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1. 发明授权

US5591257A Pigment preparations based on monoazo pigments 失效
标题翻译：基于单偶氮颜料的颜料制剂
公开(公告)号：US5591257A
公开(公告)日：1997-01-07
申请号：US559572
申请日：1995-11-16
申请人： Joachim Weide , R udiger Jung , Hans J. Metz
发明人： Joachim Weide , R udiger Jung , Hans J. Metz
IPC分类号： C07D251/70 , C09B67/20 , C09B67/22 , C09D17/00 , C09B29/20 , C09D11/02
CPC分类号： C09B67/0065 , C09B67/0041
摘要： Pigment preparations comprisinga) at least one monoazo pigment of the formula (I) ##STR1## in which R is identical or different at each occurrence and is C.sub.1 -C.sub.3 -alkyl, C.sub.1 -C.sub.3 -alkoxy, chlorine or hydrogen, andn is a number from 1 to 3,b) at least one compound of the formula (II) ##STR2## in which R.sup.1 and R.sup.2 are identical or different and are a radical of the formula ##STR3## or a five- to seven-membered, saturated or unsaturated, aliphatic or aromatic heterocyclic ring which includes from 1 to 3 heteroatoms from the group consisting of nitrogen, oxygen and sulfur,m is the number 1 or 2, andX is hydrogen, an alkali metal or a stoichiometric equivalent of an alkaline earth metal;and, if desired,c) further, conventional constituents and additives are particularly suitable for the production of printing inks.
摘要翻译：包含a）至少一种式（I）的单偶氮颜料（I）其中R在每次出现时相同或不同，为C 1 -C 3 - 烷基，C 1 -C 3 - 烷氧基，氯或氢，并且n是1至3的数，b）至少一种式（II）的化合物其中R 1和R 2相同或不同，并且是下式的基团：＆lt; IMAGE＆gt; （HOCH2CH2）2N，HOCH2CH2NH或5至7元饱和或不饱和的脂族或芳族杂环，其包含1至3个来自氮，氧和硫的杂原子，m为数1或2， X为氢，碱金属或化学计量当量的碱土金属; 并且如果需要，c）进一步地，常规组分和添加剂特别适用于生产印刷油墨。

2. 发明授权

US5352281A Use of azo pigment preparations for solvent-containing packaging intaglio and flexographic printing inks 失效
标题翻译：使用偶氮颜料制剂用于含溶剂的包装凹版和柔版印刷油墨
公开(公告)号：US5352281A
公开(公告)日：1994-10-04
申请号：US115445
申请日：1993-09-01
申请人： Joachim Weide , Hans J. Metz , Ruediger Jung , Rainer Winter
发明人： Joachim Weide , Hans J. Metz , Ruediger Jung , Rainer Winter
IPC分类号： C09B67/20 , C09B41/00 , C09B67/00 , C09B67/08 , C09B67/10 , C09D11/037 , C09D11/10
CPC分类号： C09D11/037 , C09B41/005 , C09B67/0004 , C09B67/0015
摘要： Mono- and disazo pigments from the group of the acetoacetarylide, pyrazolone, .beta.-naphthol, 2-hydroxy-3-naphthanilide, 2-hydroxynaphthoic acid, benzimidazolone, diaryl yellow, diarylpyrazolone and disazobenzimidazolone pigments in whose preparation a nonionic surfactant which has a cloud point in aqueous solution was added at the latest immediately prior to the isolation, excluding pigments which have a bis(acetoacetylamino)benzene coupling component, are useful for pigmenting solvent-containing packaging intaglio and flexographic printing inks.
摘要翻译：乙酰乙酰芳胺，吡唑啉酮，β-萘酚，2-羟基-3-萘甲酰苯胺，2-羟基萘甲酸，苯并咪唑酮，二芳基黄，二芳基吡唑酮和二苯并咪唑酮颜料的单和双偶氮颜料，其制备具有云的非离子表面活性剂在分离前立即加入水溶液，不包括具有双（乙酰乙酰氨基）苯偶联组分的颜料，可用于着色含溶剂的包装凹版和柔性版印刷油墨。

3. 发明授权

US5559216A Single-step process for the preparation of bis-(acetoacetylamino) benzene disazo pigments 失效
标题翻译：用于制备双（乙酰乙酰氨基）苯二偶氮颜料的单步方法
公开(公告)号：US5559216A
公开(公告)日：1996-09-24
申请号：US115894
申请日：1993-09-01
申请人： Ruediger Jung , Joachim Weide , Hans J. Metz
发明人： Ruediger Jung , Joachim Weide , Hans J. Metz
IPC分类号： C09B33/153 , C09B41/00 , C09B67/20 , C09D11/037 , B41M1/00 , C09B56/12 , C09D11/02
CPC分类号： C09D11/037 , C09B33/153 , C09B41/005 , C09B67/006
摘要： An ecologically and economically advantageous process for preparing a disazo pigment of the formula (I) or a mixture of said disazo pigments ##STR1## where D.sup.1 and D.sup.2 are identical or different and each is unsubstituted phenyl, phenyl with from 1 to 5 substituents, unsubstituted naphthyl, naphthyl with from 1 to 3 substituents, unsubstituted anthraquinonyl, anthraquinonyl with from 1 to 3 substituents, or a radical of a fused aromatic heterocycle which contains from 1 to 3 identical or different heteroatoms from nitrogen or oxygen and sulfur and is unsubstituted or has from 1 to 3 substituents,R.sup.1 and R.sup.2 are identical or different and each is hydrogen, halogen, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.5 -alkoxycarbonyl, nitro, cyano, phenoxy or trifluoromethyl, by azo coupling, comprisesa) azo coupling in an aqueous medium and in the absence of an organic solvent in a single step andb) adding at the latest immediately prior to the isolation of the disazo pigment at least one nonionic surfactant which has a cloud point in aqueous solution.
摘要翻译：用于制备式（I）的双偶氮颜料或所述双偶氮颜料（I）的混合物的生态和经济上有利的方法，其中D1和D2相同或不同，并且各自为未取代的苯基，具有1至5个的苯基取代基，未取代的萘基，具有1至3个取代基的萘基，未取代的蒽醌基，蒽醌基与1至3个取代基，或稠合芳族杂环基团，其含有1至3个相同或不同的来自氮或氧和硫的杂原子，并且为未取代或具有1至3个取代基，R 1和R 2相同或不同，各自为氢，卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，C 1 -C 5 - 烷氧基羰基，硝基，氰基，苯氧基或三氟甲基，偶氮偶合包括：a）在水性介质中偶氮偶合，并且在单一步骤中不存在有机溶剂，和b）在分离双偶氮颜料之前立即加入至少一种非离子表面活性剂 nt在水溶液中具有浊点。

4. 发明授权

US5428136A Water-insoluble azo colorants having two azo groups and a 1,4-bis (acetoacetylamino) benzene coupling component 失效
标题翻译：具有两个偶氮基和1,4-双（乙酰乙酰氨基）苯偶联组分的水不溶性偶氮着色剂
公开(公告)号：US5428136A
公开(公告)日：1995-06-27
申请号：US99715
申请日：1993-07-29
申请人： Rudiger Jung , Joachim Weide , Hans J. Metz
发明人： Rudiger Jung , Joachim Weide , Hans J. Metz
IPC分类号： C08K5/45 , C09B33/153 , C09B63/00 , C09B67/10 , D06P1/44 , C09D11/02 , C09D17/00
CPC分类号： C09B33/153 , C09B67/0015 , Y10S534/04 , Y10S8/919 , Y10S8/924 , Y10S8/928
摘要： Disazo compounds of the formula (I) ##STR1## in which R.sup.1 and R.sup.2 are identical or different and are a hydrogen or halogen atom or a C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.5 -alkoxycarbonyl, nitro, cyano or trifluoromethyl group and the rings A, B, C and D independently of one another are unsubstituted or contain one or more substituents from the group comprising C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, carboxyl, C.sub.1 -C.sub.5 -carbalkoxy, C.sub.2 -C.sub.5 -alkanoyl, benzoyl, acyloxy, acylamino, unsubstituted or N-mono- or N,N-disubstituted carbamoyl or unsubstituted or N-mono- or N,N-disubstituted sulfamoyl, possible substituents being C.sub.1 -C.sub.4 -alkyl or mono- to trisubstituted phenyl; C.sub.1 -C.sub.4 -alkylamino or phenylamino; C.sub.1 -C.sub.4 -alkylsulfonyl or phenylsulfonyl; phenylsulfonylamino; cyano; halogen, nitro and trifluoromethyl, are suitable for coloring naturally occurring and synthetic materials, for formulating enamels, emulsion paints and printing inks, for spin coloring artificial silk and for coloring paper.
摘要翻译：其中R 1和R 2相同或不同并且是氢或卤素原子或C 1 -C 4烷基，C 1 -C 4 - 烷氧基，C 1 -C 5 - 烷氧基羰基，硝基，氰基或三氟甲基，环A，B，C和D彼此独立地是未取代的或含有一个或多个取代基，所述取代基包括C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，羧基，C 1 -C 5 - 碳酰氧基，C 2 -C 5 - 烷酰基，苯甲酰基，酰氧基，酰基氨基，未取代或N-单或N，N-二取代的氨基甲酰基或未取代或N-单或N，N-二取代的氨磺酰基，可能的取代基是C 1 -C 4烷基或单 - 三取代的苯基; C 1 -C 4烷基氨基或苯基氨基; C 1 -C 4 - 烷基磺酰基或苯基磺酰基; 苯磺酰氨基; 氰基; 卤素，硝基和三氟甲基，适用于着色天然存在和合成的材料，用于配制搪瓷，乳液漆和印刷油墨，用于旋转着色人造丝和着色纸。

5. 发明授权

US5382288A Azo pigment preparation 失效
标题翻译：偶氮颜料制剂
公开(公告)号：US5382288A
公开(公告)日：1995-01-17
申请号：US54004
申请日：1993-04-26
申请人： Karl H. Schenk , Angelika Heinrichs , Hans J. Metz
发明人： Karl H. Schenk , Angelika Heinrichs , Hans J. Metz
IPC分类号： C09B41/00 , C09B67/18 , C09B67/20 , C09B67/46 , C09D11/037 , C09D11/02
CPC分类号： C09D11/037 , C09B41/001 , C09B67/002 , C09B67/0065
摘要： Azo pigment preparations essentially comprisinga) an amide or a mixture of amides obtainable from the reactiona1) of an aminocarboxylic acid ora2) a lactam, in each case in the presence of a long-chain primary or secondary aliphatic amine ora3) of a dicarboxylic acid, a diamine and a long-chain primary or secondary aliphatic amine with one another,b) at least one diamine,c) at least one long-chain primary or secondary aliphatic amine,d) at least one azo pigment ande) if desired, further customary additives upon incorporation in halftone intaglio printing inks give glossy prints of high color strength which do not strike through even thin papers.
摘要翻译：偶氮颜料制剂基本上包含：a）可从氨基羧酸或a2）内酰胺的反应a1）得到的酰胺或酰胺混合物，在各种情况下，在长链伯或仲脂族胺存在下，或a3）二羧酸，二胺和长链伯或仲脂族胺，b）至少一种二胺，c）至少一种长链伯或仲脂族胺，d）至少一种偶氮颜料和e ）如果需要，在半色调凹版印刷油墨中加入的进一步的常规添加剂产生高色强度的光泽印刷品，其不会穿透均匀的薄纸。

6. 发明授权

US4710322A Process for the preparation of alkali metal and alkaline earth salts of benzaldehyde-2,4-di-sulfonic acid 失效
标题翻译：制备苯甲醛-2,4-二磺酸的碱金属和碱土金属盐的方法
公开(公告)号：US4710322A
公开(公告)日：1987-12-01
申请号：US21622
申请日：1987-03-02
申请人： Hans J. Metz
发明人： Hans J. Metz
IPC分类号： C07C309/44 , C07C67/00 , C07C301/00 , C07C303/00 , C07C303/02 , C07C303/20 , C07C303/32 , C07C309/28 , C07C143/38
CPC分类号： C07C309/00
摘要： The invention consists in an improved process for the preparation of salts of benzaldehyde-2,4-disulfonic acid from 2,4-dichlorobenzaldehyde. In the process 2,4-di-chlorobenzaldehyde is reacted with an aqueous solution of an alkali metal or alkaline earth sulfite and/or hydrogensulfite for a reaction time of less than 7 hours at 140.degree.-180.degree. C. to form the corresponding salt of benzaldehyde-2,4-disulfonic acid with high yield. The product has application in the electroplating industry and in the preparation triphenylmethane dyestuffs.
摘要翻译：本发明是从2,4-二氯苯甲醛制备苯甲醛-2,4-二磺酸的盐的改进方法。在该方法中，2,4-二氯苯甲醛与碱金属或碱土金属亚硫酸盐和/或亚硫酸氢钠的水溶液反应，反应时间在140-180℃下反应时间小于7小时，形成相应的盐的苯甲醛-2,4-二磺酸，产率高。该产品已应用于电镀工业和制备三苯甲烷染料。

7. 发明授权

US4937395A Process for the preparation of fluorobenzenes 失效
标题翻译：制备氟苯的方法
公开(公告)号：US4937395A
公开(公告)日：1990-06-26
申请号：US379827
申请日：1989-07-14
申请人： Heinz Litterer , Hans J. Metz , Theodor Papenfuhs , Frank P. Sistig , Ernst I. Leupold
发明人： Heinz Litterer , Hans J. Metz , Theodor Papenfuhs , Frank P. Sistig , Ernst I. Leupold
IPC分类号： B01J29/06 , B01J29/40 , B01J29/65 , B01J29/83 , B01J29/85 , B01J29/89 , C07B61/00 , C07C17/00 , C07C17/361 , C07C25/13 , C07C67/00
CPC分类号： C07C17/361
摘要： A process for the preparation of fluorobenzenes of the formula I ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 are equal or different and represent H, F, Cl or alkyl having from 1 to 3 carbon atoms, at least one of these radicals being fluorine, and S.sup.1 and S.sup.2 being equal or different and represent H or a group reducing the electron density at the benzene nucleus, which comprises subjecting a compound of the formula II ##STR2## in which R.sup.1, R.sup.2, R.sup.3, S.sup.1 and S.sup.2 have the aforementioned meaning to a decarbonylation at a zeolite catalyst.
摘要翻译：制备式I的氟苯（I）的方法，其中R 1，R 2和R 3相同或不同并且表示H，F，Cl或具有1至3个碳原子的烷基，这些基团中的至少一个是氟，S1和S2相同或不同，表示H或降低苯核的电子密度的基团，其包括使其中R 1，R 2，R 3，S 1（II）的式II化合物和S2具有上述对沸石催化剂脱碳的意义。

8. 发明授权

US4715995A Process for the preparation of alkali metal and alkaline earth salts of benzaldehyde-2,4-disulfonic acid 失效
标题翻译：制备苯甲醛-2,4-二磺酸的碱金属和碱土金属盐的方法
公开(公告)号：US4715995A
公开(公告)日：1987-12-29
申请号：US775744
申请日：1985-09-13
申请人： Hans J. Metz
发明人： Hans J. Metz
IPC分类号： C07C309/44 , C07C67/00 , C07C301/00 , C07C303/00 , C07C303/02 , C07C303/32 , C07C309/28 , C07C143/38
CPC分类号： C07C309/00
摘要： The invention consists in a single-pot process for the preparation of benzaldehyde-2,4-disulfonic acid salts from 2,4-dichlorobenzal chloride, 2,4-dichlorobenzal chloride being reacted with an aqueous solution of an alkali metal or alkaline earth sulfite and/or hydrogensulfite in the presence of acid-bonding substances at 140.degree.-180.degree. C. Benzaldehyde-2,4-disulfonic acid and its salts are used in the electroplating industry and in the preparation of triphenylmethane dyestuffs.
摘要翻译：本发明包括从2,4-二氯二氯甲苯制备苯甲醛-2,4-二磺酸盐的单锅法，将2,4-二氯二氯苄氯与碱金属或碱土金属亚硫酸盐的水溶液反应和/或亚硫酸氢钠，在140-180℃的酸键物质存在下，苯甲醛-2,4-二磺酸及其盐用于电镀工业和三苯基甲烷染料的制备。

9. 发明授权

US5464941A Biphenyl pyrazine compounds 失效
标题翻译：联苯吡嗪化合物
公开(公告)号：US5464941A
公开(公告)日：1995-11-07
申请号：US326103
申请日：1994-10-19
申请人： Richard Vicari , George Kvakovszky , Olan S. Fruchey , Hans J. Metz
发明人： Richard Vicari , George Kvakovszky , Olan S. Fruchey , Hans J. Metz
IPC分类号： C07D241/12 , C07D241/18 , C07D403/14 , C09B33/044 , C09B35/039 , C07C245/08 , C07D241/00 , C09B35/03
CPC分类号： C07D241/12 , C07D241/18 , C07D403/14 , C09B33/044 , C09B35/039
摘要： The present invention provides novel substituted biphenyl pyrazines or pyrazine derivatives ("BPD") which are functional and have useful application as a monomer for a variety of high performance polymers such as polyester, polyarylate, polycarbonate, polyetherketones, epoxides, polyimides, polyamides, and polyamides-imides; and as pigments for coating compositions such as paints. These BPD have the formula: ##STR1##
摘要翻译：本发明提供新的取代的联吡啶或吡嗪衍生物（“BPD”），它们是有用的，可用作各种高性能聚合物如聚酯，聚芳酯，聚碳酸酯，聚醚酮，环氧化物，聚酰亚胺，聚酰胺和聚酰胺酰亚胺以及用作涂料组合物如颜料的颜料。这些BPD具有以下公式：（I）

10. 发明授权

US5227531A Process for the preparation of fluorobenzaldehydes 失效
标题翻译：氟苯甲醛的制备方法
公开(公告)号：US5227531A
公开(公告)日：1993-07-13
申请号：US711365
申请日：1991-06-05
申请人： Hans J. Metz , Klaus Warning
发明人： Hans J. Metz , Klaus Warning
IPC分类号： C07C45/63 , C07C47/55
CPC分类号： C07C47/55 , C07C45/63
摘要： A process for the production of fluorobenzaldehydes which comprises reacting a chlorobenzaldehyde with an alkali fluoride in a dipolar aprotic medium.
摘要翻译：一种制备氟苯甲醛的方法，其包括在偶极非质子介质中使氯苯甲醛与碱金属氟化物反应。

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