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1. 发明授权

US5604292A Polymers with electrical and non-linear optical properties 失效
标题翻译：具有电气和非线性光学性质的聚合物
公开(公告)号：US5604292A
公开(公告)日：1997-02-18
申请号：US252701
申请日：1994-05-31
申请人： John D. Stenger-Smith , William P. Norris , Andrew P. Chafin , Scott T. Sackinger
发明人： John D. Stenger-Smith , William P. Norris , Andrew P. Chafin , Scott T. Sackinger
IPC分类号： C08G61/02 , C08F112/00
CPC分类号： C08G61/02
摘要： Novel conjugated amino substituted phenylene polymers are disclosed havingon-linear optical properties, and which can be converted to electrically conductive polymers. Such polymers are produced by reacting a novel bis-cycloalkylene sulfonium salt of 2,5,N,N-tetramethylaniline hydrochloride, such as 2,5-(N,N-dimethyl)aniline hydrochloride dimethylene bis-(tetramethylene sulfonium chloride) with alkali metal hydroxide to form a cycloalkylene sulfonium salt precursor polymer, and then heating the precursor polymer under conditions to produce the amino substituted phenylene vinylene polymer, such as poly(2-(N,N-dimethylamino) phenylene vinylene). The polymers can also be made directly by treatment of the bis chlormethyl dimethyl aniline hydrochloride derivative with alkali metal alkoxide.
摘要翻译：公开了具有非线性光学性质的新型共轭氨基取代的亚苯基聚合物，并且其可以转化为导电聚合物。这种聚合物通过使2,5，N，N-四甲基苯胺盐酸盐如2,5-（N，N-二甲基）苯胺盐酸盐二亚甲基双 - （四亚甲基锍氯化物）与碱的碱的双 - 亚环烷基锍盐金属氢氧化物以形成亚环烷基锍盐前体聚合物，然后在产生氨基取代的亚苯基亚乙烯基聚合物如聚（2-（N，N-二甲基氨基）亚苯基亚乙烯基）的条件下加热前体聚合物。聚合物也可以通过用碱金属醇盐处理双氯甲基二甲基苯胺盐酸盐衍生物直接制备。

2. 发明授权

US5587488A Bis-sulfonium salts of amino substituted bis(halomethyl) benzene 失效
标题翻译：氨基取代的双（卤代甲基）苯的双锍盐
公开(公告)号：US5587488A
公开(公告)日：1996-12-24
申请号：US441178
申请日：1995-05-10
申请人： John D. Stenger-Smith , William P. Norris , Andrew P. Chafin
发明人： John D. Stenger-Smith , William P. Norris , Andrew P. Chafin
IPC分类号： C08G61/02 , C07D409/10
CPC分类号： C08G61/02
摘要： Novel bis-sulfonium salts of amino substituted bis(halomethyl)benzene are disclosed. The sulfonium salts are prepared by reaction of an amino substituted bis(halo methyl)benzene with an aliphatic sulfide. These sulfonium salts can be made into polymer having non-linear optical properties, and polymers which can be converted to electrically conductive polymers. Such polymers are produced by reacting a novel bis-cycloalkylene sulfonium salt of 2,5,N,N-tetramethylaniline hydrochloride, such as 2,5-(N,N-dimethyl)aniline hydrochloride dimethylene bis-(tetramethylene sulfonium chloride) with alkali metal hydroxide to form a cycloalkylene sulfonium salt precursor polymer, and then heating the precursor polymer under conditions to produce the amino substituted phenylene vinylene polymer, such as poly(2-(N,N-dimethylamino) phenylene vinylene).
摘要翻译：公开了氨基取代的双（卤代甲基）苯的新型双锍盐。锍盐通过氨基取代的双（卤代甲基）苯与脂族硫醚的反应来制备。这些锍盐可以制成具有非线性光学性质的聚合物和可以转化成导电聚合物的聚合物。这种聚合物通过使2,5，N，N-四甲基苯胺盐酸盐如2,5-（N，N-二甲基）苯胺盐酸盐二亚甲基双 - （四亚甲基锍氯化物）与碱的碱的双 - 亚环烷基锍盐金属氢氧化物以形成亚环烷基锍盐前体聚合物，然后在产生氨基取代的亚苯基亚乙烯基聚合物如聚（2-（N，N-二甲基氨基）亚苯基亚乙烯基）的条件下加热前体聚合物。

3. 发明授权

US5578699A Process for making amino functional poly(para-phenylene vinylene)s 失效
标题翻译：制备氨基官能聚（对亚苯基亚乙烯基）的方法
公开(公告)号：US5578699A
公开(公告)日：1996-11-26
申请号：US457350
申请日：1995-05-18
申请人： John D. Stenger-Smith , William P. Norris , Andrew P. Chafin , Scott T. Sackinger
发明人： John D. Stenger-Smith , William P. Norris , Andrew P. Chafin , Scott T. Sackinger
IPC分类号： C08G61/02 , C08G75/00 , C08F6/00
CPC分类号： C08G61/02
摘要： A process for synthesizing novel conjugated amino substituted phenylene pmers is disclosed. The process results in polymers having non-linear optical properties, and the polymers can be converted to electrically conductive polymers. The process involves reacting a novel bis-cycloalkylene sulfonium salt of 2,5,N,N-tetramethylaniline hydrochloride, such as 2,5-(N,N-dimethyl)aniline hydrochloride dimethylene bis-(tetramethylene sulfonium chloride) with alkali metal hydroxide to form a cycloalkylene sulfonium salt precursor polymer, and then heating the precursor polymer under conditions to produce the amino substituted phenylene vinylene polymer, such as poly(2-(N,N-dimethylamino) phenylene vinylene). Another process involves treatment of the bis chlormethyl dimethyl aniline hydrochloride derivative with alkali metal alkoxide.
摘要翻译：公开了一种合成新的共轭氨基取代的亚苯基聚合物的方法。该方法导致具有非线性光学性质的聚合物，并且聚合物可以转化为导电聚合物。该方法包括使2,5，N，N-四甲基苯胺盐酸盐如2,5-（N，N-二甲基）苯胺盐酸盐二亚甲基双 - （四亚甲基氯化锍）与碱金属氢氧化物的新型双亚烷基锍盐形成亚环烷基锍盐前体聚合物，然后在产生氨基取代的亚苯基亚乙烯基聚合物如聚（2-（N，N-二甲基氨基）亚苯基亚乙烯基）的条件下加热前体聚合物。另一个方法包括用碱金属醇盐处理双氯甲基二甲基苯胺盐酸盐衍生物。

4. 发明授权

US5904990A Amino functional poly (para-phenylene vinylene)s as protective coatings 失效
标题翻译：氨基官能聚（对亚苯基亚乙烯基）作为保护涂层
公开(公告)号：US5904990A
公开(公告)日：1999-05-18
申请号：US46848
申请日：1998-03-13
申请人： John D. Stenger-Smith , Melvin H. Miles , William P. Norris , John Nelson , Peter Zarras , John W. Fischer , Andrew P. Chafin
发明人： John D. Stenger-Smith , Melvin H. Miles , William P. Norris , John Nelson , Peter Zarras , John W. Fischer , Andrew P. Chafin
IPC分类号： C09D165/00 , B32B15/04 , B32B15/08 , B32B27/00
CPC分类号： C09D165/00 , Y10T428/31504 , Y10T428/31678 , Y10T428/31692 , Y10T428/31855
摘要： Until recently, conducting polymers have been used as protective coatings.lthough these types of polymers appear to be effective in most cases, problems have resulted when attempting to bind these polymers to an aluminum surface. The polymers of this invention adhere extremely well to aluminum and aluminum alloys and thus, provide a very effective form of corrosion protection.
摘要翻译：直到最近，导电聚合物已被用作保护涂层。尽管这些类型的聚合物在大多数情况下似乎是有效的，但是当试图将这些聚合物结合到铝表面时，会产生问题。本发明的聚合物非常适合于铝和铝合金，从而提供非常有效的防腐蚀形式。

5. 发明授权

US5585522A Amino substituted bishalomethyl benzene compounds 失效
标题翻译：氨基取代的双甲基苯化合物
公开(公告)号：US5585522A
公开(公告)日：1996-12-17
申请号：US441179
申请日：1995-05-10
申请人： John D. Stenger-Smith , William P. Norris , Andrew P. Chafin
发明人： John D. Stenger-Smith , William P. Norris , Andrew P. Chafin
IPC分类号： C08G61/02 , C07C211/52
CPC分类号： C08G61/02
摘要： Novel amino substituted bishalomethyl benzene compounds, which are precurs to phenylene polymers are disclosed having non-linear optical properties, and which can be converted to electrically conductive polymers. Such polymers are produced by reacting a novel amino substituted bishalomethyl benzene compound with a dialkyl sulfide to make a bis-cycloalkylene sulfonium salt of 2,5,N,N-tetramethylaniline hydrochloride, which is 2,5-(N,N-dimethyl)aniline hydrochloride dimethylene bis-(tetramethylene sulfonium chloride) and reacting this sulfonium salt with alkali metal hydroxide to form a cycloalkylene sulfonium salt precursor polymer, and then heating the precursor polymer under conditions to produce the amino substituted phenylene vinylene polymer, such as poly(2-(N,N-dimethylamino) phenylene vinylene). The polymers can also be made directly by treatment of the bis chlormethyl dimethyl aminobenzene hydrochloride derivative with alkali metal alkoxide.
摘要翻译：公开了作为亚苯基聚合物的前体的新型氨基取代的双甲基苯化合物，其具有非线性光学性质，并且可以转化为导电聚合物。这种聚合物通过使新的氨基取代的二异丙基甲基苯化合物与二烷基硫化物反应来制备2,5-N，N-四甲基苯胺盐酸盐的双亚环烷基锍盐，其为2,5-（N，N-二甲基）苯胺盐酸盐二亚甲基双 - （四亚甲基氯化锍），并使该锍盐与碱金属氢氧化物反应形成环亚烷基锍盐前体聚合物，然后在条件下加热前体聚合物，生成氨基取代的亚苯基亚乙烯基聚合物，如聚（2 - （N，N-二甲基氨基）亚苯基亚乙烯基）。聚合物也可以通过用碱金属醇盐处理二氯甲基二甲基氨基苯盐酸盐衍生物直接制备。

6. 发明授权

US5149818A Synthesis of aminonitrobenzodifuroxan 失效
标题翻译：氨基硝基苯并二呋喃的合成
公开(公告)号：US5149818A
公开(公告)日：1992-09-22
申请号：US593413
申请日：1990-10-01
申请人： Stephen L. Christian , Andrew P. Chafin , Arnold T. Nielsen , Ronald L. Atkins , William P. Norris , Richard A. Hollins
发明人： Stephen L. Christian , Andrew P. Chafin , Arnold T. Nielsen , Ronald L. Atkins , William P. Norris , Richard A. Hollins
IPC分类号： C07D498/04
CPC分类号： C07D498/04
摘要： Aminonitrobenzodifuroxan (CL-18) is prepared by directly converting pentanitroaniline to aminonitrobenzodifuroxan with heat in the presence of an excess of sodium azide. The pentanitroaniline is prepared in high yield from 3,5-dinitroaniline with a mixture of nitric acid and sulfuric acid in which the final sulfuric acid concentration is from 99.0 to 99.5%.
摘要翻译：在过量的叠氮化钠存在下，通过加热将戊基苯胺直接转化为氨基硝基苯并二呋喃来制备氨基硝基苯并二呋喃（CL-18）。以硝酸和硫酸的混合物从3,5-二硝基苯胺以高产率制备戊基苯胺，其中最终硫酸浓度为99.0-99.5％。

7. 发明授权

US4529801A Primary explosive 失效
标题翻译：主要爆炸物
公开(公告)号：US4529801A
公开(公告)日：1985-07-16
申请号：US555775
申请日：1983-11-28
申请人： William P. Norris
发明人： William P. Norris
IPC分类号： C06B25/04 , C07D271/12 , C07D271/08
CPC分类号： C06B25/04 , C07D271/12
摘要： A primary explosive, potassium 7-hydroxyamino-4,6-dinitro-4,7-dihydrobenzroxanide ##STR1## is prepared by reacting 4,6-dinitrobenzofuroxan with hydroxylamine in a methanolic solution of potassium bicarbonate.
摘要翻译：通过使4,6-二硝基苯并呋喃与羟胺在碳酸氢钾的甲醇溶液中反应制备初级炸药，7-羟基氨基-4,6-二硝基-4,7-二氢苯并呋喃草酮。

8. 发明授权

US4008139A Fluorinated compounds 失效
标题翻译：氟化合物
公开(公告)号：US4008139A
公开(公告)日：1977-02-15
申请号：US643271
申请日：1975-12-22
申请人： Joseph H. Johnson , Alvin S. Gordon , William P. Norris
发明人： Joseph H. Johnson , Alvin S. Gordon , William P. Norris
IPC分类号： C07C31/34 , B01J1/10
CPC分类号： C07C31/34
摘要： 1,1,4,4-Tetrakis(trifluoromethyl)butan-1,4-diol and 1,1-bis (trifluoromethyl)propanol-1 are prepared by reacting gaseous hexafluoroacetone and ethane in a transparent container in the presence of sunlight. The diol is a crystalline solid and the propanol-1 is a liquid. The diol is useful as a monomer in the field of polymer chemistry. That is, polymers such as polyurethans and polyesters which find many applications in the chemical industry can be made by reacting the proper material with the diol of this invention. The propanol-1 is useful as a plasticizer for polyurethans and other plastics.
摘要翻译： 1,1'-四（三氟甲基）丁-1,4-二醇和1,1-双（三氟甲基）丙醇1是通过在阳光下存在于透明容器中的气态六氟丙酮和乙烷反应来制备的。二醇是结晶固体，丙醇-1是液体。二醇可用作聚合物化学领域的单体。也就是说，可以通过使适当的材料与本发明的二醇反应来制备在化学工业中发现许多应用的聚氨酯和聚酯的聚合物。丙醇-1可用作聚氨酯和其它塑料的增塑剂。

9. 发明授权

US4935544A Polynitrobiphenyl derivative 失效
标题翻译：聚硝基二苯基衍生物
公开(公告)号：US4935544A
公开(公告)日：1990-06-19
申请号：US171919
申请日：1980-07-17
申请人： Arnold T. Nielsen , Ronald L. Atkins , William P. Norris
发明人： Arnold T. Nielsen , Ronald L. Atkins , William P. Norris
IPC分类号： C06B25/04 , C07C211/52
CPC分类号： C06B25/04 , C07C211/52
摘要： This invention illustrates a new compound, octanitrobenzidine. It is utild as a new high energy explosive compound. Octanitrobenzidine is formed by dissolving a tetrqanitrobenzidine with sulfuric acid in the presence of a metal sulfate catalyst. This reaction mixture is further reacted with nitric and sulfuric acid at a temperature sufficient to complete the reaction, then rapidly cooled, and octanitrobenzidine is recovered.
摘要翻译：本发明说明了一种新的化合物，八硝基联苯胺。它被用作新的高能爆炸物。通过在金属硫酸盐催化剂存在下用硫酸溶解四苯胺联苯胺来形成八硝基联苯胺。该反应混合物在足以完成反应的温度下进一步与硝酸和硫酸反应，然后快速冷却，并回收辛苯三唑。

10. 发明授权

US4426539A Synthesis of the isomeric aminotetranitrotoluenes 失效
标题翻译：异构氨基四硝基甲苯的合成
公开(公告)号：US4426539A
公开(公告)日：1984-01-17
申请号：US377119
申请日：1982-05-11
申请人： Ronald L. Atkins , William P. Norris , Arnold T. Nielsen , Richard A. Hollins , William S. Wilson
发明人： Ronald L. Atkins , William P. Norris , Arnold T. Nielsen , Richard A. Hollins , William S. Wilson
IPC分类号： C06B25/04 , C07C43/20
CPC分类号： C06B25/04
摘要： Aminopolynitrotoluenes, having energetic properties, including 4-amino-2,,6-tetranitrotoluene 3-amino-2,4,5,6-tetranitrotoluene and 2-amino-3,4,5,6-tetranitrotoluene, and methods for their preparation. Also, 4-amino-N,2,3,6-tetranitrotoluene and 4-amino-N-2,3,5,6-pentanitrotoluene, each having energetic properties. Further, a process for preparing 2,3,4,5,6-pentanitrotoluene.
摘要翻译：具有能量性质的氨基多硝基甲苯，包括4-氨基-2,3,5,6-四硝基甲苯-3-氨基-2,4,5,6-四硝基甲苯和2-氨基-3,4,5,6-四硝基甲苯，以及方法为他们的准备。另外，各自具有能量性质的4-氨基-N，2,3,6-四硝基甲苯和4-氨基-N-2,3,5,6-戊二硝基甲苯。此外，制备2,3,4,5,6-五硝基甲苯的方法。

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