片状硅酸钠a）的d）摩尔比与酸组分c）的可释放H +的总量为4:1至1000 ：1和ee）水分b）与酸性组分c）的可释放H +的总量的摩尔比为3:1-1000:1，彼此接触。本发明还涉及洗衣洗涤剂，清洁剂，化合物和软水剂，其包含根据本发明的助洗剂组合物。

10. 发明授权

US06455491B2 Granular alkali metal phyllosilicate compound 失效
标题翻译：颗粒状碱金属页硅酸盐化合物
公开(公告)号：US06455491B2
公开(公告)日：2002-09-24
申请号：US09738583
申请日：2000-12-15
申请人： Harald Bauer , Josef Holz , Günther Schimmel
发明人： Harald Bauer , Josef Holz , Günther Schimmel
IPC分类号： C11D308
CPC分类号： C11D3/1273 , C11D1/662 , C11D1/667 , C11D1/72 , C11D1/74 , C11D3/40
摘要： The invention relates to a granular alkali metal phyllosilicate compound which comprises a crystalline alkali metal phyllosilicate, a colorant and an additive. The invention also relates to a process for its preparation, and to detergents and cleaners which comprise such a granular alkali metal phyllosilicate compound.
摘要翻译：本发明涉及一种颗粒状碱金属页硅酸盐化合物，其包含结晶性碱金属页硅酸盐，着色剂和添加剂。本发明还涉及其制备方法，以及包含这种颗粒状碱金属页硅酸盐化合物的洗涤剂和清洁剂。

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